电子探针微区紫外阴极荧光分析系统及在沉积碎屑岩分析中的应用

杨勇; 陈能松

Volume 28 Issue 3

May 2003

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Article Navigation > Earth Science > 2003 > 28(3): 357-360

YANG Yong, CHEN Neng-song, 2003. An EPMA Ultraviolet Cathodoluminescence Micro-Area Measuring System and Its Application to Petrogenetic Analysis for Clasolites. Earth Science, 28(3): 357-360.

Citation:

YANG Yong, CHEN Neng-song, 2003. An EPMA Ultraviolet Cathodoluminescence Micro-Area Measuring System and Its Application to Petrogenetic Analysis for Clasolites. Earth Science, 28(3): 357-360.

YANG Yong, CHEN Neng-song, 2003. An EPMA Ultraviolet Cathodoluminescence Micro-Area Measuring System and Its Application to Petrogenetic Analysis for Clasolites. Earth Science, 28(3): 357-360.

Citation:

YANG Yong, CHEN Neng-song, 2003. An EPMA Ultraviolet Cathodoluminescence Micro-Area Measuring System and Its Application to Petrogenetic Analysis for Clasolites. Earth Science, 28(3): 357-360.

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An EPMA Ultraviolet Cathodoluminescence Micro-Area Measuring System and Its Application to Petrogenetic Analysis for Clasolites

YANG Yong^{1, 2
,},
CHEN Neng-song²

1.
Laser Institute, Huazhong University of Science and Technology, Wuhan 430074, China
2.
Faculty of Earth Sciences, China University of Geosciences, Wuhan 430074, China

Received Date: 2002-06-08
Publish Date: 2003-05-25

Abstract

Abstract

A practical detection scheme with JCXA-733 EPMA-based micro-ultraviolet visible cathodoluminescence has been constructed to analyze both invisible and visible luminescence phenomena for the micro-area surface of solid samples. The wavelength and intensity of the luminescence depend largely on composition, crystal structure and crystal defection of the materials, and also on the growth conditions, growth processes and the environmental conditions where occur the materials. Ultraviolet and ultra-infrared detection of samples will yield more inherent information over broad waveband. Application of this method to the analysis of the source for quartz detritus and of the generation relation between micro rims of secondary enlargement quartz in glauconite-bearing quartz sandstone from Tangshan region, Hebei Province, reveals both the distinct features of ultraviolet luminescence and the radiate-damnification-induced color center at 287 nm wavelength. Hence, it can be deduced that this sandstone experienced two generations of cementation and that its quartz detritus were derived from complex sources. This technique provides a new tool for the investigation into the detritus sources and cementation histories for clasonites and shows a great significance for the analysis of sedimentary basins, oil and gas reservoir.
- cathodoluminescence (CL),
- micro-area analysis,
- ultraviolet (UV),
- spectrum

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References(14)

References

[1]	刘恩科, 朱秉升. 半导体物理学[M]. 上海: 上海科学技术出版社, 1984. LIU E K, ZHU B S. Semiconductor physics[M]. Shanghai: Shanghai Science and Technology Press, 1984.
[2]	张铭诚, 袁自强, 万固存, 等. 电子扫描成象及微区分析[M]. 北京: 原子能出版社, 1987. ZHANG M C, YUAN Z Q, WAN G C, et al. Electron scan image and micro-area analysis[M]. Beijing: Atomic Energy Press, 1987.
[3]	宋志敏. 阴极发光地质学基础[M]. 武汉: 中国地质大学出版社, 1993. SONG Z M. Cathodoluminescence basic for geology[M]. Wuhan: China University of Geosciences Press, 1993.
[4]	陈丽华, 缪昕, 于众. 扫描电镜在地质上的应用[M]. 北京: 科学出版社, 1986. CHEN L H, MIAO X, YU Z. SEM application in geology[M]. Beijing: Science Press, 1986.
[5]	周科子. 扫描电镜中的阴极发光技术及其在地学中的应用[J]. 电子显微学报, 1985, 4(3): 31-40. https://www.cnki.com.cn/Article/CJFDTOTAL-DZXV198503003.htm ZHOU K Z. SEM cathodoluminescence technology and application in geology[J]. Journal of Electron Micro-Analyses, 1985, 4(3): 31-40. https://www.cnki.com.cn/Article/CJFDTOTAL-DZXV198503003.htm
[6]	程峰, 于少勇, 邢德敬, 等. 阴极发光技术在储层研究中的应用[J]. 断块油气田, 1998, 5(6): 17-19. https://www.cnki.com.cn/Article/CJFDTOTAL-DKYT199806004.htm CHENG F, YU S Y, XING D J, et al. Application of cathodoluminescence technology in study of oil and gas reservoirs[J]. Faultage Oil and Gas Field, 1998, 5(6): 17-19. https://www.cnki.com.cn/Article/CJFDTOTAL-DKYT199806004.htm
[7]	林传易, 田淑贵, 洪文兴, 等. 不同变生程度锆石的阴极射线发光谱[J]. 矿物学报, 1992, 12(4): 323-328. doi: 10.3321/j.issn:1000-4734.1992.04.006 LIN C Y, TIAN S G, HONG W X, et al. Cathodoluminescence spectra of zircons with different degrees of metamictization[J]. Acta Mineralogica Sinica, 1992, 12(4): 323-328. doi: 10.3321/j.issn:1000-4734.1992.04.006
[8]	孙铁铮, 李援朝, 高山. 阴极射线发光测试系统的应用[J]. 分析测试技术与仪器, 1997, 3(3): 129-134. https://www.cnki.com.cn/Article/CJFDTOTAL-FXCQ703.000.htm SUN T Z, LI Y C, GAO S. Principle and application of CR-3 measuring system for cathodoluminescence[J]. Analysis and Testing Technology and Instruments, 1997, 3(3): 129-134. https://www.cnki.com.cn/Article/CJFDTOTAL-FXCQ703.000.htm
[9]	方伟. 储集砂岩碎屑石英次生加大边定量分析技术及其演变特征研究[J]. 石油实验地质, 1992, 14(1): 96- 101. https://www.cnki.com.cn/Article/CJFDTOTAL-SYSD199201012.htm FANG W. Quantitative analysis technology of the secondary enlarged pore-fringes in the clastic quartz of reservoir sandstones, and an approach to the evolution characteristics of reservoir sandstones[J]. Experiment Petroleum Geology, 1992, 14(1): 96-101. https://www.cnki.com.cn/Article/CJFDTOTAL-SYSD199201012.htm
[10]	傅竹西, 吴自勤. 阴极射线发光分析方法及其在新材料研究中的应用[J]. 物理, 2000, 29(2): 96-104. https://www.cnki.com.cn/Article/CJFDTOTAL-WLZZ200002007.htm FUZ X, WU Z Q. Cathodoluminescence analysis and its applications in new materials[J]. Physics, 2000, 29(2): 96-104. https://www.cnki.com.cn/Article/CJFDTOTAL-WLZZ200002007.htm
[11]	Dlemos R S, Kearsley A T, Pembroke J W, et al. Complex quartz growth histories in granite revealed by scanning cathodoluminescence techniques[J]. Geol Mag, 1997, 134(4): 549-552. doi: 10.1017/S0016756897007280
[12]	郭常新, 傅竹西, 施朝淑. 阴极射线激发下ZnO薄膜室温紫外发光的超线性增长规律[J]. 发光学报, 1998, 19 (3): 239-241. https://www.cnki.com.cn/Article/CJFDTOTAL-FGXB803.010.htm GUO C X, FU Z X, SHI C S. Super linear increase phenomenon of UV luminescence of ZnO film under cathodoluminescent excitation[J]. Chinese Journal of Luminescence, 1998, 19(3): 239-241. https://www.cnki.com.cn/Article/CJFDTOTAL-FGXB803.010.htm
[13]	Demars C, Pagel M, Deloule R, et al. Cathodoluminescence of quartz from sandstones: interpretation of UV range by determination of trace element distributions and fluid-inclusion P-T-X properties in authigenic quartz[J]. American Mineralogist, 1996, 81: 891-901. https://pubs.geoscienceworld.org/msa/ammin/article/81/7-8/891/43190/Cathodoluminescence-of-quartz-from-sandstones
[14]	Barbarand J, Pagel M. Cathodoluminescence study of apatite crystals[J]. American Mineralogist, 2001, 86: 473 -484. https://pubs.geoscienceworld.org/msa/ammin/article/86/4/473/133839/cathodoluminescence-study-of-apatite-crystals