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    手持X射线衍射仪(ED-XRF)在旋回地层学中的应用:以酒泉盆地青西凹陷早白垩世下沟组为例

    曹海洋 王华 赵睿

    曹海洋, 王华, 赵睿, 2017. 手持X射线衍射仪(ED-XRF)在旋回地层学中的应用:以酒泉盆地青西凹陷早白垩世下沟组为例. 地球科学, 42(12): 2299-2311. doi: 10.3799/dqkx.2017.571
    引用本文: 曹海洋, 王华, 赵睿, 2017. 手持X射线衍射仪(ED-XRF)在旋回地层学中的应用:以酒泉盆地青西凹陷早白垩世下沟组为例. 地球科学, 42(12): 2299-2311. doi: 10.3799/dqkx.2017.571
    Cao Haiyang, Wang Hua, Zhao Rui, 2017. The Application of the Handheld Energy-Dispersive X-Ray Fluorescence (ED-XRF) in the Cyclostratigraphy Research-A Case Study from the Xiagou Formation of the Lower Cretaceous in the Qingxi Sag, Jiuquan Basin. Earth Science, 42(12): 2299-2311. doi: 10.3799/dqkx.2017.571
    Citation: Cao Haiyang, Wang Hua, Zhao Rui, 2017. The Application of the Handheld Energy-Dispersive X-Ray Fluorescence (ED-XRF) in the Cyclostratigraphy Research-A Case Study from the Xiagou Formation of the Lower Cretaceous in the Qingxi Sag, Jiuquan Basin. Earth Science, 42(12): 2299-2311. doi: 10.3799/dqkx.2017.571

    手持X射线衍射仪(ED-XRF)在旋回地层学中的应用:以酒泉盆地青西凹陷早白垩世下沟组为例

    doi: 10.3799/dqkx.2017.571
    基金项目: 

    国家科技重大专项课题 2016ZX05006006-002

    详细信息
      作者简介:

      曹海洋(1988-), 男, 博士, 主要从事层序地层学、沉积学、旋回地层学研究

    • 中图分类号: P595

    The Application of the Handheld Energy-Dispersive X-Ray Fluorescence (ED-XRF) in the Cyclostratigraphy Research-A Case Study from the Xiagou Formation of the Lower Cretaceous in the Qingxi Sag, Jiuquan Basin

    • 摘要: 在旋回地层学研究中,高分辨率地球化学数据作为一重要的替代指标,其一般获取方式(ICP-MS或WD-XRF)较耗费时间和经费,而手持X射线衍射仪(ED-XRF)能够高效的解决这一问题,目前将ED-XRF运用在沉积地层研究中,尤其是旋回地层学研究领域中较少.以酒泉盆地青西凹陷早白垩世下沟组深湖相泥岩、白云质泥岩为研究对象,将连续采集的岩心样品通过ED-XRF测试,该测试方法能够保证在不破坏样品的前提下,并在误差允许的范围内的条件下,短时间内(5 min)完成对单一样品的测试.通过测试精确得出24种主量及微量元素的含量,将得出的地球化学特征作为旋回地层学研究的替代指标,并针对K/Al,Ca/Al,Si/Al,Fe/Al,Ti/Al,Mn/Al,Ni/Al,Zn/Al和Pb/Al的比值进行频谱分析.数据表明W2井下沟组一段(SQK1g1)地层旋回性表现出与天文旋回明显的对应关系.沉积地层中的旋回厚度比值为20.25:4.75:1.75:1.00,与米兰科维奇旋回中长偏心率、短偏心率、斜率和岁差的周期比值:400 ka:95 ka:37 ka:20 ka相对应.该地区的沉积记录受天文轨道周期的影响得到了证明,与此同时,为手持X射线衍射仪在旋回地层学中的应用开辟了新领域.

       

    • 图  1  研究区地质

      a.主要白垩系盆地分布范围及酒泉盆地位置(旷红伟等,2013);b.酒泉盆地构造区划,主要分为3个构造单元:酒西坳陷、嘉峪关隆起和酒东坳陷;c.青西凹陷及钻井位置示意图

      Fig.  1.  Geology of research area

      图  2  青西凹陷下白垩统综合柱状图

      包括:岩性描述、古生物(马其鸿等,1984牛绍武,1987)、沉积环境、构造演化阶段(Chen et al., 2014)

      Fig.  2.  The stratigraphy column of Lower Cretaceous inthe Qingxi Sag

      图  3  酒泉盆地青西凹陷W2井下沟组典型岩心柱

      W2井采样位置为4 426~4 466 m,厚度40 m,均匀采样41个,样品间隔1 m

      Fig.  3.  Typical lithologic cores and sampling section inMember1 of the Xiagou Formation (SQK1g1) of well W2

      图  4  色散X射线分析

      a.W2井12号样品下沟组低能量色散X射线分析(15 kV,0.055 0 mA);b.W4井15号样品下沟组高能量色散X射线分析(40 kV,0.006 5 mA),Al-Ti滤波(Ti:25 μm;Al:300 μm)

      Fig.  4.  Dispersive X-ray spectrum

      图  5  手持X射线衍射仪测量各种元素的标准值与测量值

      基于Bruker AXS的校准软件(SPECTRAEDX S2 CONFIGURATION),校准值见表 3

      Fig.  5.  Accepted (acc) versus measured (meas) values for elements analyzed by ED-XRF

      图  6  W2井下沟组一段地化数据快速傅里叶变换

      Fig.  6.  Fast Fourier Transformation (FFT) spectrum for the geochemical data in Member 1 of the Xiagou Formation in Well W2, the Qingxi Sag, Jiuquan Basin

      表  1  青西凹陷采样分布

      Table  1.   Sections of sample analyzed in the Qingxi Sag

      井名样品数样品分类
      W148白云质泥岩;泥岩;灰质粉砂岩
      W241白云质泥岩;灰质粉砂岩
      W329白云质泥岩;
      W432白云质泥岩;泥质白云岩;细砂岩
      W521白云质泥岩;泥质白云岩;灰质粉砂岩
      总计171泥岩;白云质泥岩;泥质白云岩;灰质粉砂岩;细砂岩
      下载: 导出CSV

      表  2  标样主量及微量元素浓度的计算标准(加拿大Bureau Veritas矿物检测公司)

      Table  2.   Major and trace elemental concentrations for the calibration standards

      W1-3W3-14W3-9W2-13W4-15W4-13W5-16W5-19W1-23W2-19
      K2O(%)3.072.712.883.362.442.443.342.952.962.61
      CaO(%)3.496.849.0110.841.8915.064.816.578.2711.96
      Al2O3(%)17.1714.9912.5411.4816.068.6117.7414.8813.2912.01
      SiO2(%)51.6242.8737.9337.0452.0526.0645.8343.2238.0134.10
      P2O5(%)0.060.020.050.030.040.010.040.050.000.08
      TiO2(%)0.730.530.510.480.660.320.610.510.490.40
      V(10-6)148.00113.00105.0093.0096.0073.00126.0087.00114.00106.00
      Cr2O3(%)0.0200.0170.0170.0150.0160.0080.0190.0160.0150.014
      MnO(%)0.130.130.120.120.120.110.100.100.110.18
      Fe2O3(%)6.164.874.603.184.282.165.637.135.155.76
      Co(10-6)19.5021.3020.2015.5040.509.6024.9019.8015.7014.00
      Ni(10-6)66.0054.0078.0047.00133.0020.0068.0064.0042.0047.00
      Cu(10-6)41.6039.3049.1033.0047.7025.2051.5055.3039.5036.10
      Zn(10-6)59.0043.0066.0060.0091.0030.0062.0070.0092.0048.00
      Rb(10-6)144.60115.10128.00120.1091.2084.90137.6095.60120.5093.30
      Sr(10-6)127.30335.00535.80603.00206.70988.10256.10524.20630.10590.20
      Y(10-6)26.2015.8019.6017.9020.8014.7013.4022.9012.7020.40
      Zr(10-6)154.00114.80101.1096.60144.3068.00120.70108.3089.9085.90
      Nb(10-6)13.409.209.808.7012.206.0011.209.808.207.40
      Mo(10-6)0.202.903.302.100.902.700.701.302.700.90
      Pb(10-6)18.4011.6036.606.1043.507.5019.4049.6024.0020.90
      W(10-6)2.801.502.001.802.601.302.301.601.900.90
      Ba(10-6)573.00504.00732.00705.00234.00386.00474.00289.00319.00280.00
      Ce(10-6)72.2043.8053.6048.8060.4042.6025.0052.8023.4040.80
      Sum(%)82.6073.1267.8566.7377.6854.9578.2675.5768.4567.25
      下载: 导出CSV

      表  3  Corrections used for ED-XRF calibration ED-XRF标准值校正

      Table  3.   Corrections used for ED-XRF calibration

      元素峰能偏移量和二次修正α校正(强度修正)标准值省略校正标准偏差
      AlKa1On;OffP,Mn,RbW4-15;W1-230.076 1%
      SiKa1Off;OnP,Rb,PbW3-14;0.256 0%
      PKa1Off;OnSr,Ba00.005 0%
      KKa1On;OffCa,Ti,00.027 2%
      CaKa1On;OnAl,Si,K00.117 0%
      TiKa1On;OnP,MnW3-90.003 4%
      MnKa1Off;OffAl,Ca,RhW1-328×10-6
      FeKa1On;OnP,Ca00.035 4%
      CrKa1Off;OffSi,P,Ca03×10-6
      VKa1On;OnAl,PW1-3;W2-1910-6
      CoKa1On;OffTi,Mo010-6
      NiKa1Off;OnV,Fe,W010-6
      CuKa1Off;OffSi,Ca,Ba010-6
      ZnKa1On;OffPW2-13;W4-1310-6
      RbKa1On;OffP,V,Nb010-6
      SrKa1On;OnAl,Si,016×10-6
      YKa1On;OnAl,Ba00
      ZrKa1On;OffSi,P,MnW3-14;W5-2010-6
      NbKa1On;OffP,Rb00
      MoKa1Off;OffAl,P,CaW5-12;0
      BaKa1On;OnAl,Cr,PbW1-5;W2-1736×10-6
      CeKa1Off;OffP,Ce,010-6
      WKa1On;OnP,V,FeW3-6;W1-120
      PbKa1On;OffP,Cr,Zn00
      下载: 导出CSV

      表  4  元素比值与天文周期的比例关系

      Table  4.   The proportion of element ratios and astronomical cycle

      K/AlCa/AlSi/AlFe/AlTi/AlMn/AlNi/AlZn/AlPb/Al
      19.21 m19.30 m19.30 m81.30 m19.21 m81.23 m81.30 m81.30 m81.30 m
      10.22 m6.47 m7.35 m9.17 m12.01 m10.87 m19.21 m19.29 m19.30 m
      7.14 m4.30 m6.29 m7.36 m7.35 m7.35 m8.33 m8.33 m7.35 m
      6.35 m4.43 m4.72 m5.70 m5.13 m4.21 m7.35 m
      4.28 m3.67 m3.87 m4.05 m
      下载: 导出CSV
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