Zircon U-Pb and Molybdenite Re-Os dating of the Shangfang Tungsten Deposit in Northern Fujian Province: Implications for Regional Mineralization
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摘要: 上房钨矿床是武夷山成矿带新近发现的大型白钨矿矿床，也是福建省发现的钨矿新类型.矿床产于上房似斑状黑云母正长花岗岩体的外接触带上，赋矿围岩主要为古元古代大金山岩组斜长角闪岩和黑云斜长变粒岩，矿体产状与围岩的片理一致，矿石类型为石英细脉型和浸染型，金属矿物主要为白钨矿和辉钼矿，其次为少量磁黄铁矿、黄铁矿和黄铜矿等.野外地质观察和矿化特征研究表明，上房钨矿的矿床类型为接触交代型.采用LA-ICP-MS锆石U-Pb和辉钼矿Re-Os测年技术，对与成矿有关的上房似斑状黑云母正长花岗岩和与白钨矿共生的辉钼矿进行成岩成矿年代测定，获得上房似斑状正长花岗岩体的成岩年龄为158.8±1.6 Ma(1σ)，辉钼矿Re-Os模式年龄为159.40±0.86~149.92±1.39 Ma(n=5)，模式年龄的加权平均值为156.5±4.0 Ma，等时线年龄为158.1±5.4 Ma(2σ).同位素定年结果表明，上房钨矿床与矿区似斑状黑云母正长花岗岩关系密切，二者均形成于晚侏罗世，与华南地区中生代大规模钨多金属矿床的成矿时代一致.传统观点认为，华南地区晚侏罗世(160~150 Ma)钨多金属矿床大规模成矿作用集中于南岭成矿带中东段的湘南、粤北和赣南地区，而本文的研究结果则说明这一区域成矿作用向北东延伸进入到武夷山成矿带的闽西和闽北地区.因此，华南钨多金属矿床的空间分布不是传统认为的近东西向，而是具有北东向或北东东向展布的特点，是滨太平洋构造-岩浆-成矿域的重要组成部分.
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关键词:
- 锆石U-Pb定年 /
- 辉钼矿Re-Os定年 /
- 地质年代学 /
- 白钨矿 /
- 成矿带
Abstract: The newly discovered large-scale Shangfang tungsten deposit represents a new type of tungsten mineralization in Fujian Province, offering new pespectives for exploration of tungsten deposits in the province. The ore bodies are mostly hosted in amphibolite and biotite leptynite of the Paleoproterozoic Dajinshan Formation proximal to the Shangfang syenogranite intrusion and, less significantly, in the contact zone between the intrusion and the metamorphic rocks. Tungsten mineralization consists of quartz-scheelite veins and disseminated scheelite in alteration assemblages, with scheelite and molybdenite as the main ore minerals coexisting with minor pyrrhotite, pyrite, and chalcopyrite. Field relations and petrographic characterization indicate that the Shangfang deposit is typified by skarn mineralization. Zircons from the Shangfang syenogranite intrusion have LA-ICP-MS U-Pb age of 158.8±1.6 Ma (1σ), whereas five molybdenite separates yield model ages ranging from 159.40±0.86 to 149.92±1.39 Ma with a weighted mean of 156.5 ± 4.0 Ma, which is consistent with an isochrone age of 158.1±5.4 Ma (2σ). The geochronological data thus demonstrate that the Shangfang tungsten deposit formed in the Late Jurassic and is genetically related to the syenogranite intrusion in the mine. The data also indicate that the Shangfang deposit resulted from the pervasive Late Mesozoic tunsgten mineralization in South China. It has long been considered that the Late Jurassic tungsten metallogenic belt in South China is restricted in the middle-eastern portion of the Nanling Range covering areas of southern Hunan, northern Guangdong, and southern Jiangxi Province. The discovery of the Shangfang deposit, however, allows this metallogenic belt to extend into western and northern Fujian Province, which is an integral part of the Wuyishan metallogenic belt. As such, the South China polymetallic belt is distributed along a northeast strike, rather than an east-west extension as previously thought, and can be regarded as an important part of the giant Circle-Pacific tectono-magmtic-metallogenic domain.-
Key words:
- Zicron U-Pb dating /
- molybdenite Re-Os dating /
- geochronology /
- scheelite deposit /
- metallogenic belt
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图 1 闽北上房白钨矿大地构造位置图(a)和区域地质简图(b)
1.晚侏罗世南园组火山岩；2.早侏罗世梨山组沉积岩；3.新元古马面山群变质岩；4.古元古代麻源群变质岩；5.晚侏罗世黑云母正长花岗岩；6.加里东期片麻状花岗岩；7.地质界线；8.脆性断裂；9.详查矿区范围；10.矿区位置示意
Fig. 1. Tectonic location (a) and regional geology (b) of the Shangfang tungsten deposit in northern Fujian Province
图 2 闽北上房白钨矿矿区地质简图(据福建省地质调查研究院资料修编)
1.晚侏罗世黑云母正长花岗岩；2.古元古代麻源群变质岩；3.花岗斑岩；4.白钨矿体；5.详查区范围及勘探线编号；6.土壤测量钨异常等值线
Fig. 2. Simplified geological map of the Shangfang tungsten deposit (modified from Fujian Geological Survey, unpublished data)
图 3 上房钨矿床4号勘探线剖面图(据福建省地质调查研究院资料修编)
Fig. 3. No.4 geological cross section of the Shangfang tungsten deposit (modified from Fujian Geological Survey, unpublished data)
图 4 福建上房钨矿黑云母正长花岗岩样品锆石U-Pb谐和图
Fig. 4. Zircon U-Pb concordia diagram of the biotite syenite granite in the Shangfang tungsten deposit
图 5 上房钨矿辉钼矿Re-Os同位素模式年龄加权平均值图(a)及Re-Os同位素等时线图(b)
Fig. 5. Weighted mean of Re-Os model age of molybdenite (a) and Re-Os isotopic isochron (b) of the Shangfang tungsten deposit
图 6 华南晚侏罗世(160~150 Ma)主要钨矿床分布示意图(据毛景文等, 2008, 修改)
Fig. 6. Spatial distribution of the Late Jurassic W deposits in South China (modified from Mao et al., 2008)
表 1 福建上房钨矿似斑状黑云母正长花岗岩LA-ICP-MS锆石U-Pb同位素分析结果
Table 1. LA-ICP-MS zircon U-Pb isotope data of the bioite syenogranite from the Shangfang tungsten deposit
样品号 同位素原子比值 表面年龄(Ma) 232Th/238U ±1σ 207Pb/206Pb ±1σ 207Pb/235U ±1σ 206Pb/238U ±1σ 208Pb/232Th ±1σ 207Pb/235U ±1σ 206Pb/238U ±1σ 208Pb/232Th ±1σ SFZK410-1 0.746 3 0.01 0.050 0 0.007 3 0.171 9 0.026 4 0.025 0 0.001 3 0.008 1 0.001 2 161 23 159 8 162 24 SFZK410-2 0.362 3 0.03 0.049 8 0.006 0 0.239 7 0.030 6 0.034 9 0.001 5 0.013 0 0.001 6 218 25 221 9 261 33 SFZK410-3 0.847 5 0.01 0.055 7 0.006 0 0.190 6 0.021 7 0.025 1 0.001 0 0.008 4 0.000 9 177 18 160 6 169 18 SFZK410-4 0.561 8 0.02 0.050 2 0.004 5 0.163 9 0.015 4 0.023 8 0.000 7 0.008 3 0.000 7 154 13 152 4 166 14 SFZK410-5 0.917 4 0.01 0.050 0 0.004 2 0.166 3 0.014 4 0.024 6 0.000 6 0.008 1 0.000 5 156 13 157 4 164 10 SFZK410-6 0.657 9 0.02 0.052 1 0.002 7 0.177 5 0.009 4 0.024 9 0.000 4 0.008 5 0.000 4 166 8 158 2 171 7 SFZK410-7 0.666 7 0.01 0.047 7 0.002 5 0.161 5 0.008 8 0.024 9 0.000 3 0.008 5 0.000 3 152 8 158 2 172 5 SFZK410-8 1.111 1 0.01 0.050 2 0.001 7 0.170 4 0.006 0 0.024 8 0.000 2 0.007 8 0.000 2 160 5 158 1 157 3 SFZK410-9 0.917 4 0.01 0.048 3 0.002 8 0.163 7 0.009 6 0.024 7 0.000 3 0.008 2 0.000 3 154 8 158 2 165 5 SFZK410-10 0.91 74 0.01 0.051 8 0.002 5 0.173 6 0.008 8 0.024 6 0.000 5 0.007 7 0.000 2 163 8 156 3 155 4 SFZK410-11 0.492 6 0.02 0.054 0 0.002 0 0.184 4 0.007 2 0.024 6 0.000 3 0.008 1 0.000 3 172 6 157 2 164 6 SFZK410-12 0.341 3 0.03 0.050 1 0.001 4 0.170 1 0.005 2 0.024 6 0.000 3 0.007 5 0.000 2 159 5 157 2 151 3 SFZK410-13 0.645 2 0.02 0.052 2 0.001 5 0.176 1 0.005 2 0.024 4 0.000 2 0.008 0 0.000 2 165 5 155 1 162 4 SFZK410-14 0.653 6 0.02 0.052 3 0.002 5 0.178 1 0.009 0 0.024 6 0.000 3 0.008 2 0.000 2 166 8 157 2 164 5 SFZK410-15 0.578 0 0.02 0.050 8 0.002 2 0.175 9 0.008 3 0.025 1 0.000 2 0.007 9 0.000 1 164 7 160 1 159 1 SFZK410-16 0.689 7 0.01 0.050 0 0.001 6 0.178 1 0.006 5 0.025 8 0.000 2 0.008 2 0.000 1 166 6 164 1 164 1 SFZK410-17 0.497 5 0.02 0.049 4 0.001 5 0.174 2 0.005 9 0.025 6 0.000 3 0.008 2 0.000 2 163 5 163 2 164 4 SFZK410-18 1.041 7 0.01 0.055 8 0.004 0 0.189 3 0.014 0 0.025 2 0.000 4 0.008 0 0.000 3 176 12 160 3 161 5 SFZK410-19 0.970 9 0.01 0.112 6 0.001 8 5.336 5 0.096 3 0.342 8 0.002 8 0.095 8 0.001 7 1875 15 1900 13 1849 31 
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表 2 福建上房钨矿床中辉钼矿Re-Os同位素分析结果
Table 2. Re-Os isotope data of molybdenite from the Shangfang tungsten deposit
编号 样重(g) Re(10-6) 187Re(10-6) 187Os(10-9) 模式年龄(Ma) 测定值 2σ 测定值 2σ 测定值 2σ 年龄值 2σ SFMo-01 0.037 2.90 0.023 1.82 0.015 4.65 0.029 153.02 1.49 SFMo-02 0.042 6.32 0.044 3.97 0.028 10.37 0.057 156.45 1.32 SFMo-03 0.039 1.15 0.011 0.73 0.007 1.93 0.012 159.40 1.71 SFMo-04 0.049 0.60 0.010 0.38 0.007 0.95 0.007 149.92 2.79 SFMo-05 0.040 7.15 0.050 4.49 0.031 11.92 0.066 159.00 1.35
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表 3 华南地区若干钨矿床的成矿年龄
Table 3. Ore-forming ages of representative W-Sn deposits in South China
产地 矿床名称 成因类型 测试矿物 测试方法 年龄值(Ma) 数据来源 湘南 香花铺白钨矿 矽卡岩型 白云母 Ar-Ar 161.3±1.1 Yuan et al.2007 白云母 Ar-Ar 158.7±1.2 白云母 Ar-Ar 154.4±1.1 新田岭白钨矿 矽卡岩型 羟铁云母 Ar-Ar 157.1±0.2 毛景文等，2004b 锆石 U-Pb 160.0±2.0 付建明等，2004 黄沙坪白钨矿 矽卡岩型 辉钼矿 Re-Os 154.8±1.9 姚军明等，2007 锆石 U-Pb 161.6±1.1 柿竹园白钨矿 矽卡岩-云英岩型 白云母 Ar-Ar 153.4±0.2 毛景文等，2004b 辉钼矿 Re-Os 151.0±3.5 李红艳等，1996 锆石 U-Pb 161.8±1.0 Li et al., 2004 瑶岗仙白钨矿 矽卡岩型 辉钼矿 Re-Os 154.9±2.6 Peng et al., 2006 金云母 Ar-Ar 153.0±1.1 Peng et al., 2006 白云母 Ar-Ar 155.1±1.1 Peng et al., 2006 锆石 U-Pb 157.0+2.0 李顺庭等，2011 赣南 淘锡坑黑钨矿 石英脉型 辉钼矿 Re-Os 154.4+3.8 陈郑辉等，2006 锆石 U-Pb 158.7±3.9 郭春丽等，2007 柯树岭钨锡矿 石英脉型 白云母 Ar-Ar 158.8±1.2 刘善宝等，2008 锆石 U-Pb 161.8±1.0 张文兰等，2009 漂塘黑钨矿 石英脉型 白云母 Ar-Ar 152.1±1.9 张文兰等，2009 茅坪钨锡矿 石英脉型 白云母 Ar-Ar 158.9±1.4 刘善宝等，2008 辉钼矿 Re-Os 156.8±3.9 曾载淋等，2009 大吉山黑钨矿 石英脉型 锆石 U-Pb 151.7±1.6 张文兰等，2006 包裹体 Rb-Sr 150.0±？ 李华芹等，1993 摇篮寨黑钨矿 石英脉型 锆石 U-Pb 156.9±1.7 丰成友等，2011 辉钼矿 Re-Os 155.8±2.8 丰成友等，2011 牛岭钨锡矿 石英脉型 辉钼矿 Re-Os 154.9±4.1 丰成友等，2011 锆石 U-Pb 151.4±3.0 丰成友等，2011 洪水寨钨矿 云英岩型 锆石 U-Pb 155.8±1.2 丰成友等，2011 辉钼矿 Re-Os 156.3±1.3 丰成友等，2011 木梓园钨锡矿 石英脉型 锆石 U-Pb 153.3±1.9 张文兰等，2009 白云母 Ar-Ar 151.1±8.5 张文兰等，2009 浒坑黑钨矿 石英脉型 锆石 U-Pb 151.6±2.6 刘珺等，2008 辉钼矿 Re-Os 150.2±2.2 刘珺等，2008 西华山黑钨矿 石英脉型 钾长石 K-Ar 148.1±1.0 穆治国等，1988 樟斗黑钨矿 石英脉型 辉钼矿 Re-Os 154.6±9.7 丰成友等，2007 大坳钨锡矿 云英岩及石英脉型 辉钼矿 Re-Os 151.3±2.4 付建明等，2007 锆石 U-Pb 156.0±2.0 粤北 师姑山钨铋矿 石英脉型 辉钼矿 Re-Os 154.2±2.7 付建明等，2007 石人嶂黑钨矿 石英脉型 辉钼矿 Re-Os 159.1±2.2 付建明等，2007 红岭钨矿 石英脉型 辉钼矿 Re-Os 159.1±1.5 王小飞等，2010 梅子窝钨矿 石英脉型 辉钼矿 Re-Os 157.7±1.4 王小飞等，2010 瑶岭钨矿 石英脉 辉钼矿 Re-Os 159.2±2.3 王小飞等，2010 闽西 行洛坑钨矿 斑岩型 辉钼矿 Re-Os 156.3±4.8 张家菁等，2008 闽北 上房白钨矿 接触交代型 锆石 U-Pb 158.8±1.4 本文 辉钼矿 Re-Os 158.1±5.4 本文 注：由于篇幅限制，本表仅列出部分测试数据，主要说明燕山早期(160~150 Ma)岩浆活动与钨多金属成矿事件的关系.
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