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    石油包裹体热动力学模拟古压力改进: 饱和压力预测和体积校正

    平宏伟 陈红汉 RégisThiéry

    平宏伟, 陈红汉, RégisThiéry, 2013. 石油包裹体热动力学模拟古压力改进: 饱和压力预测和体积校正. 地球科学, 38(1): 143-155. doi: 10.3799/dqkx.2013.014
    引用本文: 平宏伟, 陈红汉, RégisThiéry, 2013. 石油包裹体热动力学模拟古压力改进: 饱和压力预测和体积校正. 地球科学, 38(1): 143-155. doi: 10.3799/dqkx.2013.014
    PING Hong-wei, CHEN Hong-han, Régis Thiéry, 2013. Improvement on Paleopressure Prediction Using Petroleum Inclusions Thermodynamic Modeling: Saturaiton Pressure Prediction and Volume Calibration. Earth Science, 38(1): 143-155. doi: 10.3799/dqkx.2013.014
    Citation: PING Hong-wei, CHEN Hong-han, Régis Thiéry, 2013. Improvement on Paleopressure Prediction Using Petroleum Inclusions Thermodynamic Modeling: Saturaiton Pressure Prediction and Volume Calibration. Earth Science, 38(1): 143-155. doi: 10.3799/dqkx.2013.014

    石油包裹体热动力学模拟古压力改进: 饱和压力预测和体积校正

    doi: 10.3799/dqkx.2013.014
    基金项目: 

    国家重点基础研究发展计划"973"项目 2012CB214804

    国家自然科学基金资助项目 41202088

    详细信息
      作者简介:

      平宏伟(1982—), 男, 讲师, 博士, 主要从事含烃流体地质研究

    • 中图分类号: P618

    Improvement on Paleopressure Prediction Using Petroleum Inclusions Thermodynamic Modeling: Saturaiton Pressure Prediction and Volume Calibration

    • 摘要: 除实验室测定参数(Th, oilTh, aquFv)外, 石油包裹体热动力学模拟古压力精度还极大地受控于石油组分模型、饱和压力预测以及气、液相摩尔体积的预测精度.在改进α-β组分模型前提下, 利用微调组分和匹配饱和压力方法改进并验证了石油流体饱和压力预测精度; 在匹配饱和压力与实验实测饱和压力前提下, 利用体积转换方法匹配22组油藏流体391个常组分膨胀实验相对体积数据, 从而改善了利用Peng-Robison状态方程计算油包裹体气泡充填度(20 ℃)和等容线的能力.最终评价了真实石油流体组分甲烷摩尔含量和等效石油流体组分甲烷摩尔含量两个组分模拟约束条件下, 改进的热动力学模拟方法和PIT软件及Vtflinc软件重构捕获压力的精度.结果表明, 改进的热动力学模拟古压力方法较其他两种方法可以有效地提高捕获压力预测的精度.考虑到石油包裹体甲烷摩尔含量难获取问题, 利用改进后的方法结合等效流体组分约束条件是重构捕获压力的理想方法组合.

       

    • 图  1  石油包裹体热动力学模拟示意(Ping et al., 2011)(a)和典型的石油流体P-T相图(b)阐述了油包裹体显微测温和体积分析需要的不同.参数气/液不混溶线由泡点线和露点线组成,临界点位于泡点线和露点线的交点

      油包裹体P-T路径通过等容线来表示,其中3个比较重要的点是油包裹体捕获点(Pt, Tt)、均一化点(Ph, Th)和室温下测定的气泡充填度P-T位置点(Pv, Tv)

      Fig.  1.  Schematic view for petroleum inclusion thermodynamic modeling (Ping et al., 2011) (a) and the typical P-T phase diagram of a petroleum, illustrating the different elements required for the analysis of microthermometric and volumetric data (b)

      表  1  不同方法劈分C7+组分结果比较

      Table  1.   Comparison results for splitting hydrocarbon plus fraction using different methods

      Al-Meshari(2005) Whitson(1983)方法 α-β模型 Katz(1983)方法 Ahmed(1989)方法
      流体编号 α β Cn+ ARD AAD ARD AAD ARD AAD ARD AAD
      1 0.81 0.80 C36+ -4.36 18.45 -67.68 24.76 -32.91 51.32 -0.37 16.74
      2 0.89 0.80 C30+ -2.58 26.78 -16.13 25.83 -32.99 62.07 -8.75 30.11
      3 0.79 0.63 C20+ 6.24 14.20 -10.67 21.15 -2.52 14.33 -2.09 10.99
      4 0.88 0.68 C20+ 9.63 17.96 9.42 17.24 -10.25 22.64 2.42 9.22
      5 0.95 0.80 C20+ 8.31 20.67 -12.41 21.65 7.81 45.61 7.33 12.87
      6 0.95 0.79 C20+ 8.62 15.86 -13.75 21.65 5.63 46.98 6.00 11.55
      7 0.94 0.72 C30+ 13.03 20.01 46.09 64.44 -34.54 48.93 -4.92 12.20
      8 0.97 0.80 C36+ 0.39 9.38 -1.87 42.41 -42.78 75.76 -11.68 21.85
      9 0.97 0.79 C45+ 10.30 22.76 -6.37 40.27 -43.53 95.01 -3.17 18.97
      10 0.96 0.67 C36+ 12.40 18.01 17.54 41.79 -43.03 69.93 -4.30 11.50
      平均值 6.19 18.41 -5.58 32.12 -22.91 53.26 -1.95 15.60
      下载: 导出CSV

      表  2  石油饱和条件下压力-温度-组分实验数据来源

      Table  2.   References of experimental data from the literature

      下载: 导出CSV

      表  3  计算未改进α-β组分模型中单个碳数组分(C7~C500)动力学参数方法

      Table  3.   Methods for calculating the thermodynamics parameters of SCN (C7 to C500) for unimproved α-β composition model

      方法 正常沸点温度(Tb) 临界温度(Tc) 临界压力(Pc) 偏心因子(ω)
      Thiéry et al.(2002) - - - -
      T-method 1 Twu (1984) Twu (1984) Twu (1984) Kesler-Lee (1976)
      T-method 2 Twu (1984) Kesler-Lee (1976) Kesler-Lee (1976) Kesler-Lee (1976)
      T-method 3 Pedersen (1985) Pedersen (1989) Pedersen (1989) Kesler-Lee (1976)
      T-method 4 Pedersen (1985) Kesler-Lee (1976) Kesler-Lee (1976) Kesler-Lee (1976)
      下载: 导出CSV

      表  4  石油饱和条件下压力-温度-组分实验数据来源

      Table  4.   References of experimental data from the literature (P-T-composition conditions of petroleum saturations)

      下载: 导出CSV

      表  5  不同方法预测饱和压力误差分析

      Table  5.   Error analysis of different methods for calculation of saturation pressures

      Model-1 Model-2 Thiéry et al. (2002) T-method 1 T-method 2 T-method 3 T-method 4
      ARD -0.64 -1.51 8.70 -23.47 -9.39 3.85 -6.27
      AAD 6.23 5.12 29.50 23.65 12.56 10.56 10.95
      下载: 导出CSV

      表  6  用于改进和验证模型的输入组分范围

      Table  6.   Composition range used for developing and testing the proposed model

      用于改进模型的数据范围(mol%) 验证改进模型数据范围(mol%)
      最小值 平均值 最大值 最小值 平均值 最大值
      N2 0.00 0.50 3.95 0.00 0.91 3.91
      CO2 0.00 1.17 9.11 0.05 1.61 3.67
      H2S 0.00 0.20 4.99 0.00 0.56 4.99
      C1 0.64 35.59 74.18 6.20 46.38 70.20
      C2 0.56 7.68 14.09 1.63 9.21 14.09
      C3 0.43 6.21 11.87 1.18 6.30 10.48
      C4 0.95 4.47 8.43 1.25 4.19 8.40
      C5 0.40 3.19 6.65 0.82 2.80 5.85
      C6 0.00 3.07 6.65 0.59 2.22 4.84
      C7+ 9.87 37.97 84.41 9.87 25.90 67.69
      温度(℃) 26.70 84.08 156.67 26.70 94.87 132.50
      饱和压力(MPa) 0.55 17.88 51.39 9.69 25.78 46.68
      下载: 导出CSV

      表  7  利用T-method 3方法计算的捕获压力误差分析

      Table  7.   Error analysis of trapping pressure reconstruction for T-method 3

      Th, oil (℃) 80 80 80 120 120 120
      Tt (℃) 95 110 125 135 150 165
      AAD%(Pt) 12.05 12.24 13.13 11.43 11.50 11.56
      ACD%(P sat) 8.08 6.21 5.06 8.50 6.78 5.68
      ACD%(Piso) 4.34 6.34 7.20 3.42 5.02 6.08
      下载: 导出CSV

      表  8  利用Vtflinc软件计算的捕获压力误差分析

      Table  8.   Error analysis of trapping pressure construction for Vtflinc software

      Th, oil (℃) 80 80 80 120 120 120
      Tt (℃) 95 110 125 135 150 165
      AAD%(Pt) 10.70 9.52 9.24 7.84 8.08 7.80
      ACD%(Psat) 7.38 5.23 4.08 5.96 4.39 3.52
      ACD%(Piso) 3.55 4.59 5.38 2.24 3.15 3.68
      下载: 导出CSV

      表  9  不同的约束组分模拟的方法列表

      Table  9.   Methods for trapping pressure reconstruction with different constraint on composition modeling

      捕获压力重构方法 输入参数 组分约束条件
      本文方法 Th, oilFvTt 真实流体中甲烷的摩尔百分含量等效流体中甲烷的摩尔百分含量
      Thiéry et al.(2000, 2002)PIT软件 Th, oilFvTt 真实流体中甲烷的摩尔百分含量等效流体中甲烷的摩尔百分含量
      Aplin et al.(1999)Vtflinc软件 输入组分、Th, oilFvTt 真实流体及其各组分热动力学参数(TcPcω)等效流体组分及各组分热动力学参数(TcPcω)
      下载: 导出CSV

      表  10  不同方法重构捕获压力的总体误差分析

      Table  10.   Global error analysis of trapping pressure reconstruction for different methods

      捕获压力重构方法 本文方法 Thiéry et al.(2000, 2002)PIT软件 Aplin et al.(1999)Vtflinc软件
      组分约束条件 C1%(mol)-等效流体 C1%(mol)-真实流体 C1%(mol)-等效流体 C1%(mol)-真实流体 C1%(mol)-等效流体 C1%(mol)-真实流体
      最小绝对误差(AD%) 0.08 0.03 0.47 0.55 0.75 0.13
      最大绝对误差(AD%) 39.73 26.47 84.24 89.52 62.25 28.59
      平均绝对误差(AAD%) 12.06 6.46 20.58 14.12 19.91 7.84
      下载: 导出CSV
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    • 收稿日期:  2012-09-28
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