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    大别山皇城山银矿区及外围陈棚组火山岩U-Pb年代学、地球化学和成矿构造背景

    朱江 吴昌雄 彭三国 彭练红 张闯 刘锦明

    朱江, 吴昌雄, 彭三国, 彭练红, 张闯, 刘锦明, 2018. 大别山皇城山银矿区及外围陈棚组火山岩U-Pb年代学、地球化学和成矿构造背景. 地球科学, 43(7): 2404-2419. doi: 10.3799/dqkx.2018.187
    引用本文: 朱江, 吴昌雄, 彭三国, 彭练红, 张闯, 刘锦明, 2018. 大别山皇城山银矿区及外围陈棚组火山岩U-Pb年代学、地球化学和成矿构造背景. 地球科学, 43(7): 2404-2419. doi: 10.3799/dqkx.2018.187
    Zhu Jiang, Wu Changxiong, Peng Sanguo, Peng Lianhong, Zhang Chuang, Liu Jinming, 2018. Geochronology and Geochemistry of Volcanic Rocks from the Huangchengshan Volcanogenic Epithermal Silver Deposit, Dabie Orogen, China: Implications for Tectonic Setting. Earth Science, 43(7): 2404-2419. doi: 10.3799/dqkx.2018.187
    Citation: Zhu Jiang, Wu Changxiong, Peng Sanguo, Peng Lianhong, Zhang Chuang, Liu Jinming, 2018. Geochronology and Geochemistry of Volcanic Rocks from the Huangchengshan Volcanogenic Epithermal Silver Deposit, Dabie Orogen, China: Implications for Tectonic Setting. Earth Science, 43(7): 2404-2419. doi: 10.3799/dqkx.2018.187

    大别山皇城山银矿区及外围陈棚组火山岩U-Pb年代学、地球化学和成矿构造背景

    doi: 10.3799/dqkx.2018.187
    基金项目: 

    中国地质调查局项目 121201009000150013

    中国地质调查局项目 121201009000160902

    详细信息
      作者简介:

      朱江(1985-), 男, 博士, 高级工程师, 主要从事矿床学、矿产普查与勘探研究

    • 中图分类号: P588.1;P597

    Geochronology and Geochemistry of Volcanic Rocks from the Huangchengshan Volcanogenic Epithermal Silver Deposit, Dabie Orogen, China: Implications for Tectonic Setting

    • 摘要: 皇城山银矿床是西大别山地区代表性的浅成低温热液矿床,受陈棚组火山机构的枝叉状裂隙构造控制.目前人们对该矿床成因、成矿时间和构造环境的理解尚不深刻,因此对相关火山岩进行了激光等离子质谱(LA-ICP-MS)锆石U-Pb测年、元素地球化学和Sr-Nd-Hf同位素研究,探讨了其岩石成因和构造属性.结果表明,皇城山矿区陈棚组熔结凝灰岩及外围流纹岩锆石U-Pb年龄分别为133.4±1.5 Ma(MSWD=1.3)和133.1±0.8 Ma(MSWD=0.59),形成于早白垩世.陈棚组火山岩在较短时间内喷发形成,其喷发时限基本代表了皇城山银矿床形成时间.陈棚组流纹岩具高硅(SiO2=73.83%~77.38%)、高钾(K2O=4.65%~9.31%)特征,属于过铝质(A/CNK=1.09~1.31)和高钾钙碱性岩石系列.岩石具轻稀土富集,重稀土平坦,大离子亲石元素相对富集,Ba、Nb、Ta、P、Ti明显负异常和负Eu异常(δEu=0.33~0.88)特点.岩石锶同位素初始比值ISr为0.708 220~0.708 741,εNdt)值为-17.2~-18.5,Nd两阶段模式年龄TDM2=2.32~2.43 Ga.锆石εHft)值范围为-22.3~-26.1,Hf两阶段模式年龄TDM2=2.29~2.49 Ga.主、微量元素和Sr-Nd-Hf同位素特征共同揭示陈棚组流纹岩为扬子陆壳北缘古老地壳物质重熔演化的产物.结合区域地质特征,陈棚组火山岩及其相关皇城山银矿床形成于大别山早白垩世加厚下地壳拆沉作用初期、挤压向伸展转化环境.

       

    • 图  1  大别造山带北淮阳构造带火山岩分布及构造格架

      李双应(2004)李鑫浩等(2015)修改

      Fig.  1.  Tectonic sketch of the northern Huaiyang belt showing the distribution of volcanic rocks

      图  2  皇城山银矿区地质简图

      Fig.  2.  Geological sketch of the Huangchengshan silver deposit

      图  3  陈棚组岩屑晶屑熔结凝灰岩(a, b)和流纹岩(c, d)野外和显微照片

      a.赋矿陈棚组岩屑晶屑熔结凝灰岩野外照片,可见火山熔岩角砾和火山沉积构造;b.流纹岩野外照片;c.岩屑晶屑熔结凝灰岩单偏光显微照片,见火山沉积结构和气孔构造;d.流纹岩正交偏光显微照片,见斑状结构和气孔构造.Or.正长石;Pl.斜长石;Qz.石英

      Fig.  3.  Hand specimens and Photomicrographs of the ignimbrite (a, b) and rhyolite (c, d) from the Chenpeng Formation

      图  4  陈棚组熔结凝灰岩(a)和流纹岩(b)代表性锆石阴极发光(CL)图像

      实线圆为锆石U-Pb测点,虚线圆为锆石Lu-Hf测点.图中锆石上方为测得U-Pb年龄,锆石下方为测得εHf(t)值

      Fig.  4.  Cathodoluminescence (CL) images of representative zircons for the ignimbrite (a) and rhyolite (b) from the Chenpeng Formation

      图  5  陈棚组岩屑晶屑熔结凝灰岩(a, b)和流纹岩(c, d)锆石U-Pb年龄

      岩屑晶屑熔结凝灰岩(样品HCS-1)的4颗捕获或继承锆石数据点未显示

      Fig.  5.  U-Pb concordia diagrams and weighted mean ages for the the ignimbrite (a, b) and rhyolite (c, d) from the Chenpeng Formation

      图  6  陈棚组流纹岩主量元素图解

      陈棚组数据依据张四清等,1:5万文殊寺幅地质图说明书.河南省地质矿产勘查开发局第3地质调查队,2001年5月

      Fig.  6.  Major element diagrams for the rhyolite from the Chenpeng Formation

      图  7  陈棚组流纹岩稀土元素配分图(a)和微量元素原始地幔标准化蛛网图(b)

      图a标准化值据Boynton(1984);图b标准化值据Sun and Mcdonough(1989)

      Fig.  7.  Chondrite-normalized REE pattern (a) and primitive mantle-normalized trace elements diagram (b) for the rhyolite from the Chenpeng Formation

      图  8  陈棚组流纹岩和英安岩全岩Sr-Nd同位素组成

      底图据John et al.(1999)、赵子福和郑永飞(2009)陈伟等(2013)修改.数据来源:华北地块下地壳、中上地壳和扬子地块下地壳范围引自John et al.(1999);中生代花岗岩范围赵子福和郑永飞(2009).陈棚组流纹岩数据为本文实测,英安岩数据杨梅珍等(2012)

      Fig.  8.  εNd(t) vs. (87Sr/86Sr)i diagram for the rhyolite from the Chenpeng Formation

      图  9  陈棚组流纹岩的锆石εHf(t)-t图解

      毛坦厂组安山岩锆石εHf(t)数据为笔者实测(未发表)

      Fig.  9.  Zircon εHf(t)-t vs. age diagram for the rhyolite from the Chenpeng Formation

      图  10  北淮阳晚中生代火山岩带不同地区火山岩形成时代

      年龄数据同表 5

      Fig.  10.  Ages of the volcanic rocks in different tectonic units of the northern Huaiyang area, Dabie orogenic belt

      表  1  陈棚组火山岩LA-ICP-MS锆石U-Pb同位素测定结果

      Table  1.   LA-ICP-MS zircon isotopic U-Pb data for the volcanic rocks from the Chenpeng Formation

      样品 元素含量(10-6) 同位素比值 年龄(Ma)
      Pb Th U Th/U 207Pb/206Pb 1σ 207Pb/235U 1σ 206Pb/238U 1σ 207Pb/206Pb 1σ 207Pb/235U 1σ 206Pb/238U 1σ
      HCS-20:赋矿岩屑晶屑熔结凝灰岩
      HCS-20@01 43 527 550 0.96 0.052 8 0.004 4 0.149 1 0.014 0 0.020 0 0.000 5 318 208 141 12 128 3
      HCS-20@02 130 1 240 2 478 0.50 0.048 6 0.002 4 0.144 2 0.007 1 0.021 6 0.000 4 127 105 137 6 138 2
      HCS-20@03 53 373 1 834 0.20 0.052 2 0.003 4 0.150 5 0.009 1 0.021 1 0.000 4 292 137 142 8 135 2
      HCS-20@04 197 2 082 2 847 0.73 0.052 6 0.002 2 0.155 4 0.006 5 0.021 2 0.000 3 310 92 147 6 135 2
      HCS-20@05 195 1 876 3 358 0.56 0.052 4 0.002 1 0.152 8 0.006 2 0.020 9 0.000 3 303 90 144 5 133 2
      HCS-20@06 171 1 716 3 413 0.50 0.047 3 0.002 0 0.136 0 0.005 9 0.020 9 0.000 4 66 88 129 5 133 2
      HCS-20@07 159 1 841 1 718 1.07 0.053 2 0.002 7 0.151 7 0.007 7 0.020 7 0.000 3 338 112 143 7 132 2
      HCS-20@08 195 1 821 2 937 0.62 0.050 5 0.003 7 0.145 2 0.010 3 0.020 9 0.000 3 217 166 138 9 133 2
      HCS-20@09 339 2 881 4 320 0.67 0.052 4 0.003 7 0.152 4 0.010 4 0.021 1 0.000 3 304 161 144 9 134 2
      HCS-20@10 22 65 1 072 0.06 0.053 8 0.004 2 0.155 3 0.011 4 0.021 2 0.000 4 361 165 147 10 135 2
      HCS-20@11 221 1 228 3 188 0.39 0.047 7 0.004 0 0.134 5 0.011 0 0.020 5 0.000 3 83 186 128 10 131 2
      HCS-20@12 269 1 439 4 267 0.34 0.061 3 0.008 0 0.173 2 0.022 5 0.020 5 0.000 3 649 294 162 20 131 2
      HCS-20@13 768 541 1 193 0.45 0.127 0 0.003 0 5.009 4 0.167 6 0.286 0 0.007 8 2 057 42 1 821 28 1 621 39
      HCS-20@14 43 96 129 0.75 0.067 9 0.004 5 0.991 8 0.069 7 0.105 4 0.002 8 866 137 700 36 646 17
      HCS-20@15 686 2 113 2 191 0.96 0.072 1 0.002 4 0.601 6 0.029 5 0.058 9 0.001 9 991 67 478 19 369 11
      HCS-20@16 56 437 1 372 0.32 0.049 9 0.003 4 0.177 2 0.013 1 0.025 5 0.000 6 191 153 166 11 163 4
      D001-3:流纹岩
      D001-3@01 110 924 751 1.23 0.049 5 0.001 8 0.143 9 0.005 1 0.021 0 0.000 2 169 83 136 5 134 2
      D001-3@02 423 3 691 1 849 2.00 0.049 3 0.001 4 0.140 9 0.003 9 0.020 7 0.000 2 161 64 134 3 132 1
      D001-3@03 118 917 663 1.38 0.049 2 0.001 8 0.141 3 0.005 1 0.020 9 0.000 3 167 82 134 5 133 2
      D001-3@04 362 3 159 1 685 1.88 0.049 4 0.001 3 0.142 2 0.004 0 0.020 8 0.000 2 165 63 135 4 132 1
      D001-3@05 45 378 232 1.63 0.047 3 0.003 3 0.133 7 0.008 6 0.020 5 0.000 4 65 156 127 8 131 3
      D001-3@06 233 1 937 1 309 1.48 0.049 1 0.001 5 0.139 4 0.004 5 0.020 5 0.000 2 154 77 132 4 131 2
      D001-3@07 224 1 871 1 191 1.57 0.047 3 0.001 8 0.134 5 0.005 0 0.020 6 0.000 3 61 89 128 4 132 2
      D001-3@08 280 2 375 1 471 1.61 0.049 3 0.001 4 0.142 3 0.004 1 0.020 9 0.000 2 161 64 135 4 133 1
      D001-3@09 51 417 386 1.08 0.047 2 0.002 2 0.135 0 0.005 7 0.020 9 0.000 3 58 107 129 5 134 2
      D001-3@10 242 1 884 1 231 1.53 0.049 9 0.001 4 0.144 1 0.004 2 0.020 9 0.000 3 191 65 137 4 133 2
      D001-3@11 286 2 526 1 574 1.60 0.049 6 0.001 5 0.143 1 0.004 3 0.020 9 0.000 2 176 77 136 4 133 1
      D001-3@12 160 1 332 927 1.44 0.048 7 0.002 1 0.140 3 0.006 0 0.020 9 0.000 3 132 99 133 5 133 2
      D001-3@13 225 1 949 1 224 1.59 0.047 7 0.001 3 0.138 1 0.003 8 0.021 0 0.000 2 83 65 131 3 134 1
      D001-3@14 52 440 283 1.56 0.049 6 0.003 6 0.140 6 0.009 5 0.020 9 0.000 4 176 168 134 8 133 2
      D001-3@15 520 4 123 1 999 2.06 0.053 0 0.003 6 0.154 2 0.010 3 0.021 1 0.000 2 330 157 146 9 135 1
      下载: 导出CSV

      表  2  陈棚组流纹岩主量元素(%)和微量、稀土元素(10-6)分析结果

      Table  2.   Major elements (%), trace elements (10-6) and rare earth elements (10-6) of the rhyolite from the Chenpeng Formation

      样号 D001-1 D001-2 D001-3 D001-4 D004-2
      岩性 流纹岩 流纹岩 流纹岩 流纹岩 流纹岩
      SiO2 76.67 76.16 77.38 77.17 73.83
      TiO2 0.11 0.14 0.12 0.12 0.06
      Al2O3 12.44 12.83 12.32 12.34 13.86
      Fe2O3 0.72 0.78 0.63 0.55 0.91
      FeO 0.63 0.58 0.52 0.55 0.58
      MnO 0.05 0.04 0.04 0.03 0.03
      MgO 0.15 0.16 0.12 0.12 0.22
      CaO 0.36 0.30 0.28 0.28 0.10
      Na2O 3.04 3.50 3.38 3.34 0.22
      K2O 5.05 5.10 4.65 4.77 9.31
      P2O5 0.02 0.02 0.02 0.03 0.03
      Total 99.25 99.61 99.46 99.29 99.13
      LOI 0.48 0.11 0.24 0.41 0.55
      A/NK 1.19 1.14 1.16 1.16 1.33
      A/CNK 1.12 1.09 1.11 1.11 1.31
      La 27.80 34.50 20.10 20.30 4.08
      Ce 45.50 56.30 37.10 35.80 8.27
      Pr 4.02 5.37 3.00 3.01 1.07
      Nd 9.34 13.50 7.05 7.12 3.16
      Sm 1.38 2.13 1.05 1.05 0.63
      Eu 0.14 0.23 0.13 0.13 0.15
      Gd 1.22 1.69 0.94 0.94 0.43
      Tb 0.18 0.26 0.15 0.15 0.08
      Dy 1.10 1.55 0.93 0.96 0.44
      Ho 0.24 0.31 0.21 0.22 0.09
      Er 0.78 0.98 0.67 0.72 0.30
      Tm 0.15 0.17 0.13 0.13 0.06
      Yb 1.12 1.24 0.98 1.02 0.54
      Lu 0.17 0.17 0.14 0.15 0.09
      Y 7.48 8.99 6.35 6.59 3.59
      Li 4.00 2.94 2.96 9.86 15.60
      Cr 13.20 4.89 4.58 15.30 4.36
      Co 1.54 2.05 1.08 <1 1.20
      Ni 4.46 4.85 2.98 3.13 4.53
      Ga 15.20 15.90 15.10 16.00 36.60
      Nb 15.40 15.50 14.20 15.30 12.80
      Mo 1.20 0.77 0.39 0.48 0.44
      Ta 1.34 1.44 1.26 1.33 1.18
      Th 8.66 11.00 8.67 22.00 32.30
      U 3.46 4.96 2.63 3.11 14.90
      Cl 53.80 58.70 80.40 45.60 82.00
      Ba 75.20 157.00 189.00 186.00 354.00
      Hf 4.46 4.67 4.23 4.47 16.50
      Pb 36.70 42.60 92.10 113.00 69.00
      Rb 176.00 156.00 141.00 159.00 570.00
      Sr 42.60 113.00 53.30 52.20 22.60
      Zr 85.40 99.60 80.30 86.60 152.00
      Cs 1.74 1.45 1.04 1.09 11.50
      As 1.01 0.78 0.70 0.78 3.66
      Sb 0.17 0.10 0.16 0.10 0.32
      Bi 0.07 0.05 0.23 0.20 0.25
      Be 3.37 1.48 1.86 2.06 2.68
      V 2.51 4.51 4.18 3.66 6.41
      Sc 3.66 4.61 4.53 4.17 4.92
      Cu 8.46 8.29 9.48 5.79 10.20
      Zn 11.20 11.00 113.00 99.60 54.30
      Au 0.46 0.59 0.51 0.56 11.90
      Ag 0.09 0.07 0.24 0.13 56.00
      F 337.00 439.00 210.00 634.00 892.00
      ∑REE 93.14 118.40 72.58 71.70 19.39
      (La/Yb)N 17.80 19.96 14.71 14.28 5.42
      δEu 0.33 0.37 0.40 0.40 0.88
      δCe 1.06 1.01 1.17 1.12 0.97
      下载: 导出CSV

      表  3  陈棚组流纹岩全岩Sr-Nd同位素分析结果

      Table  3.   Whole rock Sr-Nd isotopic data of the rhyolite from the Chenpeng Formation

      样品 岩石
      类型
      年龄
      (Ma)
      Rb
      (10-6)
      Sr
      (10-6)
      87Rb/
      86Sr
      87Sr/
      86Sr
      ISr Sm
      (10-6)
      Nd
      (10-6)
      147Sm/
      144Nd
      143Nd/
      144Nd
      (143Nd/
      144Nd)i
      εNd(t) TDM2
      (Ga)
      D001-1 流纹岩 133 184.4 45.3 0.730 47 11.770 0.708 220 1.218 9.348 0.078 8 0.511 586 0.511 517 -18.5 2.43
      D001-3 流纹岩 133 158.4 57.2 0.723 58 7.995 0.708 466 1.244 10.010 0.075 2 0.511 614 0.511 549 -17.9 2.38
      D001-4 流纹岩 133 161.2 57.6 0.724 01 8.077 0.708 741 0.914 6.905 0.080 3 0.511 656 0.511 586 -17.2 2.32
      注:计算过程所用参数(147Sm/143Nd)CHUR=0.196 7;(143Nd/144Nd)CHUR=0.512 638;(147Sm/143Nd)DM=0.213 7;(143Nd/144Nd)DM=0.513 15.
      下载: 导出CSV

      表  4  陈棚组流纹岩的锆石Lu-Hf同位素LA-MC-ICP-MS原位分析结果

      Table  4.   LA-MC-ICP-MS zircon Lu-Hf isotopic data for the rhyolite from the Chenpeng Formation

      样品点 年龄(Ma) 176Lu/177Hf 176Yb/177Hf 176Hf/177Hf 1σ εHf(0) 1σ εHf(t) 1σ TDM2(Ga) fLu/Hf
      D001-3@01 134 0.001 890 0.092 306 0.282 055 0.000 011 -25.4 0.7 -22.6 0.7 2.30 -0.94
      D001-3@02 132 0.002 035 0.094 551 0.282 030 0.000 018 -26.2 0.8 -23.5 0.8 2.35 -0.94
      D001-3@04 132 0.002 192 0.103 828 0.282 049 0.000 019 -25.6 0.8 -22.9 0.8 2.31 -0.93
      D001-3@05 131 0.001 748 0.080 929 0.282 063 0.000 012 -25.1 0.7 -22.4 0.7 2.29 -0.95
      D001-3@08 133 0.002 032 0.103 773 0.282 043 0.000 013 -25.8 0.7 -23.0 0.7 2.32 -0.94
      D001-3@09 134 0.001 034 0.054 393 0.282 060 0.000 013 -25.2 0.7 -22.3 0.7 2.29 -0.97
      D001-3@10 133 0.002 037 0.101 663 0.282 046 0.000 016 -25.7 0.8 -23.0 0.8 2.32 -0.94
      D001-3@12 133 0.003 170 0.118 901 0.282 018 0.000 025 -26.7 1.0 -24.0 1.0 2.38 -0.90
      D001-3@13 134 0.002 736 0.113 463 0.281 957 0.000 025 -28.8 1.0 -26.1 1.0 2.49 -0.92
      D001-3@14 133 0.002 100 0.105 706 0.281 982 0.000 015 -27.9 0.7 -25.2 0.8 2.44 -0.94
      注:测试点序号与表 1测年点序号对应.
      下载: 导出CSV

      表  5  大别造山带北淮阳地区白垩纪火山岩年龄

      Table  5.   Ages of the Cretaceous volcanic rocks in the northern Huaiyang belt, Dabie orogenic belt

      组名 岩性 年龄值(Ma) 测试方法 数据来源
      陈棚组 石英安山岩 133.4±1.5 LA-ICP-MS锆石U-Pb 杨梅珍等(2012)
      熔结凝灰岩 133.1±1.5 LA-ICP-MS锆石U-Pb 本文
      流纹岩 133.1±0.8 LA-ICP-MS锆石U-Pb 本文
      英安斑岩 133.2±1.7 LA-ICP-MS锆石U-Pb 笔者实测,未发表
      金刚台 粗安岩 129±2.0 SHRIMP锆石U-Pb 黄丹峰等(2010)
      正长斑岩 129.2±0.7 LA-ICP-MS锆石U-Pb 黄皓和薛怀民(2012)
      熔结凝灰岩 128.8±0.7 LA-ICP-MS锆石U-Pb 黄皓和薛怀民(2012)
      粗面安山岩 127.6±0.5 LA-ICP-MS锆石U-Pb 黄皓和薛怀民(2012)
      流纹岩 127±3.6 SHRIMP锆石U-Pb 黄丹峰等(2010)
      流纹英安岩 127.5±0.6 LA-ICP-MS锆石U-Pb 李鑫浩等(2015)
      英安岩 124.8±2.3 LA-ICP-MS锆石U-Pb 李鑫浩等(2015)
      安山岩 123.3±0.7 LA-ICP-MS锆石U-Pb 李鑫浩等(2015)
      毛坦厂组 粗面质熔结凝灰岩 130.8±1.8 LA-ICP-MS锆石U-Pb 张定源等(2014)
      安山岩 126.7±1.4 LA-ICP-MS锆石U-Pb 朱江等(2017)
      晓天组 粗面岩 126.9±1.7 LA-ICP-MS锆石U-Pb 张定源等(2014)
      望母山组 粗面岩 126.7±1.4 LA-ICP-MS锆石U-Pb 张定源等(2014)
      下载: 导出CSV
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    • 收稿日期:  2017-08-22
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