浙西大铜坑斑岩型钨钼矿床成岩成矿年代学

胡开明; 唐增才; 孟祥随; 周汉文; 董学发; 杜雄; 陈忠大

doi:10.3799/dqkx.2016.502

浙西大铜坑斑岩型钨钼矿床成岩成矿年代学

doi: 10.3799/dqkx.2016.502

胡开明^1,,
唐增才^1,2, ,,
孟祥随^1,2,
周汉文²,
董学发^1,3,
杜雄⁴,
陈忠大¹

1.
浙江省地质调查院，浙江杭州 311203
2.
中国地质大学地球科学学院，湖北武汉 430074
3.
中国地质大学地球科学与资源学院，北京 100083
4.
浙江省第一地质大队，浙江杭州 311200

基金项目:

浙江省国土资源厅地勘资金项目 200702

浙江省国土资源厅地勘资金项目 201400

中国地质调查局地质调查项目 12120114068901

详细信息

作者简介:
胡开明(1963-)，男，高级工程师，长期从事地质矿产调查研究.E-mail: 784444517@qq.com

通讯作者:
唐增才, E-mail: zjgstzc@163.com

中图分类号: P588.12; P597
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- 被引次数: 0
出版历程
- 收稿日期: 2016-01-11
- 刊出日期: 2016-09-15

Chronology of Petrogenesis and Mineralization of Datongkeng Porphyry W-Mo Deposit in West Zhejiang

1.
Zhejiang Institute of Geological Survey, Hangzhou 311203, China
2.
School of Earth Sciences, China University of Geosciences, Wuhan 430074, China
3.
School of Earth Sciences and Resources, China University of Geosciences, Beijing 100083, China
4.
No.1 Geological Party of Zhejiang Province, Hangzhou 311200, China

摘要

摘要: 浙西淳安大铜坑斑岩型钨钼矿位于扬子陆块东南缘，矿体主要产于花岗岩体与南华系休宁组变质砂岩内外接触带上，是揭示浙皖赣相邻区域成矿规律的重要组成.成矿花岗岩为高钾钙碱性系列准过铝质Ⅰ型花岗岩，岩石富集Rb、K，亏损Sr、Ba等大离子亲石元素，富集Th、U，相对亏损Nb、Ta、Ti等高场强元素，稀土元素含量较低(ΣREE=106.2×10^-6~211.5×10^-6)，轻重稀土分异明显(ΣLREE/ΣHREE=6.4~12.2)，中等的Eu负异常(δEu=0.50~0.63)，具有类似岛弧岩浆岩的特征.锆石SHRIMP U-Pb定年结果表明花岗岩侵位时间为148.3±1.9 Ma，辉钼矿Re-Os等时线年龄显示成矿作用发生于146.47±0.81 Ma，成岩年龄与成矿时代高度耦合，进一步证实钨钼成矿作用与花岗岩体的形成有着密切的成因联系，二者在时间上是一个连续的过程，形成于晚侏罗世古太平洋板块俯冲挤压的构造环境，也是华南地区中生代第2次大规模钨钼成矿作用延续到浙西的响应.
- 锆石SHRIMP U-Pb年龄 /
- 辉钼矿Re-Os年龄 /
- 地球化学 /
- 年代学 /
- 大铜坑钨钼矿 /
- 花岗岩 /
- 浙西
Abstract: As an important component to reveal the metallogenic regularity in the Zhejiang-Anhui-Jiangxi border region, the Datongkeng porphyry W-Mo deposit in Chun'an County is located in the southeastern margin of the Yangtze block, and the W-Mo ore bodies are mainly located in the internal or external contact zones between granite and sandstone of Xiuning Formation. The Datongkeng granite is characterized by quasi-aluminous, showing the nature of Ⅰ-type granite and high-K calc-alkalic series rock. The granite is rich in Rb, K, Th, U, and relatively depleted in Sr, Ba, Nb, Ta, Ti. The total REE contents are relatively low (ΣREE=106.2×10^-6-211.5×10^-6), and the rocks show obvious LREE and HREE fractionation (ΣLREE/ΣHREE=6.4-12.2), moderately negative Eu anomalies (δEu=0.50-0.63), suggesting that these rocks have the characters of typical volcanic arc rocks. The SHRIMP U-Pb zircon age of 148.3±1.9 Ma for granite is close to the Re-Os isochron age of 146.47±0.81 Ma for five molybdenite samples from the Datongkeng W-Mo deposit, indicating magmatism and mineralization are a continuous process, which took place in the compression tectonic environment related to the subduction of pacific plate at Late Jurassic, and corresponds to the second large-scale W-Mo mineralization in South China.
- SHRIMP U-Pb dating of zircon /
- Re-Os age of molybdenite /
- geochemistry /
- chronology /
- Datongkeng W-Mo deposit /
- granite /
- West Zhejiang

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图 1 研究区地质略图

Fig. 1. Geological map of the study region

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图 2 大铜坑钨钼矿区地质图(a)和L12勘探线剖面(b)

Fig. 2. Geological map of the Datongkeng tungsten-molybdenum deposit (a) and a profile from No.12 exploration line (b)

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图 3 大铜坑花岗岩地质特征和镜下显微照片

a.基性岩墙群；b.含辉钼矿石英脉体；c.花岗岩岩心；d.斜长石斑晶，正交偏光；e.钾长石斑晶，正交偏光；f.石英斑晶，正交偏光.Bt.黑云母；Kfs.钾长石；Pl.斜长石；Qz.石英

Fig. 3. Geological feature and photomicrography of the Datongkeng granite

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图 4 大铜坑花岗岩A/NK-A/CNK(a)及K₂O-SiO₂(b)图解

图a据Maniar and Piccoli(1989)；图b据Rickwood(1989)

Fig. 4. A/NK vs. A/CNK diagram (a) and K₂O vs. SiO₂ diagram (b) for the Datongkeng granite

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图 5 大铜坑花岗岩稀土元素球粒陨石标准化曲线(a)和微量元素蛛网图(b)

标准值据Sun and McDonough(1989)

Fig. 5. Chondrite-normalized REE patterns (a) and trace element spider diagram (b) for the Datongkeng granite

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图 6 大铜坑花岗岩锆石的阴极发光图像及SHRIMP分析点位和²⁰⁶Pb-²³⁸U视年龄

Fig. 6. CL photomicrographs, meansured points and age data (²⁰⁶Pb/²³⁸U) of zircons from the Datongkeng granite

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图 7 大铜坑花岗岩锆石SHRIMP U-Pb年龄谐和图(a, b, c, d)和加权平均年龄(e, f)

Fig. 7. SHRIMP U-Pb concordia ages (a, b, c, d) and average model ages (e, f) of zircons from the Datongkeng granite

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图 8 大铜坑钨钼矿床辉钼矿Re-Os同位素等时线年龄(a)及模式年龄加权平均值(b)

Fig. 8. Re-Os weighted isochronage (a) and average model ages (b) of molybdenite from the Datongkeng W-Mo deposit

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图 9 大铜坑花岗岩Sr/Y-Y(a)和La_N/Yb_N-Yb_N(b)图解

据Defant and Drummond(1990)和Defant and Kepezhinskas(2001)

Fig. 9. Sr/Y vs. Y diagram (a) and La_N/Yb_N vs. Yb_N (b) diagram for the Datongkeng granite

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图 10 大铜坑花岗岩构造环境判别图解

图a, b, c, d据Pearce et al.(1984)；图e据Harris et al.(1986)；图f据Batchelor and Bowden(1985)

Fig. 10. Tectonic setting discriminative diagram for the Datongkeng granite

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表 1 大铜坑花岗岩主量元素(%)和微量元素(10^-6)组成

Table 1. Major elements (%) and trace elements (10^-6) of the Datongkeng granite

样品	DTK01	DTK02	DTK03	DTK04	DTK05	DTK06	DTK07	DTK08	DTK09	DTK10	DTK11
SiO₂	68.78	69.16	68.68	67.28	68.47	70.74	67.77	67.33	69.55	68.97	68.38
TiO₂	0.43	0.45	0.40	0.44	0.34	0.39	0.44	0.40	0.43	0.40	0.44
Al₂O₃	14.80	14.27	13.78	14.80	14.68	13.01	13.64	13.64	14.84	14.25	13.97
TFe₂O₃	3.08	3.22	2.56	2.91	3.58	4.04	5.40	4.62	3.01	4.81	6.43
MnO	0.04	0.04	0.04	0.03	0.03	0.03	0.04	0.07	0.09	0.06	0.08
MgO	0.94	0.97	0.86	0.94	0.98	0.78	0.89	0.76	0.82	0.79	0.87
CaO	2.73	2.40	2.45	2.41	2.27	1.3	2.39	3.12	2.33	2.16	2.40
Na₂O	3.33	3.06	2.93	3.31	2.78	2.27	2.63	3.00	3.33	2.95	3.00
K₂O	3.82	4.34	4.43	4.30	4.5	5.84	3.89	3.84	3.91	3.91	3.45
P₂O₅	0.15	0.16	0.14	0.15	0.18	0.17	0.18	0.12	0.13	0.12	0.13
LOI	1.58	1.70	3.28	2.80	1.72	0.98	2.32	2.7	1.1	1.23	0.38
Total	99.68	99.77	99.55	99.37	99.53	99.55	99.59	99.59	99.54	99.66	99.53
A/CNK	1.02	1.01	0.98	1.02	1.08	1.05	1.06	0.92	1.06	1.10	1.07
K₂O/Na₂O	1.15	1.42	1.51	1.30	1.62	2.57	1.48	1.28	1.17	1.33	1.15
σ	1.98	2.09	2.11	2.39	2.08	2.37	1.71	1.93	1.97	1.82	1.64
Mg^#	44	43	46	45	41	33	30	30	41	29	26
A.R	2.23	2.16	2.13	2.25	1.98	3.62	1.98	2.12	2.27	2.12	2.16
DI	79.70	81.18	82.18	81.15	79.60	84.96	76.68	76.72	80.72	78.62	75.26
Ba	386	373	517	383	324	357	347	322	314	410	242
Rb	195	243	252	257	256	241	225	224	234	203	143
Sr	309	242	177	252	198	201	182	190	197	182	182
Y	22.6	24.5	20.0	24.7	24.2	23.9	22.4	21.8	23.9	22.3	21.5
Zr	131	141	128	154	121	118	106	109	115	108	111
Nb	15.4	15.6	13.9	18.5	18.9	21.2	19.4	17.9	19.7	18.3	19
Th	21.5	18.5	19.8	22.4	19.6	18.7	16.4	18.6	19	20.1	17.2
Ga	21.8	20.1	17.6	22.7	18.6	19.4	17.4	17.6	18.7	17.8	18.9
Hf	3.95	4.30	3.90	4.67	3.55	3.69	3.26	3.38	3.64	3.47	3.41
Ta	1.48	1.58	1.40	1.76	2.08	2.21	1.91	1.95	2.19	2.07	1.94
U	9.51	12.2	11.5	9.86	12.8	11.9	9.31	12.3	13	9.9	9.2
La	37.3	26.5	21.9	38.6	38	39	25.6	21.6	19.9	27.8	21.3
Ce	72.4	54.6	43.6	76.5	93	86	51.5	44.2	43.2	56.3	44
Pr	7.91	6.35	5.03	8.71	8.60	10.10	6.00	5.04	4.87	6.38	5.01
Nd	29.1	24.6	20.0	32.2	35	43	22.7	19	18.8	23.6	19
Sm	5.70	5.13	4.08	6.45	6.4	8.6	4.84	4.15	4.36	4.82	4.15
Eu	1.01	0.94	0.80	1.03	1.04	1.35	0.86	0.71	0.78	0.81	0.76
Gd	4.80	4.64	3.72	5.29	5.50	7.80	4.44	3.9	4.2	4.3	3.91
Tb	0.70	0.71	0.57	0.78	0.66	1.15	0.71	0.64	0.7	0.69	0.64
Dy	4.01	4.06	3.34	4.30	3.60	6.20	3.91	3.59	3.96	3.72	3.57
Ho	0.71	0.74	0.61	0.76	0.66	1.14	0.73	0.68	0.75	0.69	0.67
Er	1.94	2.11	1.75	2.14	2.00	3.30	2.02	1.92	2.11	1.97	1.9
Tm	0.30	0.31	0.27	0.31	0.27	0.45	-	-	-	-	-
Yb	1.99	2.24	1.85	2.17	1.9	3.00	2.02	2.04	2.25	2.04	1.98
Lu	0.31	0.34	0.28	0.32	0.28	0.42	0.31	0.31	0.33	0.3	0.3
ΣREE	168.18	133.27	107.80	179.56	196.91	211.51	125.64	107.78	106.21	133.42	107.19
LREE/HREE	10.4	7.8	7.7	10.2	12.2	8.0	7.9	7.2	6.4	8.7	7.3
Rb/Sr	0.63	1.00	1.42	1.02	1.29	1.20	1.24	1.18	1.19	1.12	0.79
Sr/Y	13.67	9.88	8.85	9.20	8.18	8.41	8.13	8.72	8.24	8.16	8.47
La_N/Yb_N	13.4	8.5	8.5	12.8	14.3	9.3	9.1	7.6	6.4	9.8	7.7
La_N/Sm_N	4.2	3.3	3.5	3.9	3.8	2.9	3.4	3.4	3.0	3.7	3.3
Gd_N/Yb_N	2.0	1.7	1.7	2.0	2.4	2.2	1.8	1.6	1.5	1.7	1.6
δEu	0.59	0.59	0.63	0.54	0.54	0.50	0.57	0.54	0.56	0.55	0.58
T_Zr(℃)	809	816	804	822	805	803	792	784	801	796	797
注：A/CNK=Al₂O₃/(CaO+Na₂O+K₂O)mol；Mg^#=(MgO/40.31)/(MgO/40.31+0.7×TFe₂O₃/71.85)；DTK01~DTK06数据为本次实测，DTK07~DTK11数据引自Li et al.(2013).

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表 2 大铜坑花岗岩体中锆石的SHRIMP U-Pb年龄测定结果

Table 2. SHRIMP U-Pb dating result of zircons from the Datongkeng granite

点号	²⁰⁶Pb_c(%)	U(10^-6)	Th(10^-6)	²³²Th/²³⁸U	²⁰⁶Pb*(10^-6)	年龄(Ma)	²⁰⁶Pb/²³⁸U	±1σ(%)	²⁰⁷Pb/²⁰⁶Pb	±1σ(%)	²⁰⁷Pb*/²³⁵U	±1σ(%)	²⁰⁶Pb*/²³⁸U
CA1-1.1	1.96	225	222	1.02	4.6	148.5	3.9	0.046 3	7.9	0.153 0	8.4	0.023 3	2.7
CA1-2.1	0.73	693	814	1.21	13.4	142.6	3.4	0.056 3	3.0	0.146 8	3.9	0.022 4	2.4
CA1-3.1	0.31	1 750	300	0.18	32.6	138.1	3.2	0.046 5	2.3	0.143 1	3.3	0.021 6	2.3
CA1-4.1	0.47	1 712	288	0.17	31.8	137.0	3.2	0.048 6	2.2	0.139 3	3.2	0.021 5	2.3
CA1-5.1	0.12	2 178	361	0.17	39.0	132.7	4.0	0.047 4	1.9	0.137 5	3.6	0.020 8	3.1
CA1-6.1	0.44	1 119	146	0.13	20.6	136.2	3.2	0.048 0	3.0	0.141 4	3.8	0.021 4	2.4
CA1-7.1	0.20	1 815	361	0.21	32.9	134.4	3.1	0.046 9	2.0	0.140 4	3.1	0.021 1	2.3
CA1-8.1	0.26	2 145	424	0.20	38.3	132.2	3.0	0.047 7	1.9	0.136 5	3.0	0.020 7	2.3
CA1-9.1	0.07	1 724	362	0.22	31.5	135.5	3.5	0.047 8	2.0	0.140 8	3.3	0.021 2	2.6
CA1-10.1	0.46	158	150	0.98	17.0	756.3	17.7	0.064 8	2.6	1.126 0	3.6	0.124 5	2.5
CA1-11.1	0.43	1 938	377	0.20	34.0	129.9	3.0	0.049 8	2.3	0.137 9	3.2	0.020 4	2.3
CA1-12.1	0.22	447	184	0.43	50.0	788.1	17.5	0.069 2	1.4	1.185 0	2.8	0.130 0	2.4
CA1-13.1	0.53	1 057	345	0.34	19.9	139.1	3.2	0.049 9	2.6	0.145 8	3.5	0.021 8	2.4
CA1-14.1	0.34	2 440	536	0.23	42.9	130.1	3.0	0.049 2	1.8	0.139 1	2.9	0.020 4	2.3
CA1-15.1	0.32	1 184	253	0.22	27.7	172.8	4.1	0.037 3	3.7	0.209 8	4.4	0.027 2	2.4
CA1-16.1	0.18	894	1 161	1.34	18.0	148.9	3.1	0.048 7	1.9	0.152 4	2.9	0.023 4	2.1
CA1-17.1	/	146	30	0.21	2.88	146.7	3.6	0.047 8	5.0	0.156 3	5.9	0.023 0	2.5
CA1-18.1	0.02	1 046	336	0.33	21.5	152.7	3.1	0.050 1	1.6	0.165 0	2.9	0.024 0	2.1
CA1-19.1	10.09	2 154	3 173	1.52	46.4	144.1	3.1	0.131 5	6.6	0.160 0	23	0.022 6	2.2
CA1-20.1	/	488	465	0.99	59.1	851.1	16	0.066 5	0.90	1.293 0	2.2	0.141 1	2.0
CA1-21.1	0.69	95	74	0.81	10.5	782.0	17	0.066 2	2.1	1.075 0	4.6	0.129 0	2.3
CA1-22.1	0.02	1 078	871	0.84	126	822.2	15	0.065 5	0.66	1.226 0	2.2	0.136 1	2.0
CA1-23.1	4.82	568	405	0.74	11.8	147.0	3.2	0.090 9	1.7	0.168 0	12	0.023 1	2.2
CA1-24.1	0.00	139	203	1.51	2.81	150.3	3.6	0.050 2	4.6	0.163 2	5.2	0.023 6	2.4
CA1-25.1	0.18	799	1 062	1.37	15.6	144.2	3.0	0.051 8	2.0	0.157 1	3.5	0.022 6	2.1
CA1-26.1	/	481	54	0.12	9.71	149.6	3.2	0.047 2	2.5	0.154 7	3.3	0.023 5	2.1
CA1-27.1	0.01	539	779	1.49	10.8	148.7	3.1	0.049 2	2.3	0.158 0	3.1	0.023 3	2.1
CA1-28.1	/	322	524	1.68	6.58	151.7	3.3	0.048 2	3.2	0.164 9	5.6	0.023 8	2.2
注：误差为1σ；Pb_c和Pb*分别代表普通铅和放射性成因铅；标准校正值的误差为0.40%(不包括在上述误差内，但包括不同样品靶的数据比较).应用实测²⁰⁴Pb校正普通铅.

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表 3 大铜坑钨钼矿区辉钼矿Re-Os同位素组成

Table 3. Re-Os isotopic analyses of molybdenite from ores of the Datongkeng W-Mo deposit

编号	样号	样重(g)	Re(10^-6)	Os_普(10^-9)	¹⁸⁷Re(10^-6)	¹⁸⁷Os(10^-9)	模式年龄(Ma)
150417-4	DTK01	0.002 10	116.70±0.80	0.473 2±0.057 1	73.37±0.49	178.80±1.00	146.1±1.9
150417-5	DTK02	0.002 20	28.63±0.18	0.391 9±0.108 7	17.99±0.11	44.01±0.36	146.6±2.1
150417-6	DTK03	0.002 18	9.70±0.08	0.376 2±0.100 0	6.10±0.05	14.83±0.11	145.8±2.2
150417-7	DTK04	0.002 41	94.34±0.64	0.390 5±0.079 7	59.30±0.40	145.21±0.90	146.8±2.0
150417-8	DTK05	0.002 35	94.22±0.66	1.066 3±0.080 2	59.22±0.41	144.40±0.91	146.2±2.0

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表 4 浙皖赣相邻区钨钼矿区成岩年龄及成矿时代

Table 4. The formation age of plutons from the important deposits in West Zhejiang and adjacent regions

矿区名称	岩体岩性	成岩年龄和成矿时代	测试方法	资料来源
乐平塔前钨钼矿	花岗闪长岩	159.7±1.8 Ma	LA-ICP-MS锆石U-Pb	刘善宝等，2014
乐平塔前钨钼矿	花岗闪长岩	162±2 Ma	辉钼矿Re-Os	黄安杰等，2013
铅山永平铜钨钼矿	花岗岩	160.0±2.3 Ma	SIMS锆石U-Pb	丁昕等，2005
铅山永平铜钨钼矿	花岗岩	156.7±2.8 Ma	辉钼矿Re-Os	李晓峰等，2007
桐庐彰坞钨矿	花岗岩	159.7±2.6 Ma	LA-ICP-MS锆石U-Pb	笔者，未发表
绩溪背靠山钨矿	花岗闪长斑岩	152.7~147.7 Ma	SHRIMP锆石U-Pb	周翔等，2012
淳安县开岭脚钼矿	花岗闪长岩	151±3 Ma	SHRIMP锆石U-Pb	汪建国等，2010
余杭闲林铁钼(铜钨)矿	花岗闪长岩	151.8±2.2 Ma	SHRIMP锆石U-Pb	唐增才等，2014
余杭闲林铁钼(铜钨)矿	花岗闪长岩	149.7 Ma	辉钼矿Re-Os	王永彬等，2013
武宁石门寺钨矿	花岗岩	144.2±1.3 Ma	LA-ICP-MS锆石U-Pb	黄兰椿和蒋少涌，2012
武宁石门寺钨矿	花岗岩	149.6±1.2 Ma	辉钼矿Re-Os	项新葵等，2013
绍兴漓渚铁钼(钨)矿	花岗闪长岩	150.1±2.6 Ma	LA-ICP-MS锆石U-Pb	顾明光等，2011
绍兴漓渚铁钼(钨)矿	花岗闪长岩	149.3 Ma	辉钼矿Re-Os	王永彬等，2013
淳安大铜坑钨钼矿	花岗岩	148.3±1.9 Ma	SHRIMP锆石U-Pb	本文
淳安大铜坑钨钼矿	花岗岩	146.47±0.81 Ma	辉钼矿Re-Os	本文
祁门东源钨钼矿	花岗闪长斑岩	146±1 Ma	SHRIMP锆石U-Pb	周翔等，2011
淳安大铜坑钨钼矿	花岗岩	146.4±2.3 Ma	辉钼矿Re-Os	周翔等，2011
淳安木瓜钨矿	花岗斑岩	142.2±1.2 Ma	LA-ICP-MS锆石U-Pb	厉子龙等，2013
歙县邓家坞钼矿	花岗闪长斑岩	141.8±2.2 Ma	辉钼矿Re-Os	李双等，2012
安吉港口铅锌钨钼矿	花岗闪长岩	141.0±1.4 Ma	LA-ICP-MS锆石U-Pb	唐燕文等，2013
安吉港口铅锌钨钼矿	花岗闪长岩	141.2±1.1 Ma	辉钼矿Re-Os	唐燕文等，2013
龙泉毛断钼多金属矿	花岗岩	140.0±1.6 Ma	LA-ICP-MS锆石U-Pb	李艳军等，2011
龙泉毛断钼多金属矿	花岗岩	139.0±0.8 Ma	辉钼矿Re-Os	李艳军等，2011

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