Geochemical Characteristics, Detrital Zircon Age and Provenance Analysis of Upper Cretaceous Quantou Formation in Kalun Lake Area, Southeast Margin of Songliao Basin
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摘要: 选取吉林长春卡伦湖地区的上白垩统泉头组砂岩，通过X荧光光谱仪、ICP-MS等离子体质谱仪以及锆石LA-ICP-MS U-Pb定年等方法进行岩石地球化学及碎屑锆石U-Pb年代学研究，探讨研究区物源以及区域沉积构造背景. 结果显示，研究区泉头组源区岩石的主要类型为具有大陆边缘构造背景的火成岩组合；根据研究区主、微量元素和稀土元素特征以及样品锆石的U-Pb年龄，松辽盆地张广才岭地区与研究区所采集样品的地化数据表现出相似性，二者岩石都富集大离子亲石元素以及轻稀土元素，亏损高场强元素和重稀土元素，具有火山弧岩浆岩的地球化学特征等，并且研究区泉头组的碎屑锆石U-Pb年龄分布峰值和比例与前人研究的张广才岭地区的花岗岩锆石U-Pb年龄分布具有极大相似性. 结合研究区泉头组砂体展布、沉积体系以及东部隆起区水系展布特征及前人研究结果，综合认为研究区物源来自张广才岭地区，泉头组下段主要沉积作用为填平补齐，充填粗碎屑岩和红色泥岩不整合于阜新组之上，上段以超覆式沉积作用为主，以河流相红色砂泥岩沉积逐渐向盆地中心过渡. 对于重塑松辽盆地东南缘构造与物源演化过程、矿产资源分布以及松辽盆地东南缘泉头组砂岩储层评价做出重要贡献，为盆地东南缘潜在铀矿层的预测以及铀矿区铀源的进一步评价等方面提供了重要借鉴.Abstract: In this paper, the sandstone of Upper Cretaceous Quantou Formation in Kalun Lake area, Changchun, Jilin Province is selected to study the rock geochemistry and detrital zircon U-Pb chronology by means of X-fluorescence spectrometer, ICPMS plasma mass spectrometer and zircon La-ICP-MS U-Pb dating, so as to explore the provenance and regional sedimentary tectonic background of the study area. The results show that the main types of rocks in the source area of Quantou Formation in the study area are igneous rock assemblages with continental margin tectonic background; According to the characteristics of major elements, trace elements and rare earth elements in the study area and the U-Pb age of zircon samples, the geochemical data of samples collected in Zhangguangcailing area of Songliao basin and the study area show similarity. Both rocks are rich in large ion lithophile elements and light rare earth elements, and depleted in high field strength elements and heavy rare earth elements, showing the geochemical characteristics of volcanic arc magmatic rocks. The peak value and proportion of detrital zircon U-Pb age distribution of Quantou Formation in the study area are very similar to that of granite zircon U-Pb age distribution in zhangguangcailing area. Combined with the sand body distribution, sedimentary system and water system distribution characteristics of the eastern uplift area in the study area and the previous research results, it is comprehensively considered that the material source in the study area comes from Zhangguangcailing area. The main sedimentation of the lower section of Quantou Formation is leveling and filling, and the filled coarse clastic rock and red mudstone are not integrated on Fuxin Formation, and the upper section is dominated by overlapping sedimentation. The red sandstone and mudstone deposits of fluvial facies show gradual transition to the center of the basin. This paper makes an important contribution to reshaping the structure and provenance evolution process, mineral resource distribution and sandstone reservoir evaluation of Quantou Formation in the southeast edge of Songliao basin, and provides an important reference for the prediction of potential uranium deposits in the southeast edge of Songliao basin and the further evaluation of uranium sources in uranium mining areas.
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图 3 研究区含矿目的层钻孔柱状图（a）及矿段岩心（b）
Fig. 3. Borehole histogram (a) and ore section core of ore bearing target layer (b) in study area
图 4 卡伦湖地区泉头组砂岩碎屑锆石CL图像（a, c, e, g）和LA-ICP MS U-Pb年龄谐和图（b, d, f, h）
Fig. 4. CL images of detrital zircon (a, c, e, g) and LA-ICP MS U-Pb age concordia map (b, d, f, h) of detrital zircon from Quantou Formation in Kalun Lake area
图 5 卡伦湖地区泉头组砂岩碎屑锆石年龄谱（a, b, c, d）
a.KLHZK2.G1锆石年龄谱图；b.KLHZK2.G2锆石年龄谱图；c.KLHZK3.G1锆石年龄谱图；d.KLHZK3.G2锆石年龄谱图
Fig. 5. Detrital zircon age spectrum of Quantou Formation sandstone in Kalun Lake area (a, b, c, d)
图 6 研究区泉头组样品主量元素对SiO2哈克图解
Fig. 6. Huck diagram of major elements of Cretaceous Quantou Formation samples in the study area
图 7 SiO2-K2O图解(a)和A/CNK-A/NK图解(b)
Fig. 7. SiO2-K2O diagram (a) and A/CNK-A/NK diagram (b)
图 8 原始地幔标准化微量元素蛛网图(a)和砂岩球粒陨石标准化稀土配分模式(b)
Fig. 8. Normalized trace element spider diagram of primitive mantle (a) and normalized REE distribution pattern of sandstone chondrites (b)
图 9 研究区泉头组砂岩F1-F2源区环境判别(a)、La/Th-Hf判别(b)和Th-Hf-Co判别(c)
a. 据Roser and Korsch（1986）；b. 据Floyd et al.（1989）；c. 据Condie（1993）
Fig. 9. Environmental discrimination map (a), La/Th-Hf discrimination map (b) and Th-Hf-Co discrimination map (c) of F1-F2 source area of Quantou Formation sandstone in the study area
图 10 研究区泉头组砂岩构造环境La-Th-Sc, Th-Co-Zr/10, Th-Sc-Zr/10判别图解
A. 大洋岛弧；B. 大陆岛弧；C. 活动大陆边缘；D. 被动大陆边缘
Fig. 10. Discrimination diagrams of structural environment La-Th-Sc, Th-Co-Zr/10, Th-Sc-Zr/10 of Quantou Formation sandstone in the study area
图 12 松辽盆地东南缘上白垩统泉头组泉四段砂体等厚图
Fig. 12. Isopach map of sand body in the fourth member of Quantou Formation of Upper Cretaceous in the southeast edge of Songliao basin
图 13 卡伦湖地区泉头组砂岩锆石U-Pb年龄谱与邻区锆石年龄谱对比
Fig. 13. Zircon U-Pb age spectrum of sandstone of Quantou Formation in Kalun Lake area and its adjacent area
表 1 研究区周围地区锆石年龄数据统计
Table 1. Statistical table of zircon age data in the area around the study area
序号 样品号 年龄 分布地区 测试方法 参考文献 1 NZS-4 96~135 Ma 齐齐哈尔碾子山 LA-ICP-MS 秦锦华（2017） 2 NZS-7 102~131 Ma 齐齐哈尔碾子山 LA-ICP-MS 秦锦华（2017） 3 NZS-3 (112.54±0.44) Ma 齐齐哈尔碾子山 LA-ICP-MS 秦锦华（2017） 4 15YL38-1 (163±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 5 3082TW (166±2.2) Ma 张广才岭南部 LA-ICP-MS 任永健（2019） 6 DB07TW (168.15±0.4) Ma 张广才岭南部 LA-ICP-MS 任永健（2019） 7 1074TW (171±2)~(181±3) Ma 张广才岭南部 LA-ICP-MS 任永健（2019） 8 14GW327 (172±5) Ma 依兰团山子 LA-ICP-MS 董玉（2018） 9 014-1-TW02 (172.7±1.6) Ma 张广才岭南部 LA-ICP-MS 任永健（2019） 10 BCGE-01 (173±1.5) Ma 张广才岭 LA-ICP-MS 冯光英等（2019） 11 BCG-01 (173±2.0) Ma 张广才岭 LA-ICP-MS 冯光英等（2019） 12 14GW302 (177±11) Ma 依兰龙兰港 LA-ICP-MS 董玉（2018） 13 DA-N2-1-14 177~198 Ma 东安金矿区 LA-ICP-MS 李碧乐等（2016） 14 97SW009 (179±7) Ma 虎峰 TIMS 邵济安等（2013） 15 DP13TW17 (182.9±0.67) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 16 15YL14-1 (183±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 17 15YL18-4 (183±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 18 15YL12-4 (184±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 19 15YL10-1 (186±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 20 15YL28-1 (187±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 21 188 Ma 大稗子沟 LA-ICP-MS 冯光英等（2019） 22 11HSZ3-4 (189±1) Ma 太安屯组 LA-ICP-MS 郝文丽等（2014） 23 15YL36-5 (191±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 24 15YL40-1 (192±1) Ma 张广才岭 LA-ICP-MS Zhu et al.（2017） 25 P16LT69B8 (197±1) Ma 小兴安岭东南段 LA-ICP-MS 韩振哲（2011） 26 P6LT3 (197±1) Ma 小兴安岭东南段 LA-ICP-MS 韩振哲（2011） 27 DP12TW9 (198.8±0.56) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 28 TW6252 (199.7±0.73) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 29 TW7265 (199.7±2.6) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 30 TW6098 (200.3±1.7) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 31 D2382 (200±1) Ma 小兴安岭东南段 LA-ICP-MS 韩振哲（2011） 32 LS (201±3) Ma 亚布力冷山 LA-ICP-MS 邵济安等（2013） 33 TW3049 (201.6±1.7) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 34 STH (202.2±3.4) Ma 亚布力石头河 LA-ICP-MS 邵济安等（2013） 35 H15-09 210~185 Ma 铁力市桃山镇 LA-ICP-MS 葛茂卉等（2020） 36 M23 (212.9±1.5) Ma 小九寨沟西 LA-ICP-MS 邵济安等（2013） 37 M13 (214.5±1.4) Ma 新兴林场西北 LA-ICP-MS 邵济安等（2013） 38 H22-6 214 Ma 张广才岭 Rb-Sr 邵济安等（2013） 39 16GW026 217~180 Ma 依兰依愚公路 LA-ICP-MS 董玉（2018） 40 M24 (220.4±1) Ma 小九寨沟西 LA-ICP-MS 邵济安等（2013） 41 16GW189 220~212 Ma 依兰演武基 LA-ICP-MS 董玉（2018） 42 H26-1 220 Ma 张广才岭 Rb-Sr 邵济安等（2013） 43 H42-1 220 Ma 张广才岭 Rb-Sr 邵济安等（2013） 44 16GW022 222~189 Ma 依兰龙兰港 LA-ICP-MS 董玉（2018） 45 014-1-TW01 223~252 Ma 张广才岭南部 LA-ICP-MS 任永健（2019） 46 DP17TW11 (224.3±1.4) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 47 11HSZ2-1 (226±3) Ma 杨木岗组 LA-ICP-MS 郝文丽等（2014） 48 DP16TW7 (229.8±0.75) Ma 张广才岭南部 LA-ICP-MS 敖光（2016） 49 11HSZ5-1 234~329 Ma 唐家屯组上部 LA-ICP-MS 郝文丽等（2014） 50 M38 (244.7±1.2) Ma 红星林场南 LA-ICP-MS 邵济安等（2013） 51 15GW265 (266±2) Ma 桦南青背岩 LA-ICP-MS 董玉（2018） 52 18HL-07 271~248 Ma 依兰县德裕镇 LA-ICP-MS 葛茂卉等（2020） 53 14GW667 (274±2) Ma 依兰大理石厂 LA-ICP-MS 董玉（2018） 54 16GW032 277~218 Ma 依兰三道岗 LA-ICP-MS 董玉（2018） 55 15GW075 278~266 Ma 桦南孟家岗 LA-ICP-MS 董玉（2018） 56 16GW033 283~196 Ma 依兰团山子 LA-ICP-MS 董玉（2018） 57 16GW180 283~216 Ma 依兰高速路 LA-ICP-MS 董玉（2018） 58 16GW102 284~208 Ma 桦南宏泰村 LA-ICP-MS 董玉（2018） 59 11HSZ4-1 289~302 Ma 一面坡群 LA-ICP-MS 郝文丽等（2014） 60 16GW024 297~189 Ma 依兰龙兰港 LA-ICP-MS 董玉（2018） 61 15GW248 (300±3) Ma 桦南横头山 LA-ICP-MS 董玉（2018） 62 15GW261 (300±5) Ma 桦南青背岩 LA-ICP-MS 董玉（2018） 63 15GW235 (303±3) Ma 桦南驼腰子 LA-ICP-MS 董玉（2018） 64 18HYS-1 (392±3) Ma 张广才岭福兴屯组 LA-ICP-MS 何雨思等（2019） 65 14HYS-1 (392±3) Ma 张广才岭福兴屯组 LA-ICP-MS 何雨思等（2019） 66 11HNA13-1 (426±6) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 67 16PH20-1 (449±3) Ma 曙光和小金沟地区 LA-ICP-MS 王志伟（2017） 68 16PH21-5 (453±2) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 69 16PH15-6 453~418 Ma 曙光和小金沟地区 LA-ICP-MS 王志伟（2017） 70 15XH9-1 (461±5) Ma 曙光和小金沟地区 LA-ICP-MS 王志伟（2017） 71 15XH32-1 (475±7) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 72 HDL2-2 (482±8) Ma 曙光和小金沟地区 LA-ICP-MS 王志伟（2017） 73 11HSZ2-1 (485±12) Ma 杨木岗组 LA-ICP-MS 郝文丽等（2014） 74 15XH10-1 (495±7) Ma 曙光和小金沟地区 LA-ICP-MS 王志伟（2017） 75 15XH30-1 (496±11) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 76 16PH21-1 (502±4) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 77 11HNA7-1 (516±4) Ma 塔东地区 LA-ICP-MS 王志伟（2017） 78 11HSZ2-1 (783±9) Ma 杨木岗组 LA-ICP-MS 郝文丽等（2014） 
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