Chronology, Geochemistry and Hf Isotope of Granite Porphyry in Wenduermiao-Jining Area, Inner Mongolia and Its Geological Significance
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摘要: 为了探讨在温都尔庙-集宁地区古亚洲洋的闭合时限以及演化过程，对该地区花岗斑岩进行了岩相学、地球化学、锆石年代学以及Hf同位素组成分析.锆石U-Pb定年显示，夸子梁花岗斑岩形成于中二叠世(270±3 Ma)；乌兰淖尔花岗斑岩形成于中三叠世(241±2 Ma)，为区域上首次发现的三叠世花岗岩.两者均有较高的SiO2、Al2O3含量及极低的Mg#；轻稀土元素相对富集，重稀土元素相对亏损，存在明显的Eu负异常；富集大离子亲石元素，亏损高场强元素.夸子梁花岗斑岩的锆石εHf(t)呈负值(0.25~-12.33)，并具有较为古老的Hf二阶段模式年龄(1 278~2 071 Ma)；乌兰淖尔花岗斑岩的锆石εHf(t)呈正值(2.03~5.94)，并具有较为年轻的Hf二阶段模式年龄(892~1 144 Ma).综合分析认为：在中二叠世之前，古亚洲在温都尔庙-集宁地区已经闭合；中二叠世期间，区域上处于后碰撞阶段，并产生夸子梁花岗斑岩；晚二叠世-早三叠世，区域上继续碰撞造山；中三叠世期间，处于造山后伸展阶段，并产生乌兰淖尔花岗斑岩.Abstract: In order to explore the closure time and evolution process of the Paleo Asian ocean in Wenduermiao-Jining area, it analyzes the petrology, geochemistry, geochronology and zircon Hf isotope composition. Zircon U-Pb dating shows that, Kuaziliang granite porphyry formed in the Middle Permian (270±3 Ma), while Wulannaoer granite porphyry formed in the Middle Triassic (241±2 Ma) that is the first Triassic granite discovered in the region. These rocks characterize with high contents of SiO2, Al2O3, very low Mg# values. They also display enrichment in LREEs and LILEs, depletion in HREEs and HFSEs, with obviously negative Eu anomalies. Kuaziliang granite porphyry exhibits negative εHf(t) values (0.25 to -12.33), old Hf isotopic tDM2 from 1 278 Ma to 2 071 Ma, indicating that it was derived from partial melting of ancient crustal material, while Wulannaoer granite porphyry exhibits positive εHf(t) values (2.03-5.94), relatively new Hf isotopic tDM2 from 892 Ma to 1 144 Ma, indicating that it was derived from partial melting of juvenile crustal material. Analyzed by synthesis, it speculates that before the Middle Permian, the Paleo-Asian ocean was closed in the Wenduertemple-Jining area; during the Middle Permian, the region is in the post-collision stage, forming the Kuaziliang granite porphyry. During Late Permian through Early Triassic, continuous collision orogeny in the region; the Middle Triassic, the region is in the post-orogenic extension stage, forming the Wulannaoer granite porphyry.
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图 1 大地构造单元图和土牧尔台研究区的地质简图
1.下二叠统苏吉组；2.上石炭统-下二叠统拴马桩组；3.寒武系-奥陶系阿牙登组；4.白云鄂博群白音宝拉格组；5.白云鄂博群呼吉尔图组；6.中二叠世花岗斑岩；7.中二叠世花岗岩；8.早二叠世花岗闪长岩；9.早二叠世黑云二长花岗岩；10.早二叠世角闪辉长岩；11.实测断层；12.采样位置；大地构造单元图据Xiao et al.(2003)修改
Fig. 1. Simplified geologic map of the Tumuertai study area
图 2 大地构造单元图和温都尔庙研究区地质简图
1.下二叠统三面井组；2.上石炭统阿木山组；3.上石炭统本巴图组；4.上石炭统酒局子组；5.志留系西别河组；6.寒武-奥陶系白乃庙群；7.温都尔庙群哈尔哈达组；8.温都尔庙群桑达来呼都格组；9.中三叠世花岗斑岩；10.早二叠世花岗闪长斑岩；11.早二叠世花岗闪长岩；12.早二叠世黑云角闪石英闪长岩；13.早志留世英云闪长岩；14.晚奥陶世奥长花岗岩；15.早奥陶世蛇纹石化橄榄岩；16.寒武纪第三世辉长岩；17.实测断层；18.采样位置；大地构造单元图据Xiao et al.(2003)修改
Fig. 2. Simplified geologic map of the Wenduermiao study area
图 3 乌兰淖尔及夸子梁花岗斑岩的野外照片和岩相学照片
a.乌兰淖尔花岗斑岩野外照片；b.乌兰淖尔花岗斑岩岩相学照片；c.夸子梁花岗斑岩野外照片；d.夸子梁花岗斑岩岩相学照片；Qz.石英；Pl.斜长石；Mc.微斜长石；Bt.黑云母；Pert.条纹长石
Fig. 3. Specimen photos and photomicrographs of Wulannaoer and Kuaziliang granite porphyries
图 4 夸子梁与乌兰淖尔花岗斑岩的锆石阴极发光图像
实线圆圈为U-Pb年龄测试点，虚线圆圈为Hf同位素测试点，括号内为Hf同位素测试值
Fig. 4. CL images of zircons for Kuaziliang and Wulannaoer granite porphyries
图 5 夸子梁(a)与乌兰淖尔(b)花岗斑岩锆石U-Pb谐和图
Fig. 5. U-Pb concordia diagrams of zircon for Kuaziliang (a) and Wulannaoer (b) granite porphyries
图 6 夸子梁及乌兰淖尔花岗斑岩TAS图解(a据Middlemost，1994)和A/NK-A/CNK图解(b)
Fig. 6. TAS (a, after Middlemost, 1994) and A/NK vs. A/CNK (b) classification diagrams for Kuaziliang and Wulannaoer granite porphyries
图 7 夸子梁和乌兰淖尔花岗斑岩的球粒陨石标准化稀土元素配分图(a)和原始地幔标准化微量元素蛛网图(b)
a图标准化值据Boynton(1984)；b图标准化值据Sun and McDonough(1989)
Fig. 7. Chondrite-normalized REE patterns (a) and primitive mantle-normalized trace element spider diagrams (b) for Kuaziliang and Wulannaoer granite porphyries
图 8 夸子梁及乌兰淖尔花岗斑岩锆石εHf(t)-t图解
Fig. 8. εHf(t) vs. zircon age plot for Kuaziliang and Wulannaoer granite porphyries
图 9 夸子梁及乌兰淖尔花岗斑岩R1-R2图解(a)和Rb-Y+Nb图解(b)
a据Batchelor and Bowden(1985)；b据Pearce et al.(1984)
Fig. 9. R1-R2 (a) and Rb vs. Y+Nb (b) diagrams for Kuaziliang and Wulannaoer granite porphyries
表 1 夸子梁花岗斑岩及乌兰淖尔花岗斑岩LA-ICP-MS锆石U-Pb定年分析结果
Table 1. Zircon U-Pb dating results for Kuaziliang and Wulannaoer granite porphyries
测点号 含量(10-6) Th/U 同位素比值 年龄(Ma) Th U 206Pb/238U 1σ 207Pb/235U 1σ 206Pb/238U 1σ 207Pb/235U 1σ JN2013-10 1 215 402 0.53 0.038 2 0.000 4 0.268 3 0.012 8 242 3 241 10 2 154 318 0.48 0.038 0 0.000 5 0.266 0 0.011 5 240 3 239 9 3 154 192 0.80 0.040 1 0.001 4 0.280 6 0.025 9 253 8 251 20 4 110 242 0.45 0.038 6 0.000 5 0.286 7 0.014 4 244 3 256 11 5 94 210 0.45 0.038 3 0.000 5 0.252 2 0.012 7 242 3 228 10 6 71 175 0.40 0.038 1 0.000 5 0.287 8 0.014 6 241 3 257 11 7 131 272 0.48 0.037 5 0.000 4 0.256 0 0.010 9 237 3 231 9 8 137 285 0.48 0.038 3 0.000 5 0.273 5 0.010 1 242 3 245 8 9 159 334 0.48 0.037 9 0.000 4 0.263 5 0.010 7 240 3 237 9 10 147 261 0.56 0.036 3 0.000 9 0.256 2 0.016 5 230 5 232 13 11 129 263 0.49 0.038 1 0.000 5 0.271 9 0.011 8 241 3 244 9 12 142 314 0.45 0.038 2 0.000 7 0.291 4 0.020 8 242 4 260 16 13 12 294 0.04 0.038 3 0.001 0 0.296 1 0.016 9 242 6 263 13 14 10 236 0.04 0.037 9 0.000 5 0.280 0 0.013 1 240 3 251 10 15 12 305 0.04 0.038 1 0.000 5 0.291 0 0.010 6 241 3 259 8 P31N40-04 1 115 149 0.77 0.042 8 0.001 3 0.333 5 0.042 1 270 8 292 32 2 446 518 0.86 0.043 9 0.001 6 0.343 9 0.023 0 277 10 300 17 3 236 367 0.64 0.042 5 0.000 8 0.300 1 0.017 6 268 5 266 14 4 166 306 0.54 0.042 0 0.000 8 0.296 9 0.015 3 265 5 264 12 5 191 193 0.99 0.042 2 0.000 9 0.300 7 0.024 3 267 6 267 19 6 115 220 0.52 0.043 4 0.001 0 0.331 4 0.020 7 274 6 291 16 7 208 246 0.84 0.043 2 0.000 8 0.299 9 0.018 1 273 5 266 14 8 151 278 0.54 0.042 0 0.001 2 0.291 1 0.033 2 265 8 259 26 9 237 347 0.68 0.042 6 0.001 1 0.278 9 0.018 0 269 7 250 14 10 293 312 0.94 0.043 0 0.000 7 0.310 5 0.017 5 272 4 275 14 11 90 116 0.77 0.043 2 0.001 8 0.352 4 0.032 1 273 11 307 24 12 208 341 0.61 0.042 8 0.001 7 0.315 3 0.029 4 270 10 278 23 13 118 168 0.71 0.042 3 0.001 4 0.280 9 0.021 6 267 9 251 17 14 285 417 0.68 0.042 6 0.001 3 0.284 2 0.037 7 269 8 254 30 15 66 83 0.80 0.042 8 0.001 1 0.319 2 0.021 4 270 7 281 16 16 62 114 0.55 0.043 6 0.001 3 0.308 2 0.030 0 275 8 273 23 17 39 83 0.47 0.043 1 0.001 1 0.295 7 0.025 0 272 7 263 20 
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表 2 夸子梁花岗斑岩及乌兰淖尔花岗斑岩锆石Hf同位素分析结果
Table 2. Zircon Hf isotopic data for Kuaziliang and Wulannaoer granite porphyries
测点号 176Yb /177Hf 2σ 176 Lu/177Hf σ 176 Hf/177Hf σ εHf(0) εHf(t) 2σ t(Ma) tDM1(Ma) tDM2(Ma) JN2013-10 1 0.044 575 0.000 209 0.000 871 0.000 004 0.282 761 0.000 023 -0.4 4.77 0.81 240 693 966 2 0.118 626 0.004 567 0.002 157 0.000 087 0.282 753 0.000 026 -0.7 4.54 0.92 253 729 990 3 0.063 023 0.001 190 0.001 125 0.000 012 0.282 683 0.000 027 -3.2 2.03 0.95 244 809 1 144 4 0.154 701 0.002 172 0.002 986 0.000 040 0.282 790 0.000 026 0.6 5.49 0.91 242 691 922 5 0.136 999 0.001 993 0.002 719 0.000 031 0.282 802 0.000 037 1.1 5.94 1.30 241 668 892 6 0.075 786 0.001 540 0.001 342 0.000 019 0.282 729 0.000 027 -1.5 3.50 0.95 237 747 1 045 7 0.153 809 0.001 732 0.003 239 0.000 036 0.282 774 0.000 032 0.1 4.62 1.14 230 721 967 8 0.079 092 0.001 877 0.001 397 0.000 037 0.282 700 0.000 022 -2.5 2.51 0.79 240 790 1 110 P31N40-04 1 0.048 636 0.000 286 0.000 960 0.000 005 0.282 384 0.000 023 -13.7 -7.97 0.81 270 1 225 1 798 2 0.070 741 0.001 252 0.001 407 0.000 021 0.282 337 0.000 020 -15.4 -9.70 0.70 270 1 305 1 907 3 0.100 383 0.002 809 0.002 149 0.000 047 0.282 277 0.000 023 -17.5 -12.01 0.82 268 1 419 2 051 4 0.084 372 0.000 740 0.001 546 0.000 014 0.282 511 0.000 023 -9.2 -3.69 0.82 265 1 064 1 523 5 0.160 377 0.001 552 0.003 182 0.000 045 0.282 514 0.000 029 -9.1 -3.70 1.02 273 1 108 1 529 6 0.101 801 0.000 584 0.001 837 0.000 016 0.282 481 0.000 027 -10.3 -4.71 0.95 269 1 115 1 591 7 0.071 923 0.000 491 0.001 344 0.000 006 0.282 519 0.000 023 -8.9 -3.20 0.80 273 1 046 1 498 8 0.089 335 0.000 792 0.001 666 0.000 013 0.282 266 0.000 026 -17.9 -12.33 0.91 267 1 416 2 071 9 0.126 973 0.000 983 0.002 404 0.000 018 0.282 622 0.000 022 -5.3 0.25 0.79 272 926 1 278
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表 3 夸子梁和乌兰淖尔花岗斑岩主量元素(%)、稀土和微量元素(10-6)
Table 3. Major (%), rare earth and trace element (10-6) for Kuaziliang and Wulannaoer granite porphyries
样品号 乌兰淖尔花岗斑岩 夸子梁花岗斑岩 JN2013-10-1 JN2013-10-2 JN2013-10-3 P31H40-3 P31H40-4 P31H40-5 SiO2 73.5 71.9 71.8 74.4 74.9 75.0 Al2O3 14.05 14.50 14.50 13.05 13.25 13.30 TFe2O3 2.09 2.83 2.47 1.96 1.83 1.89 CaO 0.17 0.10 0.19 0.35 0.42 0.41 MgO 0.09 0.09 0.11 0.16 0.15 0.15 K2O 4.95 5.19 5.08 5.28 5.11 5.24 Na2O 3.55 4.04 4.38 3.18 3.43 3.34 TiO2 0.16 0.22 0.22 0.15 0.15 0.16 P2O5 0.11 0.05 0.06 0.02 0.02 0.03 MnO 0.01 0.02 0.01 0.03 0.04 0.04 LOI 1.37 1.19 1.04 0.89 0.80 0.80 Total 100.05 100.13 99.86 99.47 100.1 100.36 Mg# 7.86 5.93 8.11 13.92 13.97 13.59 Na2O+K2O 8.50 9.23 9.46 8.46 8.54 8.58 A/CNK 1.22 1.17 1.11 1.13 1.11 1.12 Cr < 10 10 10 20 20 20 Rb 146.0 131.0 116.5 182.0 196.5 198.0 Cs 4.24 2.82 0.83 3.13 5.05 3.90 Sr 25.1 35.2 105.0 63.3 69.2 70.2 Ba 241 293 384 912 910 947 V 7 6 23 16 26 14 Sc 5 5 5 5 5 5 Nb 28.7 26.2 25.3 15.4 17.5 17.0 Ta 1.4 1.2 1.1 1.0 1.1 1.1 Zr 408 498 502 264 293 290 Hf 11.3 11.4 11.2 7.9 8.7 8.6 U 6.19 4.09 6.83 2.78 3.94 4.10 Th 27.0 20.8 20.5 19.10 20.7 20.9 La 114.5 73.3 75.9 33.8 37.5 32.1 Ce 222 149.5 149.0 132.5 135.0 137.5 Pr 23.5 16.10 16.75 6.46 7.43 6.43 Nd 75.6 52.5 56.0 21.4 24.9 21.3 Sm 11.55 8.64 9.45 4.02 4.65 4.23 Eu 0.34 0.67 0.74 0.46 0.50 0.48 Gd 9.12 6.95 7.31 4.27 4.73 4.61 Tb 1.28 1.03 1.04 0.82 0.81 0.78 Dy 7.55 6.40 6.34 5.69 5.67 5.80 Ho 1.47 1.29 1.23 1.24 1.22 1.22 Er 4.17 3.68 3.62 4.28 4.40 4.39 Tm 0.61 0.53 0.49 0.63 0.65 0.63 Yb 3.91 3.25 3.30 4.44 4.61 4.36 Lu 0.58 0.48 0.52 0.62 0.66 0.61 Y 38.5 32.3 33.2 35.2 33.6 34.7 ΣREE 476.18 324.32 331.69 220.63 232.73 224.44 LREE 447.49 300.71 307.84 198.64 209.98 202.04 HREE 28.69 23.61 23.85 21.99 22.75 22.40 LREE/HREE 15.60 12.74 12.91 9.03 9.23 9.02 LaN/YbN 21.01 16.18 16.50 5.46 5.83 5.28 δEu 0.10 0.26 0.26 0.34 0.32 0.33 δCe 0.99 1.02 0.98 2.06 1.87 2.21 注：Mg#=100×(MgO/40.304 4)/(MgO/40.304 4+TFe2O3×0.899 8/71.844)，A/CNK=Al2O3/(CaO+Na2O+K2O)(摩尔比).
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