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    盆地流体年代学研究新技术:方解石激光原位U-Pb定年法

    刘恩涛 ZhaoJian-xin 潘松圻 严德天 陆江 郝少斌 龚银 邹康

    刘恩涛, ZhaoJian-xin, 潘松圻, 严德天, 陆江, 郝少斌, 龚银, 邹康, 2019. 盆地流体年代学研究新技术:方解石激光原位U-Pb定年法. 地球科学, 44(3): 698-712. doi: 10.3799/dqkx.2019.958
    引用本文: 刘恩涛, ZhaoJian-xin, 潘松圻, 严德天, 陆江, 郝少斌, 龚银, 邹康, 2019. 盆地流体年代学研究新技术:方解石激光原位U-Pb定年法. 地球科学, 44(3): 698-712. doi: 10.3799/dqkx.2019.958
    Liu Entao, Zhao Jian-xin, Pan Songqi, Yan Detian, Lu Jiang, Hao Shaobin, Gong Yin, Zou Kang, 2019. A New Technology of Basin Fluid Geochronology: In-Situ U-Pb Dating of Calcite. Earth Science, 44(3): 698-712. doi: 10.3799/dqkx.2019.958
    Citation: Liu Entao, Zhao Jian-xin, Pan Songqi, Yan Detian, Lu Jiang, Hao Shaobin, Gong Yin, Zou Kang, 2019. A New Technology of Basin Fluid Geochronology: In-Situ U-Pb Dating of Calcite. Earth Science, 44(3): 698-712. doi: 10.3799/dqkx.2019.958

    盆地流体年代学研究新技术:方解石激光原位U-Pb定年法

    doi: 10.3799/dqkx.2019.958
    基金项目: 

    青岛海洋科学与技术国家实验室海洋矿产资源评价与探测技术功能实验室开放基金 KC201701

    国家自然科学基金项目 41702121

    中国石油科技创新基金研究项目 2018D-5007-0104

    详细信息
      作者简介:

      刘恩涛(1986-), 男, 副教授, 主要从事沉积学、盆地分析研究

    • 中图分类号: P597

    A New Technology of Basin Fluid Geochronology: In-Situ U-Pb Dating of Calcite

    • 摘要: 流体活动是沉积盆地内最活跃的地质营力,与盆地内油气的生成、运移和成藏关系密切,精确确定流体活动历史一直是具有挑战性和前沿性的研究方向.前期对流体活动历史的研究主要依附于流体包裹体分析,该方法很难完整恢复盆地经历的所有流体事件,更无法确定流体事件活动年代.方解石是盆地流体的直接产物,对其开展年代学研究可以准确揭示盆地流体活动历史,然而目前较为成熟的同位素稀释法方解石U-Pb等时线定年成功率较低、耗时较长.近些年研发成功的方解石激光原位U-Pb定年技术可以精确确定U含量低至10×10-9的方解石的年代,具有空间分辨率高、测试效率高的优势.该技术已成功确定多个含油气盆地流体活动历史,显示其在盆地流体研究领域具有光明的应用前景.在详细的微观鉴定和成岩观察基础上,选取不同期次的方解石样品开展方解石激光原位U-Pb定年分析,并结合C-O同位素、微量元素研究,查明盆地流体特征及其演化历史,将是未来盆地流体研究领域的重要发展方向.

       

    • 图  1  同位素稀释法方解石U-Pb测年典型实例

      Rasbury et al. (2004)

      Fig.  1.  The typical example of calcite ages using isotope dilution U-Pb isochrones approach

      图  2  同位素稀释法方解石U-Pb定年(a)与激光原位法(b)测试结果对比

      据Robert et al.(2017)

      Fig.  2.  The comparison between ID-IRMS U-Pb data (a) and in-situ LA-ICPMS data (b)

      图  3  运用激光原位方解石U-Pb定年成功确定盆地断层活动带流体活动历史典型实例

      数据来自Nuriel et al.(2017)

      Fig.  3.  The typical example showing the application of in-situ U-Pb dating method to reconstruct the history of fluid flow events in the sedimentary basin

      表  1  盆地流体年代学主要研究方法介绍

      Table  1.   The main methods of basin fluid flow history

      研究方法 主要特点 测试仪器 代表性文献
      流体包裹体法 在盆地流体研究领域中应用最为广泛, 主要用于流体期次研究, 但该方法容易受到继承性包裹体的影响, 很难准确确定流体活动时间 偏光显微镜 Worden et al. (1999)
      自生伊利石定年法 主要有K-Ar、Ar-Ar及Rb-Sr等时线3种定年手段, 分选出纯净的伊利石是该方法的难点, 仅适用于碎屑岩盆地 GV Instrument 5400、Helix-MC稀有气体质谱仪及TIMS/MC-ICPMS Uysal et al. (2001)
      自生钾长石加大边定年法 通常采用激光显微探针Ar-Ar定年手段, 样品需求量小, 测试精度高, 但满足测试需求的样品较少 GV Instrument 5400和Helix-MC稀有气体质谱仪 Mark et al. (2005)
      同位素稀释法方解石U-Pb测年法 在方解石年代学研究领域应用较为广泛, 但测试周期长、成功率并不高 MC-ICPMS、TIMS Smith et al. (1991)
      方解石激光原位ICP-MS U-Pb定年法 发展迅速, 测试精度高, 具有空间分辨率高、测试效率高的优势, 尚有一些技术问题需要解决 LA-HR- ICPMS、LA-MC-ICPMS Roberts and Walker (2016); Nuriel et al. (2017)
      方解石U-Th定年法 测试精度高, 但仅能测量50万年以内的样品年龄 MC-ICPMS、TIMS Zhao et al. (2009)
      方解石ESR年代学 测年的年限较长, 可从几千年到几百万年, 但主要用于断层带研究, 获得可靠的古剂量值是得到准确年龄的前提 电子顺磁(自旋)共振波谱仪 王鹏昊等(2013)
      下载: 导出CSV

      表  2  同位素稀释法方解石U-Pb测年代表性数据汇总

      Table  2.   Representative data of calcite using isotope dilution U-Pb isochrone approach

      U-Pb年龄(Ma) 误差(Ma) 加权平均方差 U最大含量(10-6) 238U/204Pb 样品类型 文献
      0.83 0.05 0.86 0.003 18 638~226 350 洞穴方解石 Polyak et al. (2008)
      2.11 0.06 2.8 0.49 20 000~120 000 方解石 Walker et al. (2006)
      2.17 0.06 7.9 1.34 3 000~90 000 方解石 Walker et al. (2006)
      2.19 0.47 1.6 0.001 5 849~13 744 洞穴方解石 Polyak et al. (2008)
      2.24 0.08 85 1.71 6 000~50 000 方解石 Walker et al. (2006)
      2.68 0.49 0.53 0.001 3 056~5 420 洞穴方解石 Polyak et al. (2008)
      3.43 0.43 2.3 0.004 186~940 洞穴方解石 Polyak et al. (2008)
      3.77 0.09 0.66 1.2 52 485~224 120 石笋方解石 Woodhead et al. (2006)
      3.83 0.11 0.17 1.44 36 026~1 480 200 石笋方解石 Woodhead et al. (2006)
      4.09 0.12 2.1 2.02 33 511~170 230 石笋方解石 Woodhead et al. (2006)
      14.81 0.39 2.8 169 1 961~6 510 石灰岩方解石 Cole et al. (2005)
      15.30 0.25 2.9 175 2 707~5 891 石灰岩方解石 Cole et al. (2005)
      16.14 0.40 31 30.7 123.5~427.2 石灰岩方解石 Cole et al. (2005)
      16.24 0.23 15 162 401~2584 石灰岩方解石 Cole et al. (2005)
      80.9 11 30 0.6 22~122 方解石 Wang et al. (1998)
      91.7 1.9 126 2 7.3~3 725 洞穴方解石 Lundberg et al. (2000)
      211.9 2.1 2.67 2.7 114~617 方解石 Wang et al. (1998)
      212.4 3.4 3.5 2.5 7.4~364 方解石 Wang et al. (1998)
      271 19 877 33 637~1615 方解石 Becker (2001)
      292.3 6.5 83 16.3 356~792 方解石 Becker (2001)
      下载: 导出CSV

      表  3  激光原位方解石l > Pb定年设备LA-ICPIVIS和LA-MOICPMS格度对比数据

      Table  3.   he comi > arison l > etwecn in-situ LA-ICPMS and LA-MC-ICPMS U-Ph calcite data

      样品名 U(10-6) 238U/206Pb 207Pb/206Pb t(Ma) ±2σ 误差率 加权平均力差 点数 数据来源 仪器类型
      SFN-1 0.600 23~406 0.07~0.81 15.83 0.4 3% 1.6 26 Nuriel et al.(2017) LV-MC-ICPMS
      SFN-4 0.130 17~422 0.11~0.83 13.65 0.5 4% 1.2 16 Nuriel et al.(2017) LV-MC-ICPMS
      YG3 0.350 4.4~358 0.09~0.77 16.97 0.6 4% 2.3 48 Nuriel et al.(2017) LV-MC-ICPMS
      YF4c 1.200 1.3~266 0.33~0.82 15.53 0.5 3% 0.89 47 Nuriel et al.(2017) LV-MC-ICPMS
      AHX-1 0.140 0.50~32 0.08~0.86 209.2 0.83 < 1% 3.2 85 未发表数据 LV-MC-ICPMS
      595B-2R1-84-95 0.013 0.92~8.71 0.71~0.85 115 16 14% 1.5 18 Coogan et al.(2016) LV-HR-ICPMS
      595B-3R2-12-18 0.019 2.71~20.5 0.62~0.83 86 14 16% 6.6 41 Coogan et al.(2016) LV-HR-ILTMS
      543-16R6-114.5-118 0.050 1.51~43.9 0.41~0.85 91.3 4.9 5% 1.5 42 Coogan et al.(2016) LV-HR-ICPMS
      417D-27R4-61 0.124 0.96~58.4 0.09~0.82 103.9 3.1 3% 0.31 18 Coogan et al.(2016) LV-HR-ICPMS
      418A-15R3-144 0.534 0.43~49.4 0.09~0.82 121.9 3.8 3% 4.8 28 Coogan et al.(2016) LV-HR-ICPMS
      417D-31R4-8 2.460 18.7~52.4 0.06~0.54 127.5 4.7 4% 5.3 53 Coogan et al.(2016) LV-HR-ILTMS
      TJN-6-1 0.108 121~162 0.12~0.28 37.7 1.9 5% 2.4 35 Roberts and Walker (2016) LV-HR-ICPMS
      MOL-1-2 0.037 22.2~144 0.05~0.40 40.1 4.8 12% 5.3 29 Roberts and Walker (2016) LV-HR-ICPMS
      下载: 导出CSV
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