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    辽东连山关地区新太古代花岗杂岩SHRIMP U-Pb年龄、Hf同位素组成及地质意义

    杨凤超 孙景贵 宋运红 张朋 毕中伟

    杨凤超, 孙景贵, 宋运红, 张朋, 毕中伟, 2016. 辽东连山关地区新太古代花岗杂岩SHRIMP U-Pb年龄、Hf同位素组成及地质意义. 地球科学, 41(12): 2008-2018. doi: 10.3799/dqkx.2016.140
    引用本文: 杨凤超, 孙景贵, 宋运红, 张朋, 毕中伟, 2016. 辽东连山关地区新太古代花岗杂岩SHRIMP U-Pb年龄、Hf同位素组成及地质意义. 地球科学, 41(12): 2008-2018. doi: 10.3799/dqkx.2016.140
    Yang Fengchao, Sun Jinggui, Song Yunhong, Zhang Peng, Bi Zhongwei, 2016. SHRIMP U-Pb Age, Hf Isotope Composition and Geochemical Characteristics of Neoarchean Granitic Complex in Liaodong Lianshanguan Area, NE China. Earth Science, 41(12): 2008-2018. doi: 10.3799/dqkx.2016.140
    Citation: Yang Fengchao, Sun Jinggui, Song Yunhong, Zhang Peng, Bi Zhongwei, 2016. SHRIMP U-Pb Age, Hf Isotope Composition and Geochemical Characteristics of Neoarchean Granitic Complex in Liaodong Lianshanguan Area, NE China. Earth Science, 41(12): 2008-2018. doi: 10.3799/dqkx.2016.140

    辽东连山关地区新太古代花岗杂岩SHRIMP U-Pb年龄、Hf同位素组成及地质意义

    doi: 10.3799/dqkx.2016.140
    基金项目: 

    中国地质调查局地质资源大调查项目 12120113058800

    国家自然科学基金青年基金项目 41501093

    详细信息
      作者简介:

      杨凤超(1982-),男,博士研究生,主要从事矿产地质调查及研究工作.E-mail: yangfc123@163.com

    • 中图分类号: P588.121;P597.3

    SHRIMP U-Pb Age, Hf Isotope Composition and Geochemical Characteristics of Neoarchean Granitic Complex in Liaodong Lianshanguan Area, NE China

    • 摘要: 辽东本溪连山关花岗杂岩岩体的精细年代学和地球化学的研究匮乏,区域上辽东地区新太古代岩浆活动较少,研究也相对较弱.辽东本溪连山关地区处于铀矿集中区,是内生铀矿床的有利成矿地区.区内铀矿主要赋存于连山关花岗杂岩体与辽河群浪子山组或鞍山群的接触带附近,表明了岩体与铀矿化关系密切.连山关地区浅肉红色正长花岗岩SHRIMP U-Pb年龄为2 512±14 Ma,灰白色条痕状二长花岗岩SHRIMP U-Pb年龄为2 510±15 Ma,花岗杂岩侵位时代为新太古代.正长花岗岩SiO2含量为69.28%~72.70%,K2O含量为6.24%~7.12%,Na2O含量为2.77%~3.09%,Al2O3含量为13.68%~15.92%;二长花岗岩SiO2含量为65.53%~71.01%,K2O含量为2.95%~3.90%,Na2O含量为3.57%~4.23%,Al2O3含量为14.13%~14.90%;连山关花岗杂岩含白云母,A/CNK为1.09~1.16(平均1.12),刚玉(C)为1.37~2.28,P2O5和SiO2无负相关关系,表现为高钾的S型花岗岩.稀土总量较高,轻重稀土元素之间强烈分馏,从正铕异常到负铕异常(δEu=3.55~0.36),亏损Nb、Ta、P、Ti等高场强元素,富集Rb、Th、K等大离子亲石元素.锆石εHf(t)值为-15.19~-0.47,对应的单阶段Hf模式年龄TDM为2 826~3 400 Ma,两阶段Hf模式年龄TDMC为2 931~3 650 Ma.辽东连山关花岗杂岩可能是在高温中压条件下由中太古代和古太古代地壳物质(以变质泥岩和杂砂岩为主)发生深熔作用形成的,可能发生在后碰撞环境,指示华北克拉通各微陆块拼贴完成.

       

    • 图  1  中国东北构造地质简图(a)和辽东连山关地区花岗杂岩地质简图(b)

      Fig.  1.  Geological sketch of eastern China, showing major tectonic units (a) and geological sketch of granitic complex in the Liaodong Lianshanguan area (b)

      图  2  辽东连山关地区肉红色正长花岗岩(a、b、c)和灰白色条痕状二长花岗岩(d、e、f)照片

      a.岩石标本照片;b.显微镜下正交偏光照片(25×);c.显微镜下单偏光照片(25×);d.岩石标本照片;e.显微镜下正交偏光照片(25×);f.显微镜下单偏光照片(25×)

      Fig.  2.  Images of flesh red syenogranite (a, b, c) and white streaks shape monzonitic granite (d, e, f) from Lianshanguan area in Liaodong Peninsula

      图  3  辽东连山关地区正长花岗岩(TW6-1) 和条痕状二长花岗岩(TW6-2) 的锆石阴极发光(CL)图像

      Fig.  3.  Zircon CL image of syenogranite (TW6-1) and streaks shape monzonitic granite from Lianshanguan area in Liaodong Peninsula

      图  4  辽东连山关地区花岗杂岩SHRIMP U-Pb年龄

      Fig.  4.  SHRIMP zircon U-Pb concordia diagram and average age of the granitic complex from Lianshanguan area in Liaodong Peninsula

      图  5  辽东连山关地区花岗杂岩的SiO2-K2O相关图解和QAP图解

      图b中:1a.硅英岩(石英岩);1b.富石英花岗岩类;2.碱长花岗岩;3a.花岗岩(正长花岗岩);3b.花岗岩(二长花岗岩);4.花岗闪长岩;5.英云闪长岩;6*.石英碱长正长岩;6.碱长正长岩;7*.石英正长岩;7.正长岩;8*.石英二长岩;8.二长岩;9*.石英二长闪长岩、石英二长辉长岩;9.二长闪长岩、二长辉长岩;10*.石英闪长岩、石英辉长岩、石英斜长岩;10.闪长岩、辉长岩、斜长岩.图a据Rickwood(1989),图b据Streckeisen(1976)Le Maitre et al.(1989)

      Fig.  5.  SiO2-K2O (a) and QAP (b) of the granitic complex from Lianshanguan area in Liaodong Peninsula

      图  6  辽东连山关地区花岗杂岩的稀土配分曲线(a)和微量蛛网图(b)

      标准值据Sun and Mcdonough(1989)

      Fig.  6.  Rare earth element distribution curves (a) and trace element spider diagram (b) for granitic complex sampled from Lianshanguan area in Liaodong Peninsula

      图  7  辽东连山关地区花岗杂岩的ACF图解(a)和A/MF-C/MF图解(b)

      图b据Altherr et al.(2000)

      Fig.  7.  ACF (a) and A/MF-C/MF (b) of the granitic complex from Lianshanguan area in Liaodong Peninsula

      图  8  辽东连山关地区花岗杂岩的锆石Lu-Hf同位素特征图解

      图a和b据Yang et al.(2006)

      Fig.  8.  Zircon Lu-Hf isotope characteristics diagram of the granitic complex from Lianshanguan area in Liaodong Peninsula

      附表 1  辽东连山关地区花岗杂岩锆石SHRIMP U-Pb年龄数据

      附表 1.   SHRIMP zircon U-Pb dating of the the granitic complex sampled from Lianshanguan area in Liaodong Peninsula

      Spot 206Pbc
      (%)
      10-6 232Th/
      238U
      206Pb*
      (10-6)
      207Pb*/
      206Pb*
      1σ
      (%)
      207Pb*/
      235U
      1σ
      (%)
      206Pb*/
      238U
      1σ
      (%)
      Err
      corr
      206Pb/238U 207Pb/206Pb Disc.
      (%)
      U Th (Ma) (Ma)
      TW6-1-1.1 0.01 1 363 731 0.55 332 0.135 61 0.47 5.31 1.5 0.283 8 1.4 0.948 1 610 ±20 2 171.9 ±8.1 26
      TW6-1-2.1 0.71 982 467 0.49 345 0.158 05 0.59 8.85 1.5 0.405 9 1.4 0.924 2 196 ±27 2 434.9 ±10.0 10
      TW6-1-3.1 0.11 643 576 0.93 252 0.164 61 0.53 10.34 1.6 0.455 5 1.5 0.945 2 420 ±31 2 503.6 ±8.9 3
      TW6-1-4.1 0.02 1 491 70 0.05 443 0.148 80 0.51 7.09 1.7 0.345 5 1.6 0.955 1 913 ±27 2 332.2 ±8.7 18
      TW6-1-5.1 0.18 834 831 1.03 289 0.157 61 0.60 8.75 1.8 0.402 8 1.7 0.942 2 182 ±31 2 430.0 ±10.0 10
      TW6-1-6.1 0.91 990 88 0.09 220 0.132 00 0.85 4.67 1.8 0.256 7 1.6 0.881 1 473 ±21 2 124.0 ±15.0 31
      TW6-1-7.1 0.03 1 070 213 0.21 400 0.162 67 0.45 9.75 1.5 0.434 6 1.4 0.955 2 326 ±28 2 483.7 ±7.5 6
      TW6-1-8.1 0.06 361 296 0.85 144 0.164 12 0.56 10.53 1.6 0.465 2 1.4 0.932 2 462 ±30 2 498.5 ±9.5 1
      TW6-1-9.1 0.40 1 447 72 0.05 398 0.144 71 0.58 6.36 1.5 0.318 7 1.4 0.920 1 783 ±21 2 284.4 ±10.0 22
      TW6-1-10.1 - 1 540 87 0.06 426 0.143 08 0.42 6.35 1.4 0.321 9 1.3 0.954 1 799 ±21 2 264.8 ±7.3 21
      TW6-1-11.1 0.70 773 485 0.65 294 0.201 00 0.60 12.17 1.5 0.439 2 1.4 0.915 2 347 ±27 2 834.3 ±9.8 17
      TW6-1-12.1 2.98 272 98 0.37 89 0.153 00 1.80 7.75 2.3 0.367 3 1.4 0.617 2 017 ±25 2 380.0 ±31.0 15
      TW6-1-13.1 0.71 1 485 179 0.12 300 0.127 63 0.63 4.11 1.5 0.233 3 1.3 0.903 1 352 ±16 2 066.0 ±11.0 35
      TW6-1-14.1 0.71 944 72 0.08 176 0.130 69 0.70 3.88 1.5 0.215 4 1.3 0.884 1 257 ±15 2 107.0 ±12.0 40
      TW6-1-15.1 0.15 400 127 0.33 149 0.161 70 0.67 9.64 1.5 0.432 4 1.4 0.898 2 316 ±27 2 474.0 ±11.0 6
      TW6-1-16.1 0.06 2 081 207 0.10 366 0.097 96 0.62 2.76 1.5 0.204 4 1.3 0.907 1 199 ±15 1 586.0 ±12.0 24
      TW6-1-17.1 0.30 1 628 140 0.09 357 0.129 80 0.50 4.55 1.4 0.254 2 1.3 0.936 1 460 ±17 2 095.2 ±8.8 30
      TW6-1-18.1 0.33 1 600 871 0.56 316 0.120 47 0.53 3.81 1.4 0.229 1 1.3 0.929 1 330 ±16 1 963.2 ±9.5 32
      TW6-2-1.1 0.23 149 247 1.71 59 0.165 60 0.97 10.52 1.8 0.461 0 1.6 0.852 2 444 ±32 2 513.0 ±16.0 3
      TW6-2-2.1 0.87 544 82 0.16 115 0.140 40 0.86 4.73 1.6 0.244 3 1.4 0.851 1 409 ±18 2 232.0 ±15.0 37
      TW6-2-3.1 1.70 389 66 0.17 102 0.149 30 1.30 6.18 2.0 0.300 3 1.5 0.762 1 693 ±22 2 338.0 ±22.0 28
      TW6-2-4.1 0.45 426 146 0.35 109 0.151 10 0.78 6.20 1.7 0.297 8 1.5 0.888 1 680 ±22 2 358.0 ±13.0 29
      TW6-2-5.1 0.05 311 103 0.34 110 0.160 50 0.65 9.10 1.7 0.411 4 1.6 0.921 2 221 ±29 2 461.0 ±11.0 10
      TW6-2-6.1 0.19 483 305 0.65 151 0.156 47 0.61 7.84 1.6 0.363 5 1.4 0.920 1 999 ±25 2 418.0 ±10.0 17
      TW6-2-7.1 0.24 468 94 0.21 136 0.155 20 0.66 7.24 1.6 0.338 3 1.4 0.909 1 878 ±24 2 404.0 ±11.0 22
      TW6-2-8.1 0.25 344 291 0.88 139 0.165 60 0.62 10.71 1.6 0.469 2 1.5 0.921 2 480 ±30 2 514.0 ±10.0 1
      TW6-2-9.1 0.33 560 358 0.66 194 0.159 88 0.58 8.87 1.5 0.402 5 1.4 0.925 2 180 ±26 2 454.4 ±9.9 11
      TW6-2-10.1 0.73 241 60 0.26 84 0.159 10 1.10 8.87 1.9 0.404 4 1.5 0.797 2 189 ±27 2 446.0 ±19.0 11
      TW6-2-8.2 0.02 523 88 0.17 147 0.153 16 0.54 6.93 1.5 0.328 3 1.4 0.932 1 830 ±22 2 381.5 ±9.2 23
      TW6-2-10.2 0.06 400 73 0.19 126 0.157 53 0.59 7.95 1.5 0.366 1 1.4 0.922 2 011 ±24 2 429.0 ±10.0 17
      TW6-2-11.1 0.49 645 98 0.16 155 0.145 96 0.65 5.58 1.5 0.277 4 1.4 0.902 1 578 ±19 2 299.0 ±11.0 31
      TW6-2-12.1 0.06 491 180 0.38 141 0.153 34 0.56 7.05 1.5 0.333 4 1.4 0.926 1 855 ±22 2 383.5 ±9.6 22
      TW6-2-13.1 0.05 251 123 0.51 99 0.164 60 1.10 10.39 1.8 0.457 8 1.4 0.799 2 430 ±29 2 503.0 ±18.0 3
      TW6-2-14.1 0.01 465 103 0.23 166 0.159 58 0.53 9.11 1.5 0.414 1 1.4 0.933 2 234 ±26 2 451.2 ±8.9 9
      TW6-2-15.1 0.14 226 164 0.75 87 0.164 90 0.66 10.17 1.6 0.447 2 1.4 0.907 2 383 ±28 2 506.0 ±11.0 5
      TW6-2-16.1 - 825 77 0.10 254 0.151 02 0.46 7.47 1.4 0.359 0 1.3 0.944 1 977 ±22 2 357.5 ±7.9 16
      TW6-2-15.2 - 776 71 0.09 238 0.153 21 0.47 7.55 1.4 0.357 6 1.3 0.941 1 971 ±22 2 382.1 ±8.0 17
      下载: 导出CSV

      附表 2  辽东连山关地区花岗杂岩的主量元素含量(%)

      附表 2.   Major elements (%) data for the granitic complex from Lianshanguan area in Liaodong Peninsula

      样品号 Ls611 Ls612 Ls613 Ls614 Fj621 Fj622 Fj623 Fj624
      SiO2 72.70 72.06 72.32 69.28 71.01 65.90 66.03 65.53
      TiO2 0.23 0.22 0.24 0.24 0.33 0.67 0.68 0.62
      Al2O3 13.68 14.08 14.33 15.92 14.13 14.49 14.63 14.90
      Fe2O3 2.27 2.05 2.11 2.21 3.76 6.56 6.42 6.42
      MnO 0.033 0.029 0.039 0.040 0.051 0.074 0.075 0.076
      MgO 0.53 0.47 0.50 0.58 1.26 2.56 2.47 2.37
      CaO 0.52 0.50 0.59 0.63 1.32 1.53 1.67 1.77
      Na2O 2.96 2.94 2.77 3.09 3.57 3.95 4.23 3.62
      K2O 6.25 6.68 6.24 7.12 3.90 3.38 2.95 3.71
      P2O5 0.120 0.120 0.100 0.120 0.071 0.067 0.075 0.110
      FeO 1.26 1.03 1.03 0.99 2.70 4.67 4.45 4.58
      LOI 0.56 0.71 0.63 0.67 0.46 1.18 1.13 1.24
      A/CNK 1.089 1.085 1.158 1.143 1.131 1.121 1.110 1.129
      σ43 2.86 3.19 2.77 3.96 2.01 2.43 2.31 2.47
      Q 29.18 27.31 29.93 21.65 28.51 19.27 19.38 19.47
      An 1.79 1.72 2.24 2.33 5.98 6.88 7.52 7.83
      Ab 24.88 24.86 23.38 26.08 29.58 32.21 34.59 29.61
      Or 36.75 39.45 36.79 41.99 22.60 19.28 16.83 21.15
      下载: 导出CSV

      附表 3  辽东连山关地区花岗杂岩的微量元素含量(10-6)

      附表 3.   Major trace and rare-earth elements (10-6) data for the granitic complex from Lianshanguan area in Liaodong Peninsula

      样品号 Ls611 Ls612 Ls613 Ls614 Fj621 Fj622 Fj623 Fj624
      Cr 3 3 7 2 62 131 128 110
      Ni 2.72 2.41 1.91 2.07 21.90 49.10 49.90 45.50
      Rb 283 299 285 334 145 175 175 191
      Sr 85.7 88.2 87.5 94.6 258.0 234.0 232.0 272.0
      Zr 222 207 224 240 69 228 158 150
      Nb 11.1 11.4 11.5 13.4 12.2 13.3 18.8 18.1
      Ba 702 723 689 801 870 596 430 615
      Hf 6.09 5.52 5.07 4.75 1.82 5.79 3.77 4.25
      Ta 1.82 2.15 1.94 1.12 1.13 1.23 1.13 0.95
      Th 20.0 19.4 21.5 17.8 4.7 18.9 13.8 9.7
      U 7.94 7.82 8.49 7.47 0.50 1.15 1.77 0.76
      Li 5.94 5.83 5.86 5.52 16.10 26.80 25.90 25.50
      Be 1.69 1.78 1.70 2.14 1.81 2.38 2.26 2.21
      Co 2.68 2.50 2.74 2.92 10.70 16.20 16.90 15.70
      V 17.9 19.1 18.8 16.4 46.6 90.7 83.9 83.9
      Ga 18.0 18.2 17.6 19.1 16.4 22.0 21.0 21.1
      Y 22.5 20.2 19.7 19.5 4.7 6.5 5.2 7.1
      La 61.7 54.8 74.7 65.1 13.3 160.0 94.1 58.0
      Ce 126 114 147 141 18 207 122 77
      Pr 11.9 10.4 14.5 12.5 1.9 19.5 11.6 7.2
      Nd 39.3 33.7 47.9 40.3 6.4 57.8 34.9 21.6
      Sm 7.01 6.02 8.37 6.82 1.07 6.17 3.69 2.80
      Eu 0.82 0.81 0.91 0.90 1.20 1.35 0.96 1.04
      Gd 5.91 5.00 6.99 5.78 0.97 6.44 4.01 2.76
      Tb 0.81 0.68 0.91 0.78 0.14 0.52 0.34 0.29
      Dy 4.36 3.68 4.68 3.92 0.80 1.53 1.12 1.28
      Ho 0.79 0.67 0.83 0.70 0.16 0.23 0.18 0.24
      Er 1.95 1.68 2.15 1.72 0.39 0.65 0.55 0.61
      Tm 0.36 0.30 0.38 0.32 0.08 0.08 0.07 0.11
      Yb 2.01 1.69 2.05 1.72 0.41 0.49 0.46 0.61
      Lu 0.27 0.22 0.28 0.24 0.06 0.08 0.07 0.10
      ∑REE 263.1 233.2 311.8 281.9 45.3 461.7 274.2 173.1
      LREE 246.6 219.3 293.5 266.8 42.3 451.6 267.4 167.1
      HREE 16.45 13.93 18.29 15.17 3.00 10.03 6.80 5.99
      LREE/HREE 14.99 15.75 16.05 17.59 14.10 45.01 39.33 27.89
      LaN/YbN 22.06 23.23 26.12 27.15 23.35 233.19 148.02 68.23
      δEu 0.38 0.43 0.36 0.43 3.55 0.65 0.76 1.13
      下载: 导出CSV

      附表 4  辽东连山关地区花岗杂岩的锆石Hf同位素含量

      附表 4.   Hf isotope data of the granitic complex from Lianshanguan area in Liaodong Peninsula

      No. Age
      (Ma)
      176Yb/
      177Hf
      176Lu/
      177Hf
      176Hf/
      177Hf
      2σ 176Hf/
      177Hfi
      εHf(0) εHf(t) TDM
      (Ma)
      TDMC
      (Ma)
      fLu/Hf
      TW6-1-1.1.xls 2 171.9 0.038 034 0.001 359 0.280 934 0.000 013 0.280 892 -65.81 -19.30 3 283 3 585 -0.96
      TW6-1-2.1.xls 2 434.9 0.035 446 0.001 226 0.280 858 0.000 013 0.280 806 -68.50 -15.99 3 375 3 634 -0.96
      TW6-1-3.1.xls 2 503.6 0.030 484 0.001 124 0.280 833 0.000 013 0.280 781 -69.38 -15.19 3 400 3 650 -0.97
      TW6-1-4.1.xls 2 332.2 0.028 424 0.001 082 0.280 923 0.000 010 0.280 884 -66.20 -15.73 3 274 3 539 -0.97
      TW6-1-5.1.xls 2 430.0 0.029 336 0.001 003 0.280 890 0.000 014 0.280 848 -67.36 -14.60 3 312 3 562 -0.97
      TW6-1-6.1.xls 2 124.0 0.016 900 0.000 723 0.281 229 0.000 012 0.281 209 -55.38 -8.96 2 833 3 041 -0.98
      TW6-1-7.1.xls 2 483.7 0.041 605 0.001 479 0.280 941 0.000 015 0.280 876 -65.56 -12.39 3 284 3 498 -0.96
      TW6-1-8.1.xls 2 498.5 0.028 721 0.001 028 0.280 910 0.000 014 0.280 861 -66.66 -12.40 3 287 3 511 -0.97
      TW6-1-9.1.xls 2 284.4 0.051 533 0.001 798 0.280 905 0.000 014 0.280 844 -66.83 -18.54 3 361 3 638 -0.95
      TW6-1-10.1.xls 2 264.8 0.036 996 0.001 306 0.280 889 0.000 012 0.280 845 -67.40 -18.78 3 340 3 634 -0.96
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