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    运用方解石中流体包裹体最小均一温度确定塔河油田奥陶系油气成藏时间:来自激光原位方解石U-Pb年龄的证据

    徐豪 郭小文 曹自成 王斌 刘永立 陈家旭 张旭友 罗涛

    徐豪, 郭小文, 曹自成, 王斌, 刘永立, 陈家旭, 张旭友, 罗涛, 2021. 运用方解石中流体包裹体最小均一温度确定塔河油田奥陶系油气成藏时间:来自激光原位方解石U-Pb年龄的证据. 地球科学, 46(10): 3535-3548. doi: 10.3799/dqkx.2020.376
    引用本文: 徐豪, 郭小文, 曹自成, 王斌, 刘永立, 陈家旭, 张旭友, 罗涛, 2021. 运用方解石中流体包裹体最小均一温度确定塔河油田奥陶系油气成藏时间:来自激光原位方解石U-Pb年龄的证据. 地球科学, 46(10): 3535-3548. doi: 10.3799/dqkx.2020.376
    Xu Hao, Guo Xiaowen, Cao Zicheng, Wang Bin, Liu Yongli, Chen Jiaxu, Zhang Xuyou, Luo Tao, 2021. Application of Minimum Homogenization Temperatures of Aqueous Inclusions in Calcite Veins to Determine Time of Hydrocarbon Accumulation in Ordovician of Tahe Oilfield: Evidence from In-Situ Calcite U-Pb Dating by Laser Ablation. Earth Science, 46(10): 3535-3548. doi: 10.3799/dqkx.2020.376
    Citation: Xu Hao, Guo Xiaowen, Cao Zicheng, Wang Bin, Liu Yongli, Chen Jiaxu, Zhang Xuyou, Luo Tao, 2021. Application of Minimum Homogenization Temperatures of Aqueous Inclusions in Calcite Veins to Determine Time of Hydrocarbon Accumulation in Ordovician of Tahe Oilfield: Evidence from In-Situ Calcite U-Pb Dating by Laser Ablation. Earth Science, 46(10): 3535-3548. doi: 10.3799/dqkx.2020.376

    运用方解石中流体包裹体最小均一温度确定塔河油田奥陶系油气成藏时间:来自激光原位方解石U-Pb年龄的证据

    doi: 10.3799/dqkx.2020.376
    基金项目: 

    国家自然科学基金项目 41872139

    详细信息
      作者简介:

      徐豪(1999-), 男, 博士, 主要从事油气成藏机理研究.ORCID: 0000-0002-6265-4697.E-mail: 1169998692@qq.com

      通讯作者:

      郭小文, Email: guoxw@cug.edu.cn

    • 中图分类号: P618.13

    Application of Minimum Homogenization Temperatures of Aqueous Inclusions in Calcite Veins to Determine Time of Hydrocarbon Accumulation in Ordovician of Tahe Oilfield: Evidence from In-Situ Calcite U-Pb Dating by Laser Ablation

    • 摘要: 碳酸盐矿物中的同期烃类包裹体共生盐水包裹体均一温度变化范围较大,导致采用流体包裹体均一温度结合储层埋藏史和热演化史确定的油气成藏时间具有多解性.以塔里木盆地塔河油田奥陶系碳酸盐岩油气藏为例,基于方解石脉体中发育的流体包裹体岩相学、荧光分析和显微测温,结合激光原位方解石U-Pb定年结果,提出利用同期烃类包裹体共生盐水包裹体最小均一温度确定油气成藏时间,并确定塔河油田奥陶系碳酸盐岩储层油气充注期次和时间.塔河油田奥陶系储层共存在4期油充注,第1期至第3期油充注时间分别与3期方解石脉体形成时间一致,第4期油充注发生于3期方解石脉形成之后.对发育原生烃类包裹体的方解石脉进行激光原位U-Pb同位素绝对定年,结果指示采用同期油包裹体共生盐水包裹体最小均一温度确定的油气充注时间与方解石脉形成时间一致,说明采用同期盐水包裹体最小均一温度确定的油气充注时间更可靠.运用同期油包裹体共生盐水包裹体最小均一温度得到,塔河地区奥陶系碳酸盐岩油气藏4期油气充注时间分别对应加里东、海西、印支和燕山构造运动时期.

       

    • 图  1  塔里木盆地塔河油田构造位置和样品井位

      Fig.  1.  Structure location and location of sampling wells in the Tahe oilfield, Tarim basin

      图  2  塔河油田碳酸盐岩样品中方解石脉的透射光和阴极发光照片

      a,b. T1样品缝洞充填方解石透射光和阴极发光照片;c,d. T2样品微粉晶高角度方解石透射光和阴极发光照片;e,f. T3样品溶洞充填方解石透射光和阴极发光照片;g,h. T4样品缝洞充填方解石透射光和阴极发光照片

      Fig.  2.  Calcite vein images under transmitted light and cathodoluminescence in carbonatite samples of Tahe oilfield

      图  3  塔河油田奥陶系油包裹体透射光、荧光照片以及荧光光谱图

      a,c. T1样品缝洞充填方解石中发育的金黄色原生油包裹体透射光和荧光照片及荧光光谱图;d,f. T2样品方解石中发育的深黄色原生油包裹体透射光和荧光照片及荧光光谱图;g,i. T3样品方解石中发育的黄色原生油包裹体透射光和荧光照片及荧光光谱图;j,l. T4样品方解石中发育的蓝色次生油包裹体透射光和荧光照片及荧光光谱图

      Fig.  3.  Fluorescent, transmitted light photos and fluorescent spectrum of oil inclusions in the Ordovician of Tahe oilfield

      图  4  塔河油田碳酸盐岩中油包裹体共生盐水包裹体均一温度分布和均一温度-盐度关系

      Fig.  4.  Distribution of homogenization temperature and relationship between homogenization temperature and salinity for aqueous inclusions associated with oil inclusions developed in the carbonatite samples of Tahe oilfield

      图  5  塔河油田S118井和AT5井样品中方解石脉的稀土元素配分模式

      Fig.  5.  Rare earth element distribution pattern for calcite vein in carbonatite samples of well S118 and well AT5, Tahe oilfield

      图  6  塔河油田S118井和AT5井样品中方解石脉激光原位U-Pb同位素年龄

      Fig.  6.  In-situ calcite vein U-Pb isotope ages by laser ablation in carbonatite samples of well S118 and well AT5, Tahe oilfield

      图  7  塔河油田单个油包裹体荧光光谱λmaxQ650/500相关关系

      Fig.  7.  Plot of relationship between Q650/500 and λmax of individual oil inclusion in Tahe oilfield

      图  8  塔河油田奥陶系流体包裹体均一温度-埋藏史投影示意图

      刘永立等(2017)修改

      Fig.  8.  Schematic diagram of burial curve projected with homogenization temperatures of fluid inclusions in the Ordovician of Tahe oilfield

      表  1  塔河油田奥陶系采样清单

      Table  1.   Sampling list in Ordovician of Tahe oilfield

      样品编号 井号 层位 深度(m) 岩性描述
      T1 TS302X O1-2y 6 583.1 灰色泥晶灰岩
      T2 S118 O2yj 5 920.0 微粉晶灰岩
      T3 AT5 O2yj 6 524.7 大型溶洞巨晶方解石
      T4 S94 O1 5 959.7 黄灰色泥晶灰岩
      下载: 导出CSV

      表  2  塔河油田奥陶系T2、T3样品方解石脉稀土元素含量

      Table  2.   REE contents of calcite veins of the Ordovician in Tahe oilfield

      样品编号 La Ce Pr Nd Sm Eu Gd Tb Dy Y Ho Er Tm Yb Lu Ce异常 Eu异常
      T2-1 0.008 7 0.003 8 0.005 3 0.006 5 0.009 4 0.011 5 0.015 0 0.008 9 0.010 0 0.020 9 0.008 1 0.008 0 0.005 6 0.002 2 0.002 5 0.557 1 0.965 7
      T2-2 0.011 2 0.003 8 0.004 6 0.005 6 0.006 0 0.008 5 0.012 2 0.007 5 0.008 7 0.018 8 0.008 1 0.006 1 0.003 7 0.002 1 0.001 4 0.522 1 0.995 5
      T2-3 0.003 7 0.001 6 0.002 2 0.003 0 0.004 6 0.006 3 0.007 9 0.006 3 0.006 4 0.013 5 0.006 2 0.004 6 0.003 3 0.001 8 0.000 7 0.546 2 1.038 4
      T2-4 0.003 8 0.001 7 0.002 3 0.003 0 0.004 8 0.006 5 0.007 9 0.006 9 0.006 3 0.014 3 0.005 1 0.005 5 0.003 9 0.001 7 0.001 1 0.585 4 1.054 7
      T2-5 0.028 4 0.008 4 0.009 9 0.011 7 0.012 7 0.013 0 0.016 9 0.011 5 0.008 6 0.021 5 0.008 2 0.007 0 0.004 8 0.002 7 0.001 4 0.502 7 0.886 3
      T2-6 0.017 8 0.005 4 0.006 5 0.007 4 0.008 0 0.010 2 0.013 2 0.008 1 0.007 5 0.018 9 0.007 3 0.005 8 0.003 3 0.001 9 0.000 6 0.500 8 0.992 9
      T2-7 0.013 0 0.004 0 0.004 7 0.006 0 0.007 7 0.010 0 0.017 0 0.012 4 0.012 2 0.030 7 0.011 8 0.009 3 0.005 3 0.002 7 0.002 2 0.509 4 0.873 4
      T2-8 0.028 9 0.010 3 0.012 8 0.015 9 0.013 2 0.016 2 0.021 4 0.013 7 0.012 3 0.026 0 0.011 4 0.011 0 0.005 9 0.002 6 0.001 8 0.534 4 0.963 9
      T2-9 0.011 4 0.003 8 0.004 7 0.006 0 0.005 0 0.006 5 0.008 7 0.005 9 0.005 0 0.011 4 0.004 8 0.004 1 0.003 4 0.001 8 0.001 2 0.527 8 0.980 0
      T2-10 0.010 8 0.003 7 0.004 6 0.006 1 0.007 7 0.010 2 0.012 5 0.008 5 0.008 1 0.019 5 0.008 2 0.005 6 0.005 5 0.002 2 0.001 0 0.530 2 1.035 7
      T2-11 0.006 4 0.002 9 0.003 7 0.005 0 0.006 9 0.009 5 0.011 9 0.009 9 0.009 6 0.018 9 0.008 3 0.007 6 0.003 6 0.002 4 0.002 3 0.594 4 1.051 6
      T2-12 0.002 6 0.001 3 0.001 4 0.001 8 0.002 7 0.004 4 0.005 8 0.004 4 0.004 6 0.011 1 0.004 9 0.003 8 0.002 8 0.001 7 0.001 6 0.687 9 1.096 5
      T2-13 0.004 7 0.002 4 0.002 6 0.003 5 0.004 7 0.006 6 0.008 7 0.006 9 0.006 9 0.016 4 0.006 5 0.005 6 0.004 0 0.002 3 0.001 3 0.693 6 1.021 9
      T2-14 0.004 1 0.002 1 0.002 7 0.003 2 0.005 4 0.006 6 0.010 0 0.005 7 0.006 2 0.014 5 0.005 5 0.005 1 0.003 6 0.002 0 0.002 5 0.622 6 0.895 7
      T2-15 0.009 9 0.005 0 0.006 7 0.008 9 0.013 7 0.016 8 0.022 7 0.016 5 0.018 4 0.034 1 0.014 9 0.013 7 0.007 2 0.004 4 0.003 4 0.618 5 0.950 8
      T2-16 0.004 9 0.002 2 0.003 0 0.004 0 0.005 8 0.007 2 0.009 8 0.007 5 0.007 8 0.016 7 0.007 5 0.005 4 0.004 8 0.002 7 0.001 6 0.578 7 0.953 5
      T2-17 0.007 0 0.003 5 0.004 1 0.005 4 0.006 4 0.008 4 0.011 9 0.008 7 0.008 4 0.017 8 0.007 7 0.007 1 0.004 6 0.002 3 0.002 2 0.650 0 0.963 5
      T2-18 0.002 9 0.001 3 0.001 7 0.002 5 0.004 1 0.004 4 0.005 4 0.004 3 0.004 5 0.008 8 0.004 6 0.003 4 0.003 0 0.001 4 0.000 9 0.585 7 0.948 8
      T2-19 0.004 1 0.002 4 0.002 9 0.003 8 0.006 4 0.007 5 0.010 6 0.007 9 0.009 0 0.018 3 0.008 2 0.007 3 0.003 0 0.002 5 0.001 5 0.685 7 0.912 6
      T2-20 0.017 4 0.007 6 0.010 1 0.013 4 0.013 0 0.015 3 0.019 0 0.012 8 0.012 2 0.022 3 0.013 1 0.009 9 0.005 5 0.004 3 0.003 1 0.573 4 0.972 8
      T2-21 0.008 4 0.003 1 0.003 8 0.004 9 0.005 4 0.005 6 0.008 8 0.006 1 0.006 5 0.013 7 0.006 1 0.004 8 0.003 5 0.002 4 0.002 1 0.537 5 0.816 3
      T2-22 0.011 7 0.004 1 0.005 3 0.006 6 0.006 4 0.008 2 0.013 9 0.008 9 0.009 1 0.020 6 0.009 7 0.007 2 0.004 7 0.001 8 0.002 2 0.516 7 0.874 5
      T2-23 0.005 4 0.002 4 0.003 2 0.004 2 0.005 9 0.008 1 0.010 8 0.008 0 0.007 7 0.017 3 0.006 8 0.006 1 0.003 7 0.002 2 0.002 2 0.583 0 1.005 1
      T3-1 0.160 2 0.193 0 0.205 5 0.235 7 0.327 7 0.301 2 0.355 8 0.306 3 0.295 9 0.355 9 0.268 6 0.234 4 0.215 1 0.177 3 0.155 9 1.063 3 0.882 0
      T3-2 0.277 7 0.303 0 0.324 5 0.361 4 0.487 7 0.444 4 0.527 5 0.432 0 0.431 6 0.512 6 0.364 0 0.314 0 0.279 3 0.212 8 0.179 4 1.009 4 0.876 2
      T3-3 0.286 4 0.312 2 0.330 7 0.364 2 0.477 1 0.427 8 0.533 0 0.434 5 0.432 5 0.533 7 0.368 1 0.337 5 0.289 1 0.225 2 0.187 5 1.014 4 0.848 2
      T3-4 0.282 5 0.311 6 0.317 4 0.358 1 0.469 9 0.427 8 0.523 2 0.423 4 0.416 2 0.502 6 0.361 2 0.315 8 0.271 6 0.206 0 0.167 0 1.040 5 0.862 8
      T3-5 0.252 4 0.277 9 0.294 5 0.331 8 0.448 6 0.433 3 0.510 7 0.426 4 0.465 8 0.488 1 0.361 3 0.340 4 0.298 8 0.229 1 0.184 8 1.019 4 0.905 3
      T3-6 0.073 0 0.094 3 0.114 3 0.136 9 0.202 0 0.195 7 0.235 8 0.203 6 0.215 2 0.242 6 0.192 0 0.174 7 0.165 4 0.146 8 0.133 7 1.032 9 0.896 8
      T3-7 0.233 5 0.268 6 0.311 9 0.357 8 0.532 8 0.495 4 0.605 8 0.534 8 0.528 8 0.616 3 0.454 1 0.398 9 0.356 5 0.288 3 0.238 3 0.995 3 0.871 9
      T3-8 0.212 3 0.257 5 0.289 8 0.333 9 0.492 8 0.446 3 0.563 9 0.482 6 0.485 7 0.577 4 0.420 2 0.384 2 0.339 5 0.283 7 0.232 1 1.038 3 0.846 6
      T3-9 0.128 5 0.159 5 0.176 0 0.207 0 0.308 3 0.289 8 0.376 2 0.334 5 0.340 8 0.408 9 0.316 5 0.290 5 0.282 5 0.254 6 0.217 1 1.060 8 0.851 0
      T3-10 0.117 2 0.143 0 0.165 7 0.190 7 0.293 5 0.263 9 0.349 8 0.309 9 0.331 4 0.384 4 0.294 2 0.278 2 0.277 0 0.250 7 0.220 8 1.025 9 0.823 6
      T3-11 0.170 3 0.213 9 0.246 9 0.287 7 0.436 4 0.395 4 0.500 0 0.447 2 0.463 7 0.523 7 0.404 1 0.379 3 0.369 4 0.347 5 0.302 8 1.043 5 0.846 4
      T3-12 0.244 7 0.298 2 0.349 5 0.402 8 0.620 5 0.549 1 0.692 1 0.628 2 0.629 7 0.705 2 0.545 5 0.500 0 0.469 9 0.434 0 0.373 0 1.019 8 0.837 9
      T3-13 0.252 9 0.295 2 0.325 6 0.369 6 0.539 6 0.475 9 0.596 1 0.522 9 0.529 7 0.605 9 0.455 1 0.410 9 0.378 5 0.348 2 0.301 8 1.028 9 0.839 1
      T3-14 0.283 8 0.315 1 0.332 3 0.375 9 0.499 5 0.453 7 0.544 8 0.448 6 0.448 9 0.524 1 0.381 4 0.325 6 0.285 2 0.221 3 0.184 8 1.026 1 0.869 7
      T3-15 0.275 4 0.300 8 0.317 3 0.352 1 0.461 1 0.423 1 0.507 1 0.423 8 0.419 4 0.500 7 0.356 7 0.314 4 0.273 3 0.212 1 0.173 9 1.017 4 0.875 1
      T3-16 0.273 6 0.299 6 0.316 4 0.356 0 0.469 5 0.425 0 0.493 3 0.412 9 0.403 0 0.480 0 0.334 7 0.294 7 0.245 7 0.192 6 0.153 8 1.018 4 0.883 0
      T3-17 0.258 1 0.287 8 0.297 1 0.326 4 0.425 4 0.394 9 0.478 5 0.401 8 0.382 9 0.470 7 0.327 9 0.289 8 0.244 2 0.192 6 0.152 2 1.039 4 0.875 3
      T3-18 0.298 4 0.320 4 0.326 6 0.364 5 0.471 4 0.428 7 0.510 9 0.417 2 0.402 4 0.495 9 0.348 2 0.301 8 0.264 2 0.200 7 0.166 1 1.026 1 0.873 6
      下载: 导出CSV
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