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| Citation: | Liu Wenquan, Liu Bin, Luo Qiang, Qi Jiaming, Wu Jianyong, Wei Wenfang, 2022. In-Situ Trace Element and Sulfur Isotope of Pyrite Constrain Ore Genesis in Shulouqiu Uranium Deposit, North Guangdong. Earth Science, 47(1): 178-191. doi: 10.3799/dqkx.2021.181
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The Shulouqiu uranium deposit is an important part of Changjiang uranium ore field. However, there are relatively fewer studies on its ore-forming fluid properties, source and metallogenic environment. Based on the characteristics of pyrite and other mineral paragenesis, the formation of pyrite in the Shulouqiu uranium deposit is divided into three stages: pre-metallogenic period (Py Ⅰ), syn-metallogenic period (Py Ⅱ) and late-metallogenic period (Py Ⅲ). Meanwhile, the syn-metallogenic period (Py Ⅱ) is divided into early metallogenic stage (Py Ⅱa) and main metallogenic stage (Py Ⅱb). The trace elements and sulfur isotopes of pyrite formed in different periods were analyzed by inductively coupled plasma mass spectrometry (LA-MC-ICP-MS). The results show that the content of Co and Ni of Py Ⅰ is mostly lower than that of the test line, and the ratios of Co/ Ni of Py Ⅱa and Py Ⅱb are mainly 1-5, suggesting that it is the cause of hydrothermal. The δ34S value of Py Ⅰ ranges from +0.41‰ to +2.02‰, which is mantle sulfur. The δ34S value of Py Ⅱa ranges from -9.15‰ to -11.3‰, which is similar to that of the Py Ⅱa (-10.9‰ to -7.10‰) in the Guidong compound granite. Meanwhile, it has the same origin as the Zhuguang compound granite, indicating that the sulfur of Py Ⅱa comes from the Zhuguang compound granite. From the early metallogenic stage to the main metallogenic stage, the δ34S values of pyrite increase from (-9.15‰ to -11.3‰) to (-4.58‰ to -8.48‰), indicating that the oxygen fugacity of ore-forming fluid decreases. Uranium-rich fluid migration was formed in the oxidized fluid leaching of ore-bearing rocks in the early stage of mineralization, and uranium-rich fluid was changed into reducing environment in the main metallogenic period, which resulted in uranium precipitation. Combined with the characteristics of pyrite trace elements, the fluid in the early stage of uranium deposit in Shulouqiu is a high temperature magmatic hydrothermal, and the fluid in the metallogenic period is a medium-low temperature meteoric water.
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