Petrogenesis of Early Cretaceous Chibaisong Granitoid Dyke (Stock) from Tonghua Area, Jilin Province: Evidences from Zircon U-Pb Geochronology, Hf Isotope and Whole-Rock Geochemistry
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摘要: 中国吉林省通化县赤柏松地区早白垩世花岗质岩脉（株）的锆石U-Pb年代学、Hf同位素和全岩地球化学特征，为探讨华北克拉通东北部中生代时期大陆下地壳的属性和构造演化历史提供了重要依据.研究区花岗质岩脉（株）中的锆石普遍发育振荡生长环带，并具有较高的Th/U比值（0.53~1.94），表明其为岩浆成因.对采自花岗质岩脉（株）中4个样品的锆石U-Pb测年结果表明，它们的206Pb/238U加权平均年龄分别为116 Ma、124 Ma、127 Ma和130 Ma，即早白垩世早期和早白垩世晚期.这些花岗质岩石具有变化的SiO2（60.61%~76.07%）和MgO（0.01%~2.48%）含量、富碱（K2O+Na2O=6.26%~9.14%）及富Al2O3（11.99%~16.13%）的特征，总体属于高钾钙碱性系列岩石.微量元素上富集轻稀土和大离子亲石元素，亏损重稀土和Ba、Sr、P、Ti和Eu等元素（Eu/Eu*=0.05~0.30），暗示其主要来自地壳岩石的部分熔融，并在演化过程中经历了斜长石、碱性长石、磷灰石和钛铁矿等矿物的分离结晶作用和围岩的同化混染作用.与早白垩世早期花岗质岩石相比，早白垩世晚期岩石的碱性程度提高.样品中锆石εHf（t）值介于-21.84~-10.74之间，两阶段亏损地幔模式年龄为1.86~2.56 Ga.上述地球化学特征暗示，赤柏松地区下地壳以古元古代地壳物质为主，存在少量新太古代地壳物质.早白垩世时期研究区以双峰式岩石组合为特征，进一步结合区域上已有的火成岩和区域构造演化的研究成果，认为早白垩世时期研究区处于俯冲背景下的伸展环境.与早白垩世早期相比，早白垩世晚期伸展作用增强.Abstract: LA-ICP-MS zircon U-Pb geochronology, whole-rock geochemistry and Hf isotope of zircons of Early Cretaceous Chibaisong granitoids in Tonghua area, southern Jilin Province, northeast (NE) China provide the insights into the nature of the lower crust and tectonic evolution of the eastern North China Craton (NCC). Zircons from the Chibaisong granitoid dyke (stock) show fine-scale oscillatory zoning, and relatively high Th/U ratios (0.53~1.94), indicative a magmatic origin. The weighted mean of 206Pb/238U ages for four samples from four granitoids are 116 Ma, 124 Ma, 127 Ma and 130 Ma, respectively. The Chibaisong granitoids have variable content of SiO2 (60.61%-76.07%) and MgO (0.01%-2.48%), high content of total-alkali (K2O+Na2O=6.26%-9.14%) and Al2O3 (11.99%-16.13%), characterized by the nature of high-K calc-alkaline series.Additionally, they show enrichment of LREEs and LILEs, depletion of HREEs and HFSEs, Ba, Sr, P, Ti and Eu (Eu/Eu*=0.05-0.30), suggesting that they were derived from the partial melting of the lower crust, and suffered from the fractional crystallization of plagioclase, alkali feldspar, apatite and ilmenite. Furthermore, they were assimilated by the country rock according to their variable major element contents and zircon εHf(t)values. Granitoids were more alkaline in the early stage of the Early Cretaceous and Mg# was increased, which may be attributed to mantle material. The zircon εHf(t) values in the samples ranged from -21.84 to -10.74, and the two-stage model ages of zircon Hf isotope of granite porphyry yield 1.86-2.56 Ga, which imply that the accretion of the lower crust within the Tonghua area mainly happened in the Paleoproterozoic, with small amounts during Neoproterozoic. The bimodal rock associationin the Early Cretaceous, together with the results from the contemporaneous volcanic rocks and regional evolution history in this area, indicate that the granitoid dykes may formed in an extensional setting, and more strongly extension happened during the late stage of Early Cretaceous associated with the subduction of the Paleo-Pacific Plate beneath the Eurasian continent.
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Key words:
- Early Cretaceous /
- Chibaisong /
- granitoid dyke (stock) /
- geochemistry /
- zircon Hf isotope
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图 1 华北克拉通构造简图（a）和通化赤柏松地区地质简图（b）
Fig. 1. Simplified geological maps showing (a) major tectonic units of North China Craton and (b) of the Chibaisong area in Tonghua
图 2 通化赤柏松地区早白垩世花岗质岩石镜下照片
Qz.石英; Or.正长石; Pl.斜长石; a.花岗斑岩；b.花岗斑岩；c.石英的熔蚀结构、斜长石的碳酸盐化；d.环斑球粒结构
Fig. 2. Photomicrographs showing the petrographic features of Early Cretaceous granitoids of the Chibaisong area in Tonghua
图 3 通化赤柏松地区早白垩世花岗质岩石中部分锆石的阴极发光图像
红色实线圆圈为U-Pb年龄测试点; 黄色虚线圆圈为Hf同位素测试点; 括号内为Hf同位素测试值; 左侧短线为比例尺100 μm
Fig. 3. Cathodoluminescence (CL) images of selected zircon grains of Early Cretaceous granitoids of the Chibaisong area in Tonghua
图 4 通化赤柏松地区早白垩世花岗质岩石锆石LA-ICP-MS U-Pb年龄谐和图
Fig. 4. LA-ICP-MS zircon U-Pb concordia diagrams for Early Cretaceous granitoids in the Chibaisong area, Tonghua.
图 5 （a）通化赤柏松地区早白垩世花岗质岩石SiO2 vs. (Na2O+K2O)图解; （b）SiO2vs.K2O图解
据Peccerillo and Taylor(1976)，Middlemost(1994)；数据裴福萍等（2009）, Pei et al.(2011a), 杨凤超等，（2017）, 秦亚等（2013）
Fig. 5. Plots of SiO2 vs. (Na2O+K2O) (a), SiO2 vs K2O (b) for the Early Cretaceous granitoids in the Chibaisong area, Tonghua
图 6 通化赤柏松地区早白垩世花岗质岩石球粒陨石标准化稀土元素配分型式（a）和原始地幔标准化微量元素蛛网图（b）
球粒陨石标准数据Preston et al.(1985); 原始地幔标准化数据Sun and McDonough (1984）; 图例同图 5
Fig. 6. (a) Chondrite-normalized REE patterns and (b) primitive mantle (PM)-normalized trace element spider diagrams for the Early Cretaceous granitoids in the Chibaisong area, Tonghua
图 7 通化赤柏松地区早白垩世花岗质岩石的Hf同位素组成
据Yang et al.（2006）；CAOB.中亚造山带；YFTB.燕山褶皱带；数据杨凤超等（2017），Zhang et al.（2018)
Fig. 7. Correlations between Hf isotopic compositions and ages of zircons for the Early Cretaceous granitoids in the Chibaisong area, Tonghua
图 8 通化赤柏松地区早白垩世花岗质岩石Ba-Sr和Rb/Sr-Sr图解（图例同图 5）
Fig. 8. Ba-Sr and Rb/Sr-Sr diagram for the Early Cretaceous granitoids in the Chibaisong area, Tonghua
图 9 通化赤柏松地区早白垩世花岗质岩石的成因类型判别图解（a）Zr+Nb+Ce+Y-（Na2O+K2O）/CaO；（b）Zr+Nb+Ce+Y-FeO*/MgO（据Whalen et al., 1987）
Fig. 9. (a) (Na2O+K2O)/CaO vs. (Zr+Nb+Ce+Y) and (b) FeO*/MgO vs. (Zr+Nb+Ce+Y) discrimination diagrams
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