龙首山中段芨岭花岗岩体Sr-Nd-Pb同位素特征及意义

赵亚云; 张树明; 汤琳; 尧宏福; 杨春四

doi:10.3799/dqkx.2016.084

龙首山中段芨岭花岗岩体Sr-Nd-Pb同位素特征及意义

doi: 10.3799/dqkx.2016.084

赵亚云^1,,
张树明^1,2, ,,
汤琳¹,
尧宏福²,
杨春四¹

1.
东华理工大学省部共建核资源与环境国家重点实验室培育基地，江西南昌 330013
2.
东华理工大学放射性地质与勘探技术国防重点学科实验室，江西南昌 330013

基金项目:

国家自然科学基金项目 41172079

详细信息

作者简介:
赵亚云(1988-)，男，硕士研究生，主要从事矿物学、岩石学和矿床学方面的研究.E-mail: zyr2009163@126.com

通讯作者:
张树明，E-mail: zsmfjxy@hotmail.com

中图分类号: P597
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出版历程
- 收稿日期: 2015-12-25
- 刊出日期: 2016-06-15

Sr-Nd-Pb Isotopic Characteristics and Its Geological Significance of the Jiling Grantic Pluton in the Middle Longshou Mountains

1.
State Key Laboratory Breeding Base of Nuclear Resources and Environment, East China University of Technology, Nanchang 330013, China
2.
Key Laboratory of Radioactive Geology and Exploration Technology Fundamental Science for National Defense, East China University of Technology, Nanchang 330013, China

摘要

摘要: 龙首山中段芨岭早古生代花岗岩体与碱交代型铀矿化关系密切，是龙首山花岗质岩浆活动带重要组成部分，但人们对芨岭岩体的成因、岩浆源区性质以及与铀成矿之间的关系还了解得不多.花岗岩体Sr-Nd-Pb同位素研究结果表明，不同期次花岗岩(早古生代第一次灰白色二长花岗岩、第二次肉红色二长花岗岩、晚古生代肉红色细粒(钾长)花岗岩)的(⁸⁷Sr/⁸⁶Sr)_i值均介于大陆地壳范围内(0.706~0.718)，同时有(⁸⁷Sr/⁸⁶Sr)_i均值先升后降(0.707 12→0.710 00→0.707 89)、ε_Nd(t)均值先降后增(-7.00→-8.09→-4.65) 的特征.不同期次花岗岩体t_DM2均值分别为1 735.50 Ma、1 814.66 Ma、1 737.50 Ma，接近残留地壳年龄，表明岩体的主要物质来源为古元古代龙首山群地层，并有部分幔源组分或年轻地壳物质的加入.岩体的Pb同位素比值较高，灰白色二长花岗岩的²⁰⁶Pb/²⁰⁴Pb=18.328~19.240，²⁰⁷Pb/²⁰⁴Pb=15.549~15.619，²⁰⁸Pb/²⁰⁴Pb=38.390~39.075，μ=9.37~9.43(平均为9.40)；肉红色二长花岗岩的²⁰⁶Pb/²⁰⁴Pb=30.209~43.529，²⁰⁷Pb/²⁰⁴Pb=16.097~25.076，²⁰⁸Pb/²⁰⁴Pb=39.107~39.420，μ=18.47~30.24(平均为24.355)；肉红色细粒(钾长)花岗岩的²⁰⁶Pb/²⁰⁴Pb=19.071~19.767，²⁰⁷Pb/²⁰⁴Pb=15.577~25.438，²⁰⁸Pb/²⁰⁴Pb=38.682~42.593，μ=9.36~9.49(平均为9.41)，显示为高放射性成因铅同位素特征，表明岩体的铅为混合来源但以壳源为主.Sr-Nd-Pb同位素对比研究表明，钠交代岩(矿石)的(⁸⁷Sr/⁸⁶Sr)_i、ε_Nd(t)与早古生代第二次侵入的肉红色斑状二长花岗岩极为相似，在(⁸⁷Sr/⁸⁶Sr)_i-ε_Nd(t)图解投影点也吻合，表明研究区碱交代型铀成矿主要与早古生代第二次侵入有关.其他期次花岗岩体同样具有高铀背景值，表明其可能也提供了一定的铀源.
- 早古生代 /
- 芨岭岩体 /
- Sr-Nd-Pb同位素 /
- 岩浆源区 /
- 铀成矿 /
- 龙首山 /
- 地球化学
Abstract: The Early Paleozoic granitic pluton has a closely genetic relationship with the Alkali metasomatism type uranium mineralization in the middle Longshou Moutains area, which is an important activity zone of Longshoushan granitic magma. However, people do not know more about the cause of Jiling rock mass, properties of magma source area and the relationship between Jiling rock mass and uranium mineralization. The Sr-Nd-Pb isotopic composition characteristics of granitic pluton show that the initial Sr isotope ratios (⁸⁷Sr/⁸⁶Sr)_i of granite in different periods (with first intrusion of gray monzonitic granites in the Early Paleozoic, the pink monzonitic granites of the second intrusion, and pink fine-grained (potassium) granites of the intrusion in Late Paleozoic) fall in the range of that of the continental crust (from 0.706 to 0.718); at the same time, the average initial Sr isotope ratios (⁸⁷Sr/⁸⁶Sr)_i has a trend of falling after rising (0.707 12→0.710 00→0.707 89), and the average of ε_Nd(t) shows the trend of rising after falling (-7.00→-8.09→-4.65). t_DM2 average of granites in different periods is 1 735.50 Ma, 1 814.66 Ma and 1 737.50 Ma respectively, which is very close to the age of residual crust, indicating that the main material source of the granitic pluton should be the group strata of paleoproterozoic Longshou mountains, with the addition of mantle or young crustal materials. Its Pb Isotope ratios are high: ²⁰⁶Pb/²⁰⁴Pb range from 18.328 to 19.240, ²⁰⁷Pb/²⁰⁴Pb range from 15.549 to 15.619, ²⁰⁸Pb/²⁰⁴Pb range from 38.390 to 39.075, μ values range from 9.37 to 9.43, with an average of 9.40, ²⁰⁶Pb/²⁰⁴Pb range from 30.209 to 43.529, ²⁰⁷Pb/²⁰⁴Pb range from 16.097 to 25.076, ²⁰⁸Pb/²⁰⁴Pb range from 39.107 to 39.42, μ values range from 18.47 to 30.24, with an average of 9.40;²⁰⁶Pb/²⁰⁴Pb range from 19.071 to 19.767, ²⁰⁷Pb/²⁰⁴Pb range from 15.577 to 25.438, ²⁰⁸Pb/²⁰⁴Pb range from 38.682 to 42.593, μ values range from 9.36 to 9.49, with an average of 9.41. All samples show high radioactive Pb isotopic characteristics with a mixed source, but the crust is the main source. The comparison of Sr-Nd-Pb Isotope shows that the initial Sr isotope ratios (⁸⁷Sr/⁸⁶Sr)_i and ε_Nd(t) of sodium metasomatic rock (ore) are very similar to those of pink monzonitic granites of the second intrusion in the Early Paleozoic, and the subpoint of (⁸⁷Sr/⁸⁶Sr)_i-ε_Nd(t) diagram is also consistent, which indicates that alkali metasomatism type uranium mineralization of the study area is mainly related to the second invasion in Early Paleozoic. The high uranium background values of granitic pluton in other periods show that it may also provide a source of uranium.
- Early Paleozoic /
- Jiling pluton /
- Sr-Nd-Pb isotope /
- magma sources /
- Uranium metallogenetism /
- Longshou Moutains /
- geochemistry

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图 1 龙首山中段大地构造位置(a)及芨岭岩体地质简图(b)

1.新近系；2.侏罗系；3.寒武系中统香山群；4.震旦系孩母山群上亚群；5.震旦系孩母山群下亚群；6.墩子沟群上亚群；7.墩子沟群下亚群；8.龙首山群踏马子沟组；9.龙首山群麒麟沟组；10.早古生代第三次细粒花岗岩；11.早古生代第一次中粗粒二长花岗岩；12.早古生代一次碱性杂岩；13.早古生代一次花岗闪长岩；14.早古生代花岗闪长岩；15.早古生代混合花岗岩；16.早古生代二次斑状花岗岩；17.早古生代闪长岩；18.早古生代基性－超基性岩；19.辉绿岩；20.酸性岩脉；21.中性岩脉；22.铀矿床；23.采样位置；图a据傅成铭等(2012)

Fig. 1. Tectonic position (a) and schenmatic geological sketch (b) of Jiling pluton in the middle Longshou Moutains

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图 2 龙首山中段芨岭花岗岩体手标本及镜下显微照片

a.微斜长石格子双晶及微弱绢云母化；b.角闪石内部包含乳滴状石英；c.似斑状结构；d.细粒花岗结构及微斜长石格子双晶；Bt.黑云母；Pl.斜长石；Kfs.钾长石；Q.石英；Mc.微斜长石；Ser.绢云母化；Hbl.角闪石

Fig. 2. Photographs of the granitic pluton of Jiling in the middle Longshou Moutains

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图 3 龙首山中段芨岭花岗岩体(⁸⁷Sr/⁸⁶Sr)_i-ε_Nd(t)关系

DM.亏损地幔，据郭志军(2014)

Fig. 3. (⁸⁷Sr/⁸⁶Sr)_i-ε_Nd(t) relations of Jiling granitic pluton in the middle Longshou Moutains

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图 4 龙首山中段芨岭花岗岩体ε_Nd(t)-t关系

古-中元古代地壳和大古宙地壳的界线隋振民和徐学纯(2010)；底图据郭志军等(2014)

Fig. 4. ε_Nd(t)-t relations of Jiling granitic pluton in the middle Longshou Moutains

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图 5 龙首山中段芨岭花岗岩体(⁸⁷Sr/⁸⁶Sr)_i-t关系

M.幔源型花岗岩类源区；MC.幔壳混源型或同熔型花岗岩类源区；C.壳源型或改造型花岗岩类源区：(Ⅰ).下部大陆壳；(Ⅱ).上部大陆壳；红色虚线为玄武岩源区数值范围(0.702~0.706)；底图据吴利仁(1985)

Fig. 5. (⁸⁷Sr/⁸⁶Sr)_i-t relations of Jiling granitic pluton in the middle Longshou Moutains

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图 6 龙首山中段芨岭花岗岩体Pb同位素组成

DMM.亏损地幔端元；EM(Ⅰ、Ⅱ).富集地幔端元，据Zindler and Hart(1986); Geochron.零等时线；NHRL.北半球参考线据Hart(1984)；中国大陆地幔、下地壳和上地壳数据据李龙等(2001)；底图据张承帅等(2012)

Fig. 6. Pb isotopic diagrams of Jiling granitic pluton in the middle Longshou Moutains

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图 7 龙首山中段芨岭花岗岩体Pb同位素构造模式

A.地幔；B.造山带；C.上地壳；D.下地壳；底图据Zarnnan and Doe(1981)

Fig. 7. Pb isotopic tectonic model diagrams of Jiling granitic pluton in the middle Longshou Moutains

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表 1 Nd-Sr-Pb同位素测试样品采集位置与岩性

Table 1. Position and lithology for Nd-Sr-Pb isotope test samples

序号	样品号	北纬	东经	岩(矿)石名称
1	LSS12-01	38°33′16.37″	101°47′10.53″	斑状黑云母花岗闪长岩
2	LSS12-02	38°33′56.33″	101°48′0.87″	灰白色中细粒二长花岗岩
3	LSS12-03	38°33′57.15″	101°47′59.40″	灰白色中粗粒二长花岗岩
4	LSS12-04	38°33′59.19″	101°47′56.78″	肉红色中粗粒似斑状二长花岗岩
5	LSS12-05	38°33′2.12″	101°47′56.84″	肉红色细粒花岗岩
6	LSS12-12	38°33′59.87″	101°47′53.29″	肉红色中粗粒似斑状二长花岗岩
7	LSS12-15	38°33′59.87″	101°47′53.29″	钠交代岩(矿石)
8	LSS12-16	38°33′59.87″	101°47′53.29″	钠交代岩(矿石)
9	LSS12-18	38°38′6.5″	101°39′47.3″	钠交代岩(矿石)
10	LSS12-19	38°38′6.5″	101°39′47.3″	钠交代岩(矿石)
11	LSS12-20	38°31′28.45″	101°54′9.43″	肉红色中粒二长花岗岩
12	LSS13-26	38°34′0.84″	101°47′53.88″	肉红色细粒钾长花岗岩
13	LSS13-33	38°34′0.48″	101°47′56.4″	肉红色细粒花岗岩
14	LSS13-36	38°34′0.84″	101°47′58.92″	肉红色细粒钾长花岗岩
15	LSS13-41	38°34′0.89″	101°47′58.30″	肉红色细粒钾长花岗岩

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表 2 龙首山中段芨岭岩体花岗岩类Sr、Nd同位素组成

Table 2. Sr、Nd isotopic compositions of granitoid of Jiling pluton in the middle Longshou Moutains

样品号	年龄 (Ma)	Rb (10^-6)	Sr (10^-6)	⁸⁷Rb/⁸⁶Sr	⁸⁷Sr/⁸⁶Sr (2σ)	(⁸⁷Sr/⁸⁶Sr)_i	Sm (10^-6)	Nd (10^-6)	¹⁴⁷Sm/¹⁴⁴Nd	¹⁴³Nd/¹⁴⁴Nd (2σ)	(¹⁴³Nd/¹⁴⁴Nd)_i	ε_Nd(t)	f_Sm/Nd	t_DM2 (Ma)	u(%)
LSS12-02	425.2	45.90	686.0	0.193 6	0.707 577±0.000 015	0.706 40	16.00	88.0	0.109 9	0.512 223±0.000 008	0.511 92	-3.38	-0.44	144 1	12.78
LSS12-03	428.6	111.00	458.0	0.701 4	0.712 109±0.000 011	0.707 83	7.00	52.2	0.080 7	0.511 769±0.000 008	0.511 54	-10.62	-0.59	203 0	-88.62
LSS12-01	416.7	33.90	599.0	0.163 8	0.707 242±0.000 013	0.706 27	14.80	75.5	0.118 5	0.512 211±0.000 009	0.511 89	-4.16	-0.40	149 8	20.66
LSS12-04	416.0	13.40	211.0	0.183 8	0.709 159±0.000 009	0.708 07	8.09	52.8	0.092 6	0.511 970±0.000 006	0.511 72	-7.50	-0.53	176 8	-21.94
LSS12-12	416.0	6.24	238.0	0.075 9	0.709 780±0.000 007	0.709 33	5.81	40.6	0.086 5	0.511 924±0.000 006	0.511 69	-8.13	-0.56	181 5	-35.74
LSS12-20	416.6	5.96	191.0	0.090 3	0.713 406±0.000 013	0.712 87	17.10	83.1	0.124 4	0.511 998±0.000 007	0.511 66	-8.64	-0.37	186 1	-116.39
LSS12-05	401.3	207.00	32.9	18.319 6	0.805 374±0.000 023	0.700 68	11.90	58.3	0.123 4	0.511 961±0.000 009	0.511 64	-9.45	-0.37	191 4	-2 128.81
LSS13-26	401.3	48.60	123.0	1.143 5	0.713 135±0.000 009	0.706 60	8.37	64.7	0.078 2	0.512 167±0.000 008	0.511 96	-3.13	-0.60	140 0	-108.90
LSS13-33	401.3	0.90	42.0	0.062 2	0.709 872±0.000 009	0.709 52	7.50	77.3	0.058 6	0.512 014±0.000 008	0.511 86	-5.10	-0.70	156 1	-36.78
LSS13-36	401.3	2.81	95.4	0.085 2	0.708 035±0.000 010	0.707 55	16.30	114.0	0.086 4	0.512 302±0.000 009	0.512 08	-0.90	-0.56	122 0	3.84
LSS13-41	401.3	93.40	119.0	2.271 4	0.718 424±0.000 010	0.705 44	15.80	117.0	0.081 6	0.512 347±0.000 016	0.512 13	0.21	-0.58	112 9	-225.70
LSS12-15	398.0	3.33	379.0	0.025 4	0.709 924±0.000 011	0.709 78	6.34	38.1	0.100 6	0.511 995±0.000 009	0.511 73	-7.66	-0.49	176 6	-37.70
LSS12-16	398.0	6.23	426.0	0.042 3	0.709 854±0.000 011	0.709 61	4.98	28.8	0.104 5	0.511 975±0.000 006	0.511 70	-8.25	-0.47	181 4	-36.16
LSS12-18	398.0	2.26	233.0	0.028 1	0.710 503±0.000 012	0.710 34	6.62	35.9	0.111 5	0.511 982±0.000 006	0.511 69	-8.48	-0.43	183 1	-50.49
LSS12-19	398.0	4.98	710.0	0.020 3	0.710 552±0.000 020	0.710 44	40.00	205.0	0.123 8	0.511 956±0.000 007	0.511 63	-9.61	-0.37	192 4	-51.57
注：计算所需的参数：λ(Sr)=1.39×10^-11年^-1，λ(Nd)=6.54×10^-12年^-1，⁸⁷Sr/⁸⁶Sr和¹⁴³Nd/¹⁴⁴Nd所示的2σ误差为小数点后的最后位数，为减少¹⁴⁷Sm/¹⁴⁴Nd变化对Nd模式年龄计算产生的影响，表中所列t_DM2年龄统一采用二阶段模式计算，计算公式如下：t_DM2=(1/λ_Sm)ln(1+A)，A={(¹⁴³Nd/¹⁴⁴Nd)_m-(¹⁴³Nd/¹⁴⁴Nd)_DM-[(¹⁴⁷Sm/¹⁴⁴Nd)_m-(¹⁴⁷Sm/¹⁴⁴Nd)_c](e^λt-1)}/[(¹⁴⁷Sm/¹⁴⁴Nd)_c-(¹⁴⁷Sm/¹⁴⁴Nd)_DM]，式中：下角标m代表样品现今测定值，下角标DM代表亏损地幔值，(¹⁴⁷Sm/¹⁴⁴Nd)_DM=0.213 6.(¹⁴³Nd/¹⁴⁴Nd)_DM=0.513 151(Miller and O’Nions, 1985)，下角标CHUR代表球粒陨石值，(¹⁴⁷Sm/¹⁴⁴Nd)_CHUR=0.196 0；(¹⁴³Nd/¹⁴⁴Nd)_CHUR=0.512 630(Bouvier et al., 2008；刘亮等，2013)，u.花岗岩中幔源成分含量；下角标c代表大陆壳平均值，(¹⁴⁷Sm/¹⁴⁴Nd)_c=0.118(Jahn and Condie, 1995).

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表 3 龙首山中段芨岭岩体花岗岩类Pb同位素组成

Table 3. Pb isotopic compositions of granitoid of Jiling pluton in the middle Longshou Moutains

样品号	年龄 (Ma)	Th (10^-6)	U (10^-6)	Pb (10^-6)	²⁰⁸Pb/²⁰⁴Pb (2σ)	²⁰⁷Pb/²⁰⁴Pb (2σ)	²⁰⁶Pb/²⁰⁴Pb (2σ)	(²⁰⁸Pb/²⁰⁴Pb)_i	(²⁰⁷Pb/²⁰⁴Pb)_i	(²⁰⁶Pb/²⁰⁴Pb)_i	²⁰⁶Pb/²⁰⁷Pb	μ	ω	Th/U
LSS12-02	425.2	21.50	7.80	23.0	39.075±0.006	15.619±0.002	19.240±0.003	37.585 8	15.523 8	17.519 9	1.231 8	9.43	34.93	2.76
LSS12-03	428.6	21.50	3.49	28.5	38.390±0.003	15.549±0.001	18.328±0.001	37.205 5	15.515 1	17.715 7	1.178 7	9.37	36.29	6.16
LSS12-01	416.7	5.59	1.99	15.6	38.400±0.006	15.571±0.002	18.359±0.002	37.852 7	15.536 8	17.738 9	1.179 1	9.41	36.37	2.81
LSS12-04	416.0	47.90	44.30	47.5	39.420±0.004	16.977±0.002	43.529±0.004	37.303 6	16.633 6	37.300 1	2.564 0	30.24	32.93	1.08
LSS12-12	416.0	36.40	37.80	48.9	39.107±0.002	16.097±0.001	30.209±0.002	37.779 8	15.855 6	25.823 7	1.876 7	18.47	31.89	0.96
LSS12-20	416.6	59.10	975.00	192.0	39.375±0.007	25.076±0.004	191.806±0.030	37.725 9	20.302 2	105.226 3	7.649 0	161.24	32.78	0.06
LSS12-05	401.3	42.60	11.30	54.1	38.768±0.003	15.577±0.001	19.071±0.001	37.593 0	15.522 7	18.079 9	1.224 3	9.36	34.24	3.77
LSS13-26	401.3	27.70	9.47	30.3	39.062±0.004	15.587±0.001	19.302±0.002	37.688 0	15.505 2	17.808 3	1.238 3	9.37	34.30	2.93
LSS13-33	401.3	68.00	70.30	74.2	42.593±0.009	25.438±0.005	201.335±0.042	37.624 4	24.543 5	185.001 6	7.914 7	169.66	43.44	0.97
LSS13-36	401.3	43.50	27.60	78.1	38.682±0.003	15.637±0.001	19.543±0.002	37.845 9	15.544 6	17.856 1	1.249 8	9.45	32.30	1.58
LSS13-41	401.3	52.30	19.80	48.6	39.308±0.006	15.664±0.002	19.767±0.003	37.673 6	15.556 3	17.799 5	1.261 9	9.49	33.72	2.64
LSS12-15	398.0	69.50	232.00	103.0	40.836±0.004	24.091±0.002	167.987±0.016	37.697 3	22.269 5	134.676 4	6.973 0	140.20	37.62	0.30
LSS12-16	398.0	39.20	108.00	73.7	40.610±0.006	26.197±0.004	217.374±0.032	37.593 6	24.752 2	190.952 8	8.297 7	183.83	36.87	0.36
LSS12-18	398.0	88.80	1965.00	79.9	54.702±0.010	24.371±0.005	214.394±0.037	48.193 9	-0.665 4	-243.461 4	8.797 1	181.20	83.54	0.05
LSS12-19	398.0	＞5 000	＞5 000	397.0	259.995±0.029	65.515±0.007	942.629±0.099	-57.868 3	10.255 4	-67.937 0	14.388 0	824.61	763.38	-
注：计算所需的参数λ(²³⁸U)=1.551 25×10^-10年^-1，λ(²³⁵U)=9.848 5×10^-10年^-1，λ(²³²Th)=4.947 5×10^-11年^-1，μ为现代测定的N(²³⁸U)/N(²⁰⁴Pb)；ω为现代测定的N(²³²Th)/N(²⁰⁴Pb)(周振华等，2011)；(²⁰⁶Pb/²⁰⁴Pb)_i=(²⁰⁶Pb/²⁰⁴Pb)_实测-μ(e^λt-1)，(²⁰⁷Pb/²⁰⁴Pb)_i=(²⁰⁷Pb/²⁰⁴Pb)_实测-μ/137.88(e^λt-1)，(²⁰⁸Pb/²⁰⁴Pb)_i=(²⁰⁸Pb/²⁰⁴Pb)_实测-ω(e^λt-1)；t.侵入岩结晶年龄或成矿年龄.

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