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    中国百强科技报刊

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    Volume 39 Issue 9
    Sep.  2014
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    Article Contents
    Zhang Suxin, Zhang Yi, He Detao, 2014. Study on Particle Phase Analysis Method of Energy Disperse Spectroscopy: A Case Study of Cenozoic Basalts from Datong, Shanxi Province. Earth Science, 39(9): 1301-1308. doi: 10.3799/dqkx.2014.111
    Citation: Zhang Suxin, Zhang Yi, He Detao, 2014. Study on Particle Phase Analysis Method of Energy Disperse Spectroscopy: A Case Study of Cenozoic Basalts from Datong, Shanxi Province. Earth Science, 39(9): 1301-1308. doi: 10.3799/dqkx.2014.111

    Study on Particle Phase Analysis Method of Energy Disperse Spectroscopy: A Case Study of Cenozoic Basalts from Datong, Shanxi Province

    doi: 10.3799/dqkx.2014.111
    • Received Date: 2014-02-02
    • Publish Date: 2014-09-01
    • The Particle Phase Analysis (PPA) method by means of Quanta 200 scanning electron microscope (SEM), GENESIS energy disperse spectroscopy (EDS) can analyze particle size and phase automatically. A systematic experimental is carried out to verify the PPA method in this study, using samples of Cenozoic basalts from Datong. We apply the PPA method of EDS to study the thin section and polished section in the geological field for the first time, which yield a series of morphology and chemical composition data of different phases such as phase types, particle number of each phase, average diameter, area, roundness, length-width ratio, chemical composition. The proportion and average particle diameter of each phase can also be obtained as well, overcoming the shortages of traditional method in thin section and polished section. It proves that PPA guarantees significant data for the study of mineralogy, petrology and ore deposit geology.

       

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    • EDAX Inc., 2003. Genesis Spectrum User's Manual.
      FEI Company, 2002. The Quanta 200 User's Operation Manual, 1-22.
      Goldstein, J.I., Newbury, D.E., Joy, D.C., et al., 2003. Scanning Electron Microscopy and X-Ray Microanalysis. Springer.
      Gottlieb, P., Wilkie, G., Sutherland, D., et al., 2000. Using Quantitative Electron Microscopy for Process Mineralogy Applications. Journal of Metals, 52(4): 24-25. doi: 10.1007/s11837-000-0126-9
      Hoal, K.O., Appleby, S.K., Stammer, J.G., et al., 2009. SEM-Based Quantitative Mineralogical Analysis of Peridotite, Kimberlite, and Concentrate. Lithos, 112: 41-46. doi: 10.1016/j.lithos.2009.06.009
      Jiang, M.L., 2009. Particle Size Analysis and Its Geological Applications. Journal of Oil and Gas Technology, 31(1): 161-163 (in Chinese).
      Kong, M.G., 2004. Simple Discussion of the Analytic Technology of Energy Spectrum in Kevex SIGMATM X-Ray Energy Dispersive Spectrometer. Modern Scientific Instruments, (1): 58-59 (in Chinese with English abstract). http://en.cnki.com.cn/Article_en/CJFDTOTAL-XDYQ200401019.htm
      Li, X.T., 2006. EDS Analysis Methods and Characteristics. 2006 Oxford Instruments Microanalysis Seminar Handouts, 1-40 (in Chinese).
      Liao, Q.C., Lan, F.L., 1990. SEM Principles and Application Technology. Metallurgical Industry Press, Beijing, 285-287 (in Chinese).
      Liu, X.H., Feng, M.Y., Luo, J.L., et al., 2009. Analysis of Influence Factors on Sandstone Reservoirs of the Chang 8 and Chang 6 Members in Xifeng Oil Field, Southwestern Ordos Basin. Journal of Northwest University (Natural Science Edition), 39(1): 102-108 (in Chinese with English abstract). http://en.cnki.com.cn/Article_en/CJFDTOTAL-XBDZ200901033.htm
      Liu, X.F., 1982a. Particle Size Analysis Lectures (Four). Minerals and Rocks, (3): 96-110 (in Chinese).
      Liu, X.F., 1982b. Particle Size Analysis Lectures (Three). Minerals and Rocks, (2): 123-132 (in Chinese).
      Lyman, C.E., 1990. Scanning Electron Microscopy, X-Ray Microanalysis, and Analytical Electron Microscopy: A Laboratory Workbook. Springer.
      Pan, Z., L., Zhao, A.X., Pan, T.H., 2004. Crystallography and Mineralogy (Volume Two). Geological Publishing House, Beijing, 245-263 (in Chinese).
      Pownceby, M., MacRae, C., Wilson, N., 2007. Mineral Characterisation by EPMA Mapping. Minerals Engineering, 20(5): 444-451. doi: 10.1016/j.mineng.2006.10.014
      Ran, J., Du, G., Pan, Z.X., 2011. Study on Methods for Particle Size Analysis of Sediment Samples. Rock and Mineral Analysis, 30(6): 669-676 (in Chinese with English abstract). http://en.cnki.com.cn/Article_en/CJFDTOTAL-YKCS201106006.htm
      Yang, Y.Z., He, J.S., 1982. An Application of the Data Concerning Grain-Size Analysis of Thin Section in Discriminating Sedimentary Environment of the Late Precambrian in the Qinling Range. Geology of Shaanxi, 2(2): 95-100 (in Chinese with English abstract).
      Zhang, D.T., 2009. Scanning Electron Microscopy and Energy Dispersive Analysis Techniques. South China University of Technology Press, Guangzhou (in Chinese).
      蒋明丽, 2009. 粒度分析及其地质应用. 石油天然气学报, 31(1): 161-163. https://www.cnki.com.cn/Article/CJFDTOTAL-JHSX200901042.htm
      孔明光, 2004. 浅谈Kevex SIGMATMX射线能谱仪中的能谱分析技术. 现代科学仪器, (1): 58-59. doi: 10.3969/j.issn.1003-8892.2004.01.020
      李香庭, 2006. EDS的分析方法与特点. 2006牛津仪器显微分析研讨会讲义, 1-40.
      廖乾初, 蓝芬兰, 1990. 扫描电镜原理及应用技术. 北京: 冶金工业出版社, 285-287.
      刘小洪, 冯明友, 罗静兰, 等, 2009. 西峰油田长8和长6储层物性影响因素分析. 西北大学学报(自然科学版), 39(1): 102-108. https://www.cnki.com.cn/Article/CJFDTOTAL-XBDZ200901033.htm
      刘岫峰, 1982a. 粒度分析讲座(四). 矿物岩石, (3): 96-110. https://www.cnki.com.cn/Article/CJFDTOTAL-KWYS198106014.htm
      刘岫峰, 1982b. 粒度分析讲座(三). 矿物岩石, (2): 123-132. https://www.cnki.com.cn/Article/CJFDTOTAL-KWYS198202014.htm
      潘兆橹, 赵爱醒, 潘铁虹, 2004. 结晶学及矿物学(下册). 北京: 地质出版社, 245-263.
      冉敬, 杜谷, 潘忠习, 2011. 沉积物粒度分析方法的比较. 岩矿测试, 30(6): 669-676. doi: 10.3969/j.issn.0254-5357.2011.06.004
      杨应章, 何建社, 1984. 利用薄片粒度资料判别高山河组及罗圈组岩相的探讨. 陕西地质, 2(2): 95-100. https://www.cnki.com.cn/Article/CJFDTOTAL-SXDY198402009.htm
      张大同, 2009. 扫描电镜与能谱仪分析技术. 广州: 华南理工大学出版社.
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