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    辽宁省清原县南口前岩体锆石U-Pb年代学、地球化学及Hf同位素

    刘金龙 孙丰月 张雅静 马芳 刘峰旭 曾乐

    刘金龙, 孙丰月, 张雅静, 马芳, 刘峰旭, 曾乐, 2016. 辽宁省清原县南口前岩体锆石U-Pb年代学、地球化学及Hf同位素. 地球科学, 41(1): 55-66. doi: 10.3799/dqkx.2016.004
    引用本文: 刘金龙, 孙丰月, 张雅静, 马芳, 刘峰旭, 曾乐, 2016. 辽宁省清原县南口前岩体锆石U-Pb年代学、地球化学及Hf同位素. 地球科学, 41(1): 55-66. doi: 10.3799/dqkx.2016.004
    Liu Jinlong, Sun Fengyue, Zhang Yajing, Ma Fang, Liu Fengxu, Zeng Le, 2016. Zircon U-Pb Geochronolog, Geochemistry and Hf Isotopes of Nankouqian Granitic Intrusion in Qingyuan Region, Liaoning Province. Earth Science, 41(1): 55-66. doi: 10.3799/dqkx.2016.004
    Citation: Liu Jinlong, Sun Fengyue, Zhang Yajing, Ma Fang, Liu Fengxu, Zeng Le, 2016. Zircon U-Pb Geochronolog, Geochemistry and Hf Isotopes of Nankouqian Granitic Intrusion in Qingyuan Region, Liaoning Province. Earth Science, 41(1): 55-66. doi: 10.3799/dqkx.2016.004

    辽宁省清原县南口前岩体锆石U-Pb年代学、地球化学及Hf同位素

    doi: 10.3799/dqkx.2016.004
    基金项目: 

    全国危机矿山接替资源找矿项目 200623018

    中国地质调查局地质大调查项目 1212010630708

    全国危机矿山接替资源找矿项目 200823003

    详细信息
      作者简介:

      刘金龙(1988-),男,博士研究生,主要从事矿床学研究.E-mail:liujinlong0815@yeah.net

      通讯作者:

      孙丰月, E-mail:sfy@jlu.edu.cn

    • 中图分类号: P581

    Zircon U-Pb Geochronolog, Geochemistry and Hf Isotopes of Nankouqian Granitic Intrusion in Qingyuan Region, Liaoning Province

    • 摘要: 华北板块周边地区板块的俯冲与碰撞对华北后来的岩石圈破坏可能产生了重要影响.对南口前岩体进行了锆石LA-ICP-MS U-Pb年代学和岩石地球化学研究,确定其时代及形成的构造背景.测年结果表明,岩石为晚三叠世(224±1 Ma)岩浆侵入的产物.地球化学研究表明岩石为高钾钙碱性系列,A/CNK值为0.98~1.07,属准铝质-过铝质花岗岩类.高Sr(394×10-6~545×10-6),低Yb(0.61×10-6~0.93×10-6),判断岩石属于埃达克岩类.岩石的εHf(t)值为-13.2~-6.9,二阶段模式年龄(TDM2)变化于1 669~1 825 Ma之间,判断岩石源于元古代地壳岩石的部分熔融.综合前人研究成果,认为岩石形成于古亚洲洋闭合后的造山后拉张环境.

       

    • 图  1  中-晚三叠世华北板块北缘碱性岩分布

      Peng et al.(2008)

      Fig.  1.  Middle to Late Triassic syenite plutons in the north margin of North China plate

      图  2  研究区地质略图

      1.晚白垩世砾岩;2.早白垩世砾岩;3.早白垩世页岩夹泥灰岩;4.早白垩世中基性火山岩;5.晚侏罗世凝灰质粉砂岩;6.太古代绿岩;7.三叠纪晚期细粒花岗岩;8.三叠纪晚期中细粒花岗岩;9.三叠纪晚期中粗粒似斑状黑云母花岗岩;10.三叠纪晚期粗粒似斑状黑云母花岗岩;11.三叠纪晚期中细粒花岗闪长岩;12.三叠纪晚期似斑状花岗闪长岩;13.三叠纪早期花岗闪长岩;14.太古代花岗岩;15.断层(推测);16.取样点;据卢崇海(1988)

      Fig.  2.  Geological sketch map of the studied area

      图  3  南口前花岗岩显微照片(+)

      Bi.黑云母;Mi.微斜长石;Pl.斜长石;Or.正长石;Q.石英

      Fig.  3.  Microphotographs of the granite rocks in Nankouqian

      图  4  南口前花岗岩部分锆石阴极发光图像

      Fig.  4.  CL images of zircons from the granite rocks in Nankouqian

      图  5  南口前花岗岩的U-Pb年龄谐和图(a)和加权平均年龄(b)

      Fig.  5.  Zircon U-Pb Concordia diagram (a) and weighted average ages diagram (b) from the granite rocks in Nankouqian

      图  6  南口前花岗岩的TAS图

      1.橄榄辉长岩;2a.碱性辉长岩;2b.亚碱性辉长岩;3.辉长闪长岩;4.闪长岩;5.花岗闪长岩;6.花岗岩;7.硅英岩;8.二长辉长岩;9.二长闪长岩;10.二长岩;11.石英二长岩;12.正长岩;13.副长石辉长岩;14.副长石二长闪长;15.副长石二长正长岩;16.副长正长岩;17.副长深成岩;18.霓方钠岩/磷霞岩/粗白榴岩;分界线上方为碱性,下方为亚碱性据Irvine and Baragar(1971)

      Fig.  6.  TAS diagram for the granite rocks in Nankouqian

      图  7  南口前花岗岩的SiO2-K2O图

      Fig.  7.  K2O-SiO2 diagram of the granite rocks in Nankouqian

      图  8  南口前花岗岩稀土元素球粒陨石标准化配分图

      Boynton(1984)

      Fig.  8.  Chondrte-normalized REE patterns of the granite rocks in Nankouqian

      图  9  南口前花岗岩微量元素原始地幔标准化蛛网图

      Sun and McDonough(1989)

      Fig.  9.  Primitive mantle-normalized trace element spider diagams of the granite rocks in Nankouqian

      图  10  南口前花岗岩的Hf同位素特征

      Yang et al.(2006)

      Fig.  10.  Hf isotopic compositions of the granite rocks in Nankouqian

      图  11  南口前花岗岩Sr/Y-Y图解

      Defant and Drummond(1990)

      Fig.  11.  Sr/Y-Y diagram for the granite rocks in Nankouqian

      表  1  南口前花岗岩锆石LA-ICP-MS U-Pb同位素分析结果

      Table  1.   LA-ICP-MS zircon U-Pb analyses of the granite rocks in Nankouqian

      测点 含量(10-6) 同位素比值及误差 年龄(Ma)及误差
      238U 232Th 207Pb/206Pb 1σ 207Pb/235U 1σ 206Pb/238U 1σ 207Pb/235U 1σ 206Pb/238U 1σ
      XDP-2-1 769 284 0.050 26 0.001 58 0.247 06 0.007 64 0.035 46 0.000 26 224 6 225 2
      XDP-2-2 488 179 0.050 51 0.001 18 0.247 18 0.005 57 0.035 37 0.000 31 224 5 224 2
      XDP-2-3 829 373 0.050 76 0.004 40 0.24 61 0.019 15 0.035 21 0.000 95 224 16 223 6
      XDP-2-4 973 524 0.050 79 0.002 02 0.246 77 0.009 33 0.035 08 0.000 42 224 8 222 3
      XDP-2-5 464 204 0.050 61 0.005 09 0.247 08 0.023 76 0.035 40 0.000 58 224 19 224 4
      XDP-2-6 931 343 0.050 73 0.004 20 0.246 02 0.020 98 0.035 04 0.000 79 223 17 222 5
      XDP-2-7 965 343 0.050 11 0.003 84 0.247 68 0.018 97 0.035 76 0.000 57 225 15 227 4
      XDP-2-8 852 378 0.049 69 0.003 27 0.246 06 0.017 04 0.035 69 0.000 41 223 14 226 3
      XDP-2-9 895 509 0.049 88 0.003 48 0.246 83 0.017 40 0.035 59 0.000 46 224 14 225 3
      XDP-2-10 489 155 0.050 88 0.006 42 0.245 76 0.028 54 0.035 35 0.001 34 223 23 224 8
      XDP-2-11 722 269 0.050 39 0.001 60 0.247 39 0.007 71 0.035 41 0.000 32 224 6 224 2
      XDP-2-12 800 279 0.050 71 0.001 84 0.246 81 0.008 27 0.035 22 0.000 38 224 7 223 2
      XDP-2-13 876 425 0.050 52 0.004 29 0.247 06 0.019 59 0.035 45 0.000 37 224 16 225 2
      XDP-2-14 315 273 0.050 29 0.001 96 0.246 89 0.009 40 0.035 41 0.000 38 224 8 224 2
      下载: 导出CSV

      表  2  南口前花岗岩主量元素、稀土元素和微量元素含量及有关参数

      Table  2.   Major, REE and trace element content and parameter of the granite rocks in Nankouqian

      样品 XDP-1-1 XDP-1-2 XDP-1-3 XDP-1-4 XDP-1-5 XDP-1-6 XDP-1-7
      SiO2 71.64 70.68 68.93 69.8 69.18 70.95 71.78
      TiO2 0.23 0.30 0.33 0.31 0.33 0.31 0.27
      Al2O3 13.86 13.98 14.42 14.47 14.49 13.85 14.46
      Fe2O3 1.82 2.13 1.97 2.08 2.16 2.24 1.57
      MnO 0.03 0.03 0.03 0.02 0.03 0.03 0.02
      MgO 0.49 0.66 0.64 0.66 0.58 0.62 0.32
      CaO 1.45 1.73 1.72 1.29 1.74 1.23 0.95
      Na2O 4.19 4.27 4.29 4.41 4.43 4.44 4.30
      K2O 4.18 3.81 3.95 4.13 3.83 3.58 4.34
      P2O5 0.10 0.12 0.13 0.12 0.14 0.13 0.11
      LOI 1.01 0.94 2.19 1.51 2.06 1.61 1.51
      Total 99.14 98.83 98.73 98.96 99.11 99.13 99.78
      Mg# 34.8 38.0 39.2 38.6 34.7 35.4 28.8
      A/CNK 0.99 0.98 1.00 1.03 0.99 1.03 1.07
      Cr 20 20 20 20 20 20 20
      V 29 34 35 29 32 34 26
      Rb 126 103 119 118 117 104 134
      Ba 814 963 822 958 847 840 889
      Sr 423 545 509 400 441 395 394
      Ce 51.3 72.5 75.8 74.4 78.7 77.9 70.7
      Pr 4.8 7.6 8.1 7.0 8.4 7.6 6.6
      Nb 15.8 21.1 22.3 19.3 22.1 21.4 25
      Ta 1.4 1.8 1.9 1.7 1.8 1.8 2.3
      Zr 159 153 190 166 172 186 172
      Th 16.5 18.5 17.5 24.8 19.0 19.5 18.6
      U 2.60 4.50 3.00 3.20 2.70 3.60 8.30
      La 28.3 46.0 47.6 40.6 49.4 45.2 39.7
      Nd 15.5 24.4 26.0 22.6 26.8 24.3 21.2
      Hf 3.90 3.90 4.90 4.10 4.50 4.90 5.50
      Sm 2.22 3.35 3.64 3.16 3.71 3.37 2.83
      Eu 0.61 0.91 0.90 0.85 0.92 0.84 0.74
      Gd 1.60 2.51 2.59 2.31 2.56 2.27 2.09
      Tb 0.21 0.32 0.33 0.30 0.33 0.30 0.25
      Dy 1.07 1.66 1.70 1.54 1.72 1.58 1.26
      Ho 0.19 0.31 0.30 0.28 0.31 0.28 0.22
      Er 0.60 0.91 0.93 0.84 0.92 0.85 0.66
      Tm 0.10 0.14 0.14 0.13 0.14 0.14 0.11
      Yb 0.61 0.87 0.88 0.80 0.93 0.82 0.72
      Lu 0.10 0.12 0.13 0.13 0.14 0.13 0.12
      Y 6.20 9.20 9.50 8.50 9.50 9.00 7.10
      ∑REE 107 162 169 155 175 166 147
      Eu/Eu* 0.99 0.96 0.90 0.96 0.91 0.93 0.93
      LREE 103 155 162 149 168 159 142
      HREE 4.48 6.84 7.00 6.33 7.05 6.37 5.43
      LREE/HREE 22.9 22.6 23.2 23.5 23.8 25.0 26.1
      (La/Yb)N 33.3 37.9 38.8 36.4 38.1 39.5 39.6
      (Gd/Yb)N 2.12 2.33 2.38 2.33 2.22 2.23 2.34
      (Dy/Yb)N 1.14 1.24 1.25 1.25 1.20 1.25 1.14
        注:主量元素单位:10-2;微量、稀土元素单位:10-6.
      下载: 导出CSV

      表  3  南口前花岗岩锆石Hf同位素分析结果

      Table  3.   LA-ICP-MS zircon U-Pb analyses of the granite rocks in Nankouqian

      测点 t(Ma) 176Yb/177Hf 176Lu/177Hf 176Hf/177Hf 2σ εHf(0) εHf(t) 2σ TDM1(Hf) TDM2(Hf) fLu/Hf
      XDP-2-1 224 0.019 675 0.000 891 0.282 279 0.000 018 -18.2 -13.2 0.6 1 402 1 738 -0.97
      XDP-2-2 224 0.018 344 0.000 825 0.282 301 0.000 010 -17.5 -12.5 0.4 1 369 1 698 -0.98
      XDP-2-3 224 0.015 698 0.000 703 0.282 317 0.000 012 -16.9 -11.9 0.4 1 343 1 669 -0.98
      XDP-2-4 224 0.037 096 0.001 511 0.282 431 0.000 009 -12.1 -7.4 0.3 1 177 1 724 -0.95
      XDP-2-5 224 0.018 782 0.000 799 0.282 427 0.000 008 -12.2 -7.4 0.3 1 160 1 726 -0.98
      XDP-2-6 224 0.029 544 0.001 203 0.282 423 0.000 008 -12.3 -7.6 0.3 1 178 1 738 -0.96
      XDP-2-7 224 0.032 310 0.001 317 0.282 443 0.000 008 -11.6 -6.9 0.3 1 153 1 693 -0.96
      XDP-2-8 224 0.019 214 0.000 788 0.282 398 0.000 008 -13.2 -8.4 0.3 1 200 1 791 -0.98
      XDP-2-9 224 0.026 329 0.001 129 0.282 384 0.000 009 -13.7 -9.0 0.3 1 231 1 825 -0.97
      XDP-2-10 224 0.033 696 0.001 513 0.282 411 0.000 007 -12.8 -8.1 0.3 1 205 1 768 -0.95
      XDP-2-11 224 0.040 009 0.001 573 0.282 416 0.000 008 -12.6 -7.9 0.3 1 200 1 758 -0.95
      XDP-2-12 224 0.030 837 0.001 217 0.282 397 0.000 006 -13.3 -8.5 0.2 1 216 1 797 -0.96
      XDP-2-13 224 0.026 481 0.001 119 0.282 408 0.000 007 -12.9 -8.1 0.2 1 196 1 770 -0.97
      XDP-2-14 224 0.017 691 0.000 748 0.282 399 0.000 007 -13.2 -8.4 0.2 1 197 1 788 -0.98
      下载: 导出CSV
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