The Cretaceous Volcanic Rocks in the Eastern North China Craton: Records of Heterogeneous Modification of Recycled Crustal Components
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摘要: 华北克拉通东部在130~120 Ma早白垩世期间经历强烈改造，并伴随大规模岩浆活动.对比研究了这一时期山东鲁西地区、郯庐断裂带和胶东半岛玄武安山岩-安山岩等幔源岩石的地球化学特征和Sr-Nd同位素组成，探讨了各地区火山岩源区性质以及造成源区不均一性的可能原因. 这些火山岩均来自富集型地幔且受地壳组分的混染影响较小，并主要经历了单斜辉石、磷灰石和Ti-Fe氧化物的分离结晶，但相较于郯庐断裂带和胶东半岛而言，鲁西火山岩的演化程度更低. 不同地区火山岩均具有岛弧型微量元素和富集的Sr-Nd同位素组成，其中，鲁西北部火山岩表现为（87Sr/86Sr）i < 0.706的Ⅰ型富集地幔特征，而鲁西南部、郯庐断裂带以及胶东地区火山岩则具有（87Sr/86Sr）i > 0.706的Ⅱ型富集地幔特征，这暗示上述火山岩可能均来自被再循环地壳物质改造的富集地幔源区，且其源区富集程度具有从西北到东南逐渐增强的趋势. Sr-Nd同位素两端元混合模拟显示，鲁西北部火山岩EMⅠ型同位素特征可能与其地幔源区受华北下地壳物质的交代有关，而鲁西中-南部、郯庐断裂带和胶东地区火山岩EMⅡ型同位素特点则更可能是源区受三叠纪俯冲扬子陆壳组分改造的结果. 古太平洋板块来源的俯冲流体交代和水化也对这些地区的富集岩石圈地幔有不同程度改造. 因此，山东半岛不同地区早白垩世火山岩记录了不同性质壳源组分对华北克拉通东部岩石圈地幔的影响，这一差异性改造对华北东部岩石圈地幔的破坏和减薄有重要制约作用.Abstract: The eastern North China Craton (NCC) experienced strong modification during the Early Cretaceous(130~120 Ma), accompanied by intensive magmatism. Here we compared the geochemical and Sr-Nd isotopic compositions of the Early Cretaceous (130~120 Ma) basaltic andesites to andesites from the Luxi region, the Tan-Lu fault, and the Jiaodong Peninsula in Shandong Province, to investigatethe characteristics of their melting sources, and further discussed the possible cause for the heterogeneity of the source. These rocks with insignificant crustal contamination were generally derived from the lithospheric mantle. They mainly experienced the fractional crystallization of clinopyroxene, apatite, and Ti-Fe oxide during magma differentiation. However, compared to those volcanic rocks in the Tan-Lu fault and the Jiaodong Peninsula, the volcanic rocks from northern Luxi experienced a relatively lower degree of evolution. These volcanic rocks are characterized by arc-like trace element patterns and enriched Sr-Nd isotopes. The Luxi volcanic rocks are characterized by EMⅠ-type mantle source (87Sr/86Sri < 0.706), where as those rocks from the central-southern Luxi, the Tan-Lu fault, and the Jiaodong areas are characterized by EMⅡ-type mantle source (87Sr/86Sri > 0.706), indicating that they were both derived from an enriched lithospheric mantle reservoir which was modified by crustal components. Noticeably, the extent of the enrichment of Sr-Nd isotopes in those volcanic rocks increases gradually from the Northwest to the Southeast. End-member mixing model indicates that the EMⅠ-type mantle source beneath the northern Luxi region was possibly metasomatized by components from the lower crust of the NCC, whereas the EMⅡ-type mantle beneath the central-southern Luxi, the Tan-Lu fault, and the Jiaodong districts was likely metasomatized by materials from the subducted Yangtze continental crust. Fluids from the subducted Paleo-Pacific plate subsequently metasomatized and hydrated the enriched lithospheric mantle of the NCC, leading to the modification in different degrees. Therefore, the Early Cretaceous volcanic rocks in the Shandong Province record significant modification within the lithospheric mantle induced by diverse crustal components. The heterogeneous modification provided critical constraints on the destruction of the lithospheric mantle beneath the eastern NCC.
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图 1 山东省构造地质图（a、b）及早白垩世中基性火山岩年龄直方图（c）
图中黄色小圆圈代表火山岩分布位置，对应数字代表火山岩年龄（单位为Ma）；图a和图b分别修改自Zhu et al.，（2012b）和Cao et al.，（2020）；年龄数据来源文献详情见附件1
Fig. 1. Tectonic subdivision and simplified geological map of Shandong Province (a、b) and age histogram of the early Cretaceous mafic to intermediate volcanic rocks (c)
图 2 山东早白垩世火山岩野外露头及显微结构特征
a~c. 鲁西章丘（ZQ）斑状结构玄武安山岩，斑晶主要为自形的斜长石（Pl）和单斜辉石（Cpx），斑晶大小0.2~1 mm. 基质主要为微晶斜长石，少量玻璃质；d~f. 鲁西邹平（ZP）斑状结构玄武安山岩，斑晶主要为自形-半自形斜长石和单斜辉石，斑晶大小0.2~0.5 mm. 基质主要为微晶斜长石和玻璃质；g~i. 胶东莱阳（LY）斑状结构玄武安山岩，斑晶主要为半自形-它形斜长石和单斜辉石，斑晶大小0.2~0.5 mm. 基质主要为玻璃质和微晶斜长石
Fig. 2. Field outcrop and microstructure characteristics of Early Cretaceous volcanic rocks in Shandong Province
图 3 山东不同地区早白垩世中基性火山岩总碱度（K2O+Na2O）vs.SiO2图解（下文图例同此）
图中黑色实线参考Le Bas et al.，（1986），红色实线参考Irvine and Baragar，（1971）. 实线与虚线的范围是根据已发表的山东早白垩世中基性火山岩的主量数据进行描绘，数据来源文献见附件1，全文同此
Fig. 3. Plots of total alkalinity (K2O+Na2O) vs. SiO2 for Early Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 4 山东不同地区早白垩世中基性火山岩主量元素协变图解
图中实线与虚线的范围是根据前人已发表的山东早白垩世中基性火山岩的主量数据进行描绘
Fig. 4. SiO2 variation diagrams ofrepresentative major elements for Early Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 5 山东不同地区早白垩世中基性火山岩稀土元素配分模式图（a、c）和微量元素蛛网图（b、d）
原始地幔和球粒陨石标准化数据源自Sun and McDonough，（1989）；图中阴影区域是根据前人已发表的山东早白垩世中基性火山岩的微量数据进行描绘，数据来源的文献见附件1，全文同此
Fig. 5. Chondrite-normalized REE patterns and primitive mantle-normalized spidergrams and forEarly Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 6 山东不同地区早白垩世中基性火山岩（87Sr/86Sr）i、εNd（t）和Nb/U vs. SiO2图解
图中实线与虚线的范围是根据前人已发表的山东早白垩世中基性火山岩的主量、微量元素以及Sr-Nd同位素数据进行描绘，所有数据来源文献见附件1，下文同此
Fig. 6. Plot of (87Sr/86Sr)i、εNd(t)and Nb/U vs. SiO2 for Early Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 7 山东不同地区早白垩世中基性火山岩Sr-Nd同位素特征
华北古生代岩石圈地幔（SCLM）值据古生代金伯利岩及其种橄榄岩包体数据（Zhang et al.，2002）；鲁西EMⅠ和EMⅡ地幔域值据Lan et al.，（2018），苏鲁造山带基性岩脉和扬子下地壳组成据Cao et al.，（2019），胶东基性岩脉组成据Cao et al.，（2020）. 模拟计算使用参数见表 1
Fig. 7. Plots of Sr-Nd isotopic characteristics for Early Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 8 山东不同地区早白垩世中基性火山岩Sr-Nd同位素等值线分布图
Sr-Nd同位素填图的数据来自前人已发表的相关数据，各地区中基性火山岩的Sr-Nd同位素富集程度自西北向东南逐渐升高，揭示山东陆下岩石圈地幔性质在空间上的不均一性
Fig. 8. Sr-Nd isotopic contour maps of Early Cretaceous mafic to intermediate volcanic rocks from different regions in Shandong Province
图 9 再循环物质对华北克拉通不均一性改造模式图
扬子板块北西向俯冲，对华北板块东南缘岩石圈地幔改造程度更强，受俯冲方向和俯冲影响范围的制约，克拉通内部岩石圈地幔受俯冲扬子陆壳物质的影响逐渐趋弱；黄色圆圈代表火山岩分布点
Fig. 9. Schematic cartoon showing the heterogeneous modification of NCC by recycled component
表 1 两端元混合模拟使用的参数表
Table 1. Parameter table for mixed simulation of two end elements
端元 87Sr/86Sr Sr（10-6） εNd Nd（10-6） 参考文献 华北下地壳 0.705 1 250 -30 60 Huang et al.(2012) 扬子下地壳 0.711 300 -30 20 Jahn et al.(1999) SCLM-1 0.704 60 -5 16 Guo et al.(2013) SCLM-2 0.708 95 -4.7 21 Zhang et al.(2002) 
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