吉林延边地区棉田岩体锆石U-Pb年代学、地球化学及Hf同位素

刘金龙; 孙丰月; 林博磊; 王英德; 王硕; 胡安新

doi:10.3799/dqkx.2015.004

吉林延边地区棉田岩体锆石U-Pb年代学、地球化学及Hf同位素

doi: 10.3799/dqkx.2015.004

1.
吉林大学地球科学学院, 吉林长春 130061
2.
国土资源部信息中心, 北京 100812

基金项目:

吉黑东部区域成矿规律综合研究 1212011085485

国家自然科学基金项目 41272093

详细信息

作者简介:
刘金龙(1988-), 男, 博士研究生, 主要从事矿床学研究.E-mail: liujinlong0815@yeah.net

通讯作者:
孙丰月, E-mail: sfy@jlu.edu.cn

中图分类号: P581
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出版历程
- 收稿日期: 2014-03-10
- 刊出日期: 2015-01-15

Geochronology, Geochemistry and Zircon Hf Isotope of Miantian Granodiorite Intrusion in Yanbian Region, Southern Jinlin Province and Its Geological Significance

1.
College of Earth Sciences, Jilin University, Changchun 130061, China
2.
Information Center of Ministry of Land and Resources of People's Republic of China, Beijing 100812, China

摘要

摘要: 对延边地区棉田花岗闪长岩岩体进行了锆石U-Pb年代学、岩石地球化学以及Hf同位素的研究, 以便对其岩石成因和古太平洋板块俯冲作用的开始时间给予制约.棉田岩体主要由花岗闪长岩和次要的花岗岩组成, 花岗闪长岩中锆石LA-ICP-MS U-Pb定年结果表明, 该岩体形成于早侏罗世(177±2 Ma, MSWD=1.13).在地球化学研究方面, 它们属于高钾钙碱性-钙碱性系列, A/CNK值介于0.88~1.12之间, 属准铝质, 为I型花岗岩, 并且明显富集大离子亲石元素(如K、Ba、Rb)、轻稀土元素(LREE)以及Th、U, 相对亏损高场强元素(如Ta、Nb、Ti、P).岩石的ε_Hf(t)值和二阶段模式年龄(T_DM2)分别介于±8.72~±12.28和437~663 Ma之间.结果表明, 岩体的原始岩浆源于新增生陆壳的部分熔融.综合区域同时代火成岩的研究成果, 认为棉田花岗闪长岩岩体形成于古太平洋板块向欧亚大陆俯冲下的火山弧环境.
- 锆石U-Pb年龄 /
- 锆石Hf同位素 /
- 地球化学 /
- 延边
Abstract: This paper presents LA-ICP-MS zircon U-Pb dating, geochemical and Hf isotopic data of the granodiorite from Miantian intrusion in Yanbian region, with the aim of constraining its petrogenesis and beginning time of subduction of the Paleo-Pacific plate beneath the Eurasian continent. The Miantian intrusion consists mainly of granodiorite with minor diorite. The LA-ICP-MS U-Pb dating results of zircons from the granodiorite indicate that the intrusion formed in the Early Jurassic (177±2 Ma, MSWD=1.13). Geochemically, these rocks fall into the calc-alkaline to high-K calc-alkaline series, with A/CNK ratios of 0.88-1.12, which are sub-aluminous granites, being of the characteristics of I type granitoids, enrichment in LILE (such as K, Ba, Rb), LREE, Th and U, relatively depleted in HFSE (such as Ta, Nb, Ti, P). The ε_Hf(t) values of the granodiorite vary from ±8.72 to ±12.28, and two-stage model ages (T_DM2) vary from 437 to 663 Ma. These characteristics suggest that the primary magma was derived from the remelting of juvenile crustal materials (Neoproterozoic to Early Paleozoic). It is concluded that granodiorite from Miantian intrusion formed in compressional structure setting similar to volcanic arc which could be related to the subduction of the Paleo-Pacific plate beneath the Eurasian continent.
- zircon U-Pb chronology /
- zircon Hf isotope /
- geochemistry /
- Yanbian

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图 1 研究区地质略图

1.新生代地层及火山岩；2.中生代地层；3.二叠系；4.仲平岩体；5.棉田岩体；6.其他花岗岩；7.断层；8.采样位置；9.地名；a图据Wu et al., 2011; b图据逄伟，2009; Zhang et al., 2004

Fig. 1. Geological sketch map of the studied area

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图 2 花岗闪长岩显微照片

a.花岗闪长岩(-)；b.花岗闪长岩(+)；Bt.黑云母；Or.正长石；Pl.斜长石；Qz.石英

Fig. 2. Microphotographs of the granite rocks in Miantian

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图 3 花岗闪长岩锆石CL图像

Fig. 3. CL images of zircons from the granodiorite

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图 4 花岗闪长岩的U-Pb年龄谐和图(a)和加权平均年龄(b)

Fig. 4. Zircon U-Pb Concordia diagram (a) and weighted average ages diagram (b) from the granodiorite

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图 5 岩石TAS(a)和K₂O-SiO₂图解(b)

a.分界线上方为碱性，下方为亚碱性，据Irvine and Baragar, 1971；①小兴安岭-张广才岭地区基性-超基性岩；②东宁-汪清-珲春地区中基性岩；③小兴安岭-张广才岭地区酸性岩(Wu et al., 2002; 孙德有，2005b；许文良等，2008; Yu et al., 2012; Xu et al., 2013)

Fig. 5. TAS diagram and K₂O-SiO₂ diagram of the granodiorite in Miantian

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图 6 岩石稀土元素球粒陨石标准化配分图解(a)和微量元素原始地幔标准化蛛网图(b)

a.标准化值据Boynton, 1984; b.标准化值据Sun and Mcdonough, 1989

Fig. 6. Chondrite-normalized REE distribution patterns and primitive mantle-normalized trace element spider diagrams of the granodiorite

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图 7 岩石的Hf同位素特征

据Yang et al., 2006

Fig. 7. Hf isotopic compositions of the granodiorite

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图 8 岩石R1-R2判别图解

据Bachelor and Bowden, 1985

Fig. 8. R1-R2 factor diagram of the granodiorite

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图 9 岩石Hf-Rb/30-3Ta判别图解

据Brown et al., 1984

Fig. 9. Hf-Rb/30-3Ta diagram of the granodiorite

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表 1 花岗闪长岩中锆石LA-ICP-MS U-Pb同位素分析结果

Table 1. LA-ICP-MS zircon U-Pb analyses of the granodiorite rocks

样品	Th(10^-3)	U(10^-3)	Th/U	²⁰⁷Pb/²⁰⁶Pb		²⁰⁷Pb/²³⁵U		²⁰⁶Pb/²³⁸U		²⁰⁶Pb/²³⁸U
样品	Th(10^-3)	U(10^-3)	Th/U	比值	1σ	比值	1σ	比值	1σ	t(Ma)	1σ
NZ-N7-1	218	529	0.412 02	0.052 85	0.002 72	0.204 51	0.008 60	0.028 07	0.000 43	178	3
NZ-N7-2	279	390	0.715 44	0.053 10	0.006 43	0.201 07	0.023 18	0.027 47	0.000 82	175	5
NZ-N7-3	450	642	0.701 93	0.051 40	0.004 30	0.196 77	0.015 18	0.027 77	0.000 60	177	4
NZ-N7-4	307	498	0.616 80	0.050 57	0.002 43	0.196 36	0.007 52	0.028 16	0.000 42	179	3
NZ-N7-5	171	360	0.475 65	0.052 12	0.003 33	0.206 61	0.011 63	0.028 75	0.000 51	183	3
NZ-N7-6	278	398	0.700 28	0.052 57	0.002 81	0.197 40	0.008 81	0.027 23	0.000 44	173	3
NZ-N7-7	381	624	0.610 49	0.052 57	0.007 89	0.199 56	0.028 81	0.027 53	0.000 99	175	6
NZ-N7-8	145	268	0.540 43	0.051 02	0.003 40	0.199 82	0.011 87	0.028 40	0.000 52	181	3
NZ-N7-9	266	467	0.569 46	0.048 23	0.004 79	0.180 23	0.016 84	0.027 09	0.000 66	172	4
NZ-N7-10	360	669	0.537 67	0.051 32	0.002 29	0.199 14	0.006 84	0.028 13	0.000 43	179	3
NZ-N7-11	218	420	0.519 58	0.050 94	0.004 08	0.198 36	0.014 62	0.028 23	0.000 61	179	4
NZ-N7-12	251	410	0.611 60	0.051 43	0.004 32	0.190 19	0.014 81	0.026 80	0.000 60	170	4
NZ-N7-13	137	329	0.414 37	0.052 02	0.002 89	0.200 26	0.009 45	0.027 91	0.000 48	177	3

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表 2 棉田花岗闪长岩主量元素、稀土元素和微量元素含量及有关参数

Table 2. Major, REE and trace element content and parameter of the granodiorite in Miantian

样品	NZ-Y-1	NZ-Y-2	NZ-Y-3	NZ-Y-4	NZ-Y-5	NZ-Y-6	NZ-Y-7	NZ-Y-8	NZ-Y-9
SiO₂	62.19	63.13	64.08	63.04	63.22	63.10	63.70	62.61	63.41
TiO₂	0.70	0.68	0.62	0.64	0.68	0.66	0.66	0.67	0.71
Al₂O₃	16.31	16.24	15.97	16.11	15.97	16.46	16.05	15.91	16.37
Fe₂O₃	5.53	5.06	4.59	5.01	5.17	5.09	4.97	5.02	5.21
MnO	0.09	0.08	0.07	0.08	0.08	0.08	0.08	0.09	0.08
MgO	2.31	2.19	1.98	2.11	2.17	2.08	2.19	2.12	2.24
CaO	4.88	4.53	2.82	4.66	4.46	4.45	4.49	4.88	4.48
Na₂O	4.00	3.94	3.70	3.86	3.81	3.88	3.84	3.82	3.93
K₂O	2.38	2.43	2.87	2.59	2.43	2.26	2.31	2.62	2.34
P₂O₅	0.14	0.13	0.13	0.13	0.13	0.13	0.13	0.13	0.13
LOI	1.04	1.32	2.93	1.25	1.30	1.49	1.15	1.96	1.03
Total	99.64	99.80	99.82	99.56	99.49	99.75	99.63	99.92	100.00
ALK	6.38	6.37	6.57	6.45	6.24	6.14	6.15	6.44	6.27
Na₂O/K₂O	1.67	1.61	1.28	1.49	1.56	1.72	1.67	1.45	1.67
A/CNK	0.91	0.89	0.92	1.04	0.91	0.94	1.12	0.91	0.94
Mg^#	44.70	45.30	45.40	45.50	45.60	46.00	46.10	46.20	46.60
La	20.80	19.20	16.90	18.80	19.00	21.00	18.80	18.50	17.20
Ce	43.40	39.60	35.50	37.30	39.30	43.80	38.90	37.10	35.30
Pr	5.14	4.65	4.13	4.21	4.67	5.24	4.59	4.29	4.15
Nd	18.90	16.90	14.80	14.80	17.40	18.80	16.90	15.50	15.00
Sm	3.95	3.45	2.94	2.98	3.63	4.03	3.43	3.18	3.08
Eu	0.90	0.85	0.69	1.05	0.84	0.89	0.89	0.88	0.84
Gd	2.97	2.66	1.99	3.47	2.93	3.21	2.85	2.79	2.67
Tb	0.47	0.41	0.29	0.50	0.45	0.51	0.43	0.43	0.41
Dy	3.11	2.65	1.86	3.01	2.95	3.25	2.71	2.63	2.51
Ho	0.62	0.54	0.37	0.60	0.60	0.67	0.56	0.54	0.52
Er	1.70	1.45	1.07	1.67	1.60	1.74	1.50	1.41	1.39
Tm	0.29	0.25	0.18	0.29	0.28	0.30	0.25	0.25	0.23
Yb	1.81	1.57	1.21	1.72	1.70	1.83	1.58	1.45	1.44
Lu	0.28	0.24	0.19	0.25	0.26	0.28	0.24	0.24	0.22
Y	17.70	15.80	10.10	15.90	16.60	18.80	15.70	14.90	14.80
ΣREE	104.00	94.40	82.10	90.70	95.60	105.60	93.60	89.20	85.00
LREE	93.10	84.70	75.00	79.10	84.80	93.80	83.50	79.50	75.60
HREE	11.30	9.80	7.20	11.50	10.80	11.80	10.10	9.74	9.39
LREE/HREE	8.27	8.66	10.47	6.88	7.88	7.95	8.25	8.16	8.05
La_N/Yb_N	8.24	8.77	10.02	7.84	8.02	8.23	8.53	9.15	8.57
δEu	0.80	0.86	0.87	1.00	0.79	0.76	0.87	0.90	0.90
δCe	1.03	1.03	1.04	1.03	1.02	1.02	1.03	1.02	1.02
Rb	73.40	73.30	91.70	88.40	72.80	65.00	66.60	77.30	71.90
Ba	418.00	420.00	479.00	458.00	420.00	409.00	431.00	537.00	439.00
Th	10.80	10.90	13.30	9.30	10.70	10.80	10.30	8.70	7.96
U	2.11	1.96	1.39	2.13	3.15	3.68	3.09	2.51	1.74
Nb	5.60	5.30	5.10	5.50	5.60	5.80	5.60	5.20	5.30
Ta	0.60	0.60	0.50	0.60	0.60	0.60	0.60	0.50	0.50
Sr	366.00	365.00	344.00	433.00	386.00	397.00	383.00	439.00	389.00
Nd	18.90	16.90	14.80	14.80	17.40	18.80	16.90	15.50	15.00
Zr	150.00	140.00	130.00	120.00	150.00	130.00	130.00	140.00	160.00
Hf	4.00	3.70	3.60	3.30	4.20	3.50	3.70	3.80	4.00
Nb/Ta	9.33	8.83	10.20	9.17	9.33	9.67	9.33	10.40	10.6
Rb/Sr	0.20	0.20	0.27	0.20	0.19	0.16	0.17	0.19	0.18
Hf/Th	0.37	0.34	0.27	0.35	0.39	0.33	0.36	0.44	0.50
La/Nb	3.71	3.62	3.31	3.42	3.39	3.62	3.36	3.56	3.25
注：主量元素单位为10^-2；微量、稀土元素单位为10^-6，ALK=K₂O+Na₂O；A/CNK=Al₂O₃/(CaO+Na₂O+K₂O)，分子比；Na₂O/K₂O重量比；Mg^#=100×(MgO/40.31)/(MgO/40.31+Fe₂O₃^T×2/159.7).

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表 3 棉田花岗闪长岩锆石Hf同位素分析结果

Table 3. LA-ICPMS zircon U-Pb analyses of the granodiorite in Miantian

样品	t(Ma)	¹⁷⁶Yb/¹⁷⁷Hf	¹⁷⁶Lu/¹⁷⁷Hf	¹⁷⁶Hf/¹⁷⁷Hf	¹⁷⁶Hf/¹⁷⁷Hf(corr)	2σ	ε_Hf(0)	ε_Hf(t)	2σ	T_DM1(Hf)	T_DM2(Hf)	f_Lu/Hf
NZ-N7-1	178	0.038 490	0.001 218	0.282 963	0.282 940	0.000 017	5.94	9.71	0.59	445	602	-0.96
NZ-N7-2	175	0.037 450	0.001 153	0.282 937	0.282 914	0.000 018	5.01	8.72	0.64	482	663	-0.97
NZ-N7-3	177	0.048 968	0.001 568	0.282 973	0.282 950	0.000 016	6.28	9.98	0.58	436	584	-0.95
NZ-N7-4	179	0.025 767	0.000 773	0.282 979	0.282 956	0.000 018	6.50	10.34	0.64	418	562	-0.98
NZ-N7-5	183	0.040 833	0.001 175	0.283 011	0.282 988	0.000 016	7.62	11.50	0.55	377	491	-0.96
NZ-N7-6	173	0.042 915	0.001 219	0.283 007	0.282 984	0.000 016	7.49	11.15	0.57	383	506	-0.96
NZ-N7-7	175	0.042 466	0.001 236	0.283 025	0.283 002	0.000 015	8.15	11.85	0.54	356	462	-0.96
NZ-N7-8	181	0.043 538	0.001 231	0.282 954	0.282 931	0.000 016	5.63	9.46	0.56	458	620	-0.96
NZ-N7-9	172	0.059 948	0.001 793	0.283 017	0.282 994	0.000 017	7.86	11.44	0.61	373	486	-0.95
NZ-N7-10	179	0.044 000	0.001 264	0.283 035	0.283 012	0.000 017	8.50	12.28	0.59	342	437	-0.96
NZ-N7-11	179	0.046 063	0.001 391	0.282 960	0.282 937	0.000 012	5.82	9.59	0.42	452	610	-0.96
NZ-N7-12	170	0.052 283	0.001 667	0.283 018	0.282 995	0.000 015	7.90	11.45	0.55	370	484	-0.95
NZ-N7-13	177	0.045 334	0.001 643	0.282 992	0.282 969	0.000 015	6.96	10.65	0.54	409	541	-0.95

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