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    辽宁后仙峪硼矿区古元古代电气石岩: 锆石特征及SHRIMP定年

    张艳飞 刘敬党 肖荣阁 王生志 王瑾 包德军

    张艳飞, 刘敬党, 肖荣阁, 王生志, 王瑾, 包德军, 2010. 辽宁后仙峪硼矿区古元古代电气石岩: 锆石特征及SHRIMP定年. 地球科学, 35(6): 985-999. doi: 10.3799/dqkx.2010.112
    引用本文: 张艳飞, 刘敬党, 肖荣阁, 王生志, 王瑾, 包德军, 2010. 辽宁后仙峪硼矿区古元古代电气石岩: 锆石特征及SHRIMP定年. 地球科学, 35(6): 985-999. doi: 10.3799/dqkx.2010.112
    ZHANG Yan-fei, LIU Jing-dang, XIAO Rong-ge, WANG Sheng-zhi, WANG Jin, BAO De-jun, 2010. The Hyalotourmalites of Houxianyu Borate Deposit in Eastern Liaoning: Zircon Features and SHRIMP Dating. Earth Science, 35(6): 985-999. doi: 10.3799/dqkx.2010.112
    Citation: ZHANG Yan-fei, LIU Jing-dang, XIAO Rong-ge, WANG Sheng-zhi, WANG Jin, BAO De-jun, 2010. The Hyalotourmalites of Houxianyu Borate Deposit in Eastern Liaoning: Zircon Features and SHRIMP Dating. Earth Science, 35(6): 985-999. doi: 10.3799/dqkx.2010.112

    辽宁后仙峪硼矿区古元古代电气石岩: 锆石特征及SHRIMP定年

    doi: 10.3799/dqkx.2010.112
    基金项目: 

    国家自然科学基金项目 40073013

    辽宁省国土资源厅基金项目 20050142

    详细信息
      作者简介:

      张艳飞(1982-), 男, 在读博士生, 主要从事矿床地球化学研究.E-mail: zhangyanfei1234@163.com

    • 中图分类号: P597

    The Hyalotourmalites of Houxianyu Borate Deposit in Eastern Liaoning: Zircon Features and SHRIMP Dating

    • 摘要: 为了确定辽东硼矿含硼岩系中电气石岩的形成时代, 对后仙峪硼矿区电气石岩首次进行了锆石SHRIMP U-Pb年龄测定.阴极发光图像显示, 锆石具核-边结构, 锆石核部多具振荡环带, 为高Th/U值的岩浆碎屑锆石; 锆石边部无明显结构变化, 为变质成因.岩浆碎屑锆石和变质锆石的年龄分别为2 171~2 175 Ma和1 894~1 906 Ma.结合野外地质和岩相学研究, 认为后仙峪硼矿区电气石岩原岩为古元古代克拉通裂谷环境中源于地壳再循环组分混染的亏损地幔的中酸性岩浆活动引发海底喷流作用的产物, 其原岩形成时代为古元古代中期(2 171~2 175 Ma), 并在稍后(1 894~1 906 Ma)遭受变质作用叠加改造.

       

    • 图  1  后仙峪硼矿床地质略图(据黄作良等(1996)修改)

      1.古元古界电气石变粒岩夹黑云变粒岩;2.古元古界黑云变粒岩;3.古元古界蛇纹石化镁橄榄岩及镁质大理岩;4.古元古界电英岩;5.硼矿体;6.片麻状花岗岩;7.伟晶岩;8.闪长玢岩;9.斜长煌斑岩;10.闪长岩;11.推测断层;12.地层产状;13.第四系;14.太古宙古陆;15.裂谷斜坡区;16.裂谷中央凹陷区;17.控制裂谷的深大断裂;18.古断裂;19.地质界线;20.取样位置

      Fig.  1.  Geological map of the Houxianyu boron deposit

      图  2  电气石岩的宏观和微观构造特点

      a.条带(纹)状电气石岩;b.厚层状电气石岩被石英细脉切割;c.电气石岩中较自形的电气石颗粒;d.电气石岩中电气石的筛状结构;Tou.电气石;Q.石英

      Fig.  2.  Tectonites in the hyalotourmalites at different scales

      图  3  后仙峪硼矿区电气石岩(N13、N14、N02)的锆石阴极发光照片

      图中椭圆(~30 μm)为锆石SHRIMP U-Pb测年位置,其编号与表 1中一致

      Fig.  3.  Cathodoluminescence images of zircons from hyalotourmalite(N13, N14, N02) in Houxianyu borate deposit

      图  4  后仙峪硼矿区电气石岩锆石SHRIMP U-Pb年龄谐和图

      Fig.  4.  Concordia diagrams of SHRIMP U-Pb data for zircons from hyalotourmalites in Houxianyu borate deposit

      表  1  后仙峪硼矿区电气石岩锆石SHRIMP U-Pb年龄测定结果

      Table  1.   SHRIMP U-Pb isotope data for zircons from hyalotourmalite in Houxianyu borate deposit


      样点
      206Pbc(%) U(10-6) Th(10-6) 232Th/238U 206Pb*
      (10-6)
      206Pb/238U
      年龄(Ma)
      207Pb/206Pb
      年龄(Ma)
      不和谐度
      (%)
      207Pb*/206Pb* ±% 207Pb*/235U ±% 206Pb*/238U ±% 相关误差
      中粗粒电气石岩(N13)
      1.1C 0.08 138 77 0.57 47.1 2 152±28 2 154±13 0 0.134 25 0.73 7.340 1.7 0.396 3 1.5 0.899
      2.1C 0.05 814 274 0.35 241.0 1 906±23 2 055± 5.7 7 0.126 88 0.32 6.017 1.4 0.343 9 1.4 0.974
      2.2R 0.03 587 14 0.02 168.0 1 859±24 1 910±7.2 3 0.116 99 0.40 5.391 1.6 0.334 2 1.5 0.967
      2.3R 0.01 496 25 0.05 148.0 1 921±25 1 902±12 -1 0.116 42 0.65 5.572 1.6 0.347 1 1.5 0.916
      3.1C 0.17 167 84 0.52 57.8 2 177±28 2 163±13 -1 0.134 88 0.72 7.470 1.7 0.401 7 1.5 0.901
      3.2R 0.01 492 18 0.04 132.0 1 756±22 1 902±8.2 8 0.116 45 0.45 5.028 1.5 0.313 1 1.4 0.953
      4.1C 0.03 306 182 0.61 101.0 2 094±26 2 177±8.5 4 0.136 07 0.49 7.200 1.5 0.383 7 1.4 0.947
      4.2R 0.05 474 23 0.05 139.0 1 895±23 1 893±8.3 0 0.115 86 0.46 5.460 1.5 0.341 8 1.4 0.951
      5.1C 0.01 180 90 0.51 61.3 2 150±28 2 179±11 1 0.136 13 0.64 7.430 1.6 0.396 0 1.5 0.920
      6.1C 0.07 944 123 0.13 145.0 1 060±21 1 541±10 31 0.095 65 0.54 2.357 2.2 0.178 7 2.2 0.970
      7.1C 0.04 298 148 0.51 103.0 2 178±27 2 179±8.2 0 0.136 20 0.47 7.550 1.5 0.402 0 1.4 0.950
      7.2R 0.04 602 17 0.03 185.0 1 973±24 1 918±7.0 -3 0.117 49 0.39 5.800 1.5 0.358 0 1.4 0.964
      8.1C 0.06 129 86 0.69 45.9 2 230±29 2 173±13 -3 0.135 73 0.72 7.740 1.7 0.413 4 1.6 0.907
      8.2R 0.01 537 29 0.06 155.0 1 873±23 1 897±7.5 1 0.116 13 0.42 5.400 1.5 0.337 2 1.4 0.959
      9.1C 0.03 346 270 0.81 122.0 2 213±28 2 169±7.6 -2 0.135 43 0.43 7.650 1.6 0.409 5 1.5 0.960
      9.2R 0.03 562 30 0.06 171.0 1 954±24 1 912±7.4 -2 0.117 08 0.41 5.717 1.5 0.354 1 1.4 0.960
      10.1C 0.04 159 88 0.57 58.8 2 302±31 2 199±11 -5 0.137 76 0.63 8.150 1.7 0.429 3 1.6 0.929
      10.2R 0.03 649 27 0.04 197.0 1 951±47 1 911±6.7 -2 0.117 01 0.37 5.700 2.8 0.353 3 2.8 0.991
      11.1C 0.02 446 223 0.52 158.0 2 229±29 2 178±6.9 -2 0.136 11 0.40 7.750 1.6 0.413 1 1.5 0.968
      11.2R 0.02 467 18 0.04 134.0 1 854±24 1 916±9.4 3 0.117 38 0.53 5.395 1.6 0.333 3 1.5 0.944
      12.1C 0.07 216 125 0.60 73.2 2 142±27 2 163±9.4 1 0.134 95 0.54 7.330 1.6 0.394 1 1.5 0.939
      12.2R 0.01 547 20 0.04 161.0 1 903±23 1 889±7.2 -1 0.115 58 0.40 5.472 1.5 0.343 4 1.4 0.963
      13.1C 0.01 172 99 0.59 58.8 2 156±27 2 182±11 1 0.136 38 0.65 7.470 1.6 0.397 2 1.5 0.916
      13.2R 0.03 475 22 0.05 136.0 1 857±23 1 899±8.2 2 0.116 26 0.46 5.353 1.5 0.333 9 1.4 0.951
      14.1C 0.15 123 67 0.56 42.4 2 165±29 2 164±14 0 0.135 00 0.82 7.430 1.8 0.399 1 1.6 0.887
      14.2R 0.02 534 23 0.04 145.0 1 766±22 1 904±7.6 7 0.116 57 0.42 5.065 1.5 0.315 1 1.4 0.958
      15.1C 0.02 386 154 0.41 135.0 2 201±27 2 172±8.6 -1 0.135 66 0.50 7.610 1.5 0.407 0 1.4 0.944
      16.1C 0.04 198 137 0.72 67.6 2 161±27 2 183±10 1 0.136 51 0.58 7.500 1.6 0.398 3 1.5 0.930
      16.2R 0.01 714 27 0.04 213.0 1 922±23 1 919±6.3 0 0.117 59 0.35 5.633 1.5 0.347 4 1.4 0.971
      17.1C 0.09 138 68 0.51 48.0 2 187±32 2 180±13 0 0.136 27 0.73 7.590 1.9 0.403 8 1.7 0.920
      17.2R - 484 21 0.05 146.0 1 938±24 1 905±7.6 -2 0.116 63 0.42 5.638 1.5 0.350 6 1.4 0.958
      18.1C 0.00 149 134 0.93 49.6 2 111±30 2 197±13 4 0.137 60 0.74 7.350 1.8 0.387 5 1.7 0.912
      18.2R 0.02 562 30 0.06 156.0 1 801±22 1 900±9.8 5 0.116 34 0.55 5.171 1.5 0.322 3 1.4 0.933
      19.1C 0.06 135 147 1.13 44.1 2 084±28 2 142±13 3 0.133 33 0.73 7.020 1.7 0.381 6 1.6 0.905
      19.2R 0.02 541 18 0.03 147.0 1 776±22 1 897±8.1 6 0.116 10 0.45 5.076 1.5 0.317 1 1.4 0.953
      细粒电气石岩(N14)
      1.1 0.01 397 295 0.77 138.0 2 190±27 2 183±8.1 0 0.136 50 0.46 7.61 1.5 0.404 5 1.4 0.952
      2.1 -- 387 217 0.58 135.0 2 194±27 2 142±8.5 -2 0.133 32 0.48 7.45 1.5 0.405 3 1.4 0.947
      3.1 0.04 132 81 0.64 45.6 2 175±31 2 182±13 0 0.136 38 0.73 7.55 1.8 0.401 4 1.7 0.916
      4.1 0.01 314 176 0.58 110.0 2 198±27 2 167±8.2 -1 0.135 24 0.47 7.58 1.5 0.406 4 1.4 0.950
      5.1 0.09 257 174 0.70 83.0 2 054±27 2 153±10 5 0.134 12 0.58 6.94 1.7 0.375 3 1.6 0.937
      6.1 0.01 133 65 0.51 45.2 2 147±28 2 166±13 1 0.135 14 0.73 7.36 1.7 0.395 2 1.5 0.901
      中细粒电气石岩(N02)
      1.1C 0.08 200 81 0.42 65.7 2 081±26 2 166±11 4 0.135 14 0.62 7.10 1.6 0.381 0 1.5 0.921
      2.1C 0.13 151 71 0.49 48.7 2 058±26 2 137±12 4 0.132 93 0.69 6.89 1.6 0.376 0 1.5 0.906
      3.1C 0.04 354 199 0.58 124.0 2 204±27 2 168±7.5 -2 0.135 32 0.43 7.61 1.5 0.407 6 1.4 0.957
      3.2R 0.03 1 002 70 0.07 265.0 1 732±23 1 855±13 7 0.113 44 0.70 4.821 1.7 0.308 2 1.5 0.909
      4.1C 0.02 2 211 683 0.32 755.0 2 158±26 2 162±3.2 0 0.134 89 0.18 7.39 1.4 0.397 5 1.4 0.992
      5.1C 0.01 533 306 0.59 185.0 2 189±26 2 177±6.1 -1 0.136 05 0.35 7.59 1.4 0.404 4 1.4 0.970
      6.1C 0.00 166 77 0.48 55.7 2 121±27 2 123±12 0 0.131 87 0.66 7.08 1.6 0.389 6 1.5 0.914
      7.1C 0.04 407 108 0.27 115.0 1 838±23 1 970±8.9 7 0.120 95 0.50 5.503 1.5 0.330 0 1.4 0.944
      6.2R 0.08 667 76 0.12 189.0 1 834±22 1 888±7.2 3 0.115 54 0.40 5.242 1.5 0.329 0 1.4 0.961
      7.2R 0.01 1 191 61 0.05 349.0 1 891±28 1 846±13 -2 0.112 84 0.73 5.303 1.9 0.340 9 1.7 0.921
      8.1C 0.09 166 74 0.46 56.7 2 158±35 2 184±12 1 0.136 53 0.68 7.49 2.0 0.397 7 1.9 0.940
      9.1C 0.01 4 028 1 543 0.40 1 280.0 2 035±29 2 112±2.3 4 0.131 10 0.13 6.71 1.7 0.371 1 1.7 0.997
      10.1C 0.01 335 242 0.75 120.0 2 249±27 2 181±7.6 -3 0.136 38 0.44 7.85 1.5 0.417 5 1.4 0.956
      11.1C 0.02 359 159 0.46 112.0 1 997±26 2 077±8.1 4 0.128 50 0.46 6.43 1.6 0.363 0 1.5 0.956
      12.1C 0.02 514 366 0.74 178.0 2 181±27 2 165±6.3 -1 0.135 11 0.36 7.50 1.5 0.402 5 1.5 0.971
      13.1C 0.06 268 136 0.52 86.2 2 049±26 2 062±9.6 1 0.127 37 0.54 6.57 1.6 0.374 2 1.5 0.937
      14.1C 0.01 911 926 1.05 329.0 2 261±27 2 185±4.7 -3 0.136 67 0.27 7.92 1.5 0.420 1 1.4 0.982
      15.1C 0.07 369 197 0.55 127.0 2 178±27 2 172±7.7 0 0.135 67 0.44 7.52 1.5 0.402 0 1.5 0.958
      16.1C 0.02 418 203 0.50 126.0 1 942±26 2 157±10 10 0.134 43 0.59 6.51 1.6 0.351 5 1.5 0.933
      17.1C 0.08 249 136 0.56 84.3 2 142±30 2 177±9.5 2 0.136 06 0.55 7.39 1.7 0.394 1 1.7 0.950
      18.1C 0.02 744 374 0.52 253.0 2 153±26 2 171±5.4 1 0.135 54 0.31 7.41 1.4 0.396 5 1.4 0.976
      19.1C 0.12 221 77 0.36 60.8 1 791±23 2 049±12 13 0.126 44 0.68 5.583 1.6 0.320 2 1.5 0.905
      19.2R 0.01 525 31 0.06 159.0 1 945±24 1 901±7.8 -2 0.116 36 0.43 5.649 1.5 0.352 1 1.4 0.956
      20.1C 0.07 200 93 0.48 62.0 1 986±25 2 098±11 5 0.129 97 0.62 6.47 1.6 0.360 8 1.5 0.920
      20.2R 0.08 796 297 0.39 179.0 1 500±21 1 889±7.6 21 0.115 63 0.42 4.175 1.6 0.261 9 1.6 0.966
      21.1C 0.03 215 118 0.57 68.2 2 028±29 2 188±11 7 0.136 86 0.62 6.98 1.8 0.369 8 1.7 0.937
      注:Pb*代表放射性成因铅,对样品N13和N02;C和R分别代表锆石的核部和边部.
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